T P F ILL1NOIS BULLETIN DECEMBER 22, 1908 No. 18 ;ond-class matter under Act of Congress July 16. 1894 J CIRCULAR NO. 3 FUEL TESTS WITH ILLINOIS COAL (COMPILED FROM TESTS MADE BY THE TECHNOLOGIC BRANCH OF THE UNITED STATES GEOLOGICAL SURVEY, AT THE ST. Louis FUEL TESTING PLANT, 1904 JUNE 30, 1907). BY L. P. BRECKENRIDGE AND PAUL DISERENS UNIVERSITY OF ILLINOIS ENGINEERING EXPERIMENT STATION URJBANA, ILLINOIS PUBLISHED BY THE UNIVERSITY <? UNIVERSITY OF ILLINOIS ENGINEERING EXPERIMENT STATION CIRCULAR No. 3 DECEMBER 1908 FUEL TESTS WITH ILLINOIS COAL (COMPILED FROM TESTS MADE BY THE TECHNOLOGIC BRANCH OF THE UNITED STATES GEOLOGICAL SURVEY, AT THE ST. Louis, Mo., FUEL TESTING PLANT, 1904-JuNE 30, 1907.) BY L. P. BRECKENRIDG,., DIRECTOR OF THE ENGINEERING EXPERIMENT STATION, ALSO CONSULTING ENGINEER, TECHNOLOGIC BRANCH, U. S. G. S. AND PAUL DISERENS, M. E. CONTENTS Page I. Introduction 2 II. A Summary of Conclusions 2 III. The Coals Tested 4 IV. Chemical Properties of the Coals Tested 9 V. Washing Tests 18 VT. Coking Tests 23 VII. Steaming Tests 26 VIII. Producer-Gas Tests 43 357045 EXPERIMENT STATION I INTRODUCTION The United States Geological Survey Technologic Branch has conducted at the St. Louis, Missouri, fuel testing plant, a series of investigations on the fuels of the United States. These tests included a large number of Illinois coals. The results of the tests have been published from time to time in a series of govern- ment bulletins which contain very full descriptions of methods and very complete details of the results obtained. A complete list of the government bulletins is given at the end of this publi- cation. The tests included: (a) Steaming tests under boilers (b) Producer-gas tests (c) Washing tests (d) Coking tests (e) Briquetting tests (f) Chemical tests for composition and heating values (g) Field work tests, sampling tests and a few other minor investigations. It is the purpose of this circular to present in compact form the important results of the government tests so far as these tests relate to Illinois coals. The Engineering Experiment Station hopes that by bringing together in one circular the tests made by the government on Illinois coals, it may do a service to the engi- neering, industrial and fuel interests of the State. The compiler has presented a few conclusions which seem justified by a study of the results recorded from tests already made. It is, however, fair to say that in a few cases the number of tests made is scarcely sufficient to warrant any general application of the con- clusions stated. II A SUMMARY OF CONCLUSIONS The results of the United States Geological Survey tests of Illinois coal, presented in the following pages, seem to justify the conclusions given below. 1. The chemical properties of the coals tested indicate that FUEL TESTS WITH ILLINOIS COAL 8 VG on a basis of the volatile-carbon total-carbon ratio (-77-), all Illi- G nois coals tested belong in Class B or Class D*. The maxi- mum value of this ratio is 33.4 per cent and the minimum value is 20.9 per cent. 2. The average calorific value of Illinois coal is 14319 B. t. u. per pound of pure coal (ash and moisture free). But few samples tested varied from this value by an amount more than 2 per cent. 3. The quality of Illinois coal is greatly increased by wash- ing. The reduction in ash and in sulphur is as follows: When raw coal contains 8% ash, the reduction in ash is 20%. When raw coal contains 12% ash, the reduction in ash is 30%. When raw.coal contains 16% ash, the reduction in ash is 43%. When raw coal contains 20% ash, the reduction in ash is 53%. When raw coal contains 2% sulphur, the reduction in sulphur is 13%. When raw coal contains 3% sulphur, the reduction in sulphur is 17%. When raw coal contains 4% sulphur, the reduction in sulphur is 22%. When raw coal contains 5% sulphur, the reduction in sulphur is 28%. 4. The material rejected by the washing jig contains I coal and i noncombustible refuse. 5. One-fourth of the coal tested may be used for the manu- facture of coke. 6. The evaporative efficiency of Illinois coal when burned in a hand-fired furnace under a water- tube boiler averages 62.7 per cent. This performance compares favorably with that of any other bituminous coal tested at the United States Geological laboratory. 7. The evaporative efficiency of Illinois coal is but slightly affected by the moisture contained in it. 8. The evaporative efficiency of Illinois coal decreases as the ash and sulphur increase. Each additional per cent of ash and sulphur results in 0.4 per cent decrease in efficiency. 9. The evaporative efficiency of Illinois coal, when burned in a hand-fired furnace, decreases as the per cent of fine coal con- tained in it increases. 10. Briquetting improves the evaporative efficiency of Illinois coal only when the raw coal is in the form of slack or screenings. 11. The performance of Illinois coal in a gas producer com- pares favorably with that of any other bituminous coal tested at the United States Geological Survey laboratory. 12. The value of Illinois coal as fuel for a gas-producer *Professor Parr's classification of coal, see page 11 of this circular. 4 ILLINOIS ENGINEERING EXPERIMENT STATION decreases as the ash contained in it increases and as the calorific value decreases. 13. In small plants it requires at least two and one-half times as much coal to develop one horse- power when used in steam boiler service as when used in gas producer service. 14. Gas producers can be continuously operated with Illinois coal developing one electrical horse-power with 1.7 Ib. of dry coal. Ill THE COALS TESTED 1. The mining centers and districts of Illinois, recognized by the trade and defined with reference to geographical position, have been described as follows.* (a) Williamson, Franklin, and Perry Counties. Williamson County led the production of the State in 1907 with more than 5,500,000 tons. No. 7, the Blue Band seam, which is from 5 to 10 feet thick, averaging 9 feet over a large area, is the greatest producer. It maintains an approximate uniformity in physical character and thickness but varies from place to place in fuel value. At Spillertown another seam, 4 feet thick, is mined 60 feet below No. 7. This seam is probably equivalent to No. 5 of Saline County and may have a wide distribution in the Williamson County district. (b) Sangamon, Macoupin, Christian, Logan, and Macon Counties. The Springfield district, extending into several adjoin- ing counties, has long been one of the most important. Sangamon produced more than 5,000,000 tons in 1907. The coal of the dis- trict is commonly known as No. 5, though recent work tends to confirm the suggestion that there are probably two distinct beds mined in this district, -No 5, in the area north of Chatham, and in No. 6 south of that town. The average thickness is a little less than 6 feet at Springfield, about 4.5 feet at Decatur and from 6 to 8 feet in Macoupin County. (c) St. Clair, Madison, Clinton, and Randolph Counties. St. Clair County produced more than 4,500,000 tons in 1907. This district, known as the Bellville district, is not sharply set off from its neighbors since the same coal bed is mined under similar con- ditions in adjoining counties. It is the Blue Band seam and has a thickness of from 5 to 7 feet over much of the area. The seam is reached by shafts from 100 to 300 feet deep. * The Coal Resources of Illinois, by Prank W. DeWolf , Amer. Inst. of Mining Engineers, October, 1908. FUEL TESTS WITH ILLINOIS COAL 5 (d) Vermilion County. During 1907 Vermilion County pro- duced nearly 3,000,000 tons. It has long been an important area, shipping principally to the Chicago market. There are three per- sistent seams, two of which are worked. The top or Danville, No. 7, appears west of Vermilion river and is mined along the outcrop and by shafts from 75 to 200 feet deep. The other, known as the Grape Creek coal, No. 6, lies from 20 to 80 feet below the Danville and is the more important of the two. (e) Saline County. Saline County is one of the newest and most rapidly growing producers. In 1907 its output was about 2,1*25,000 tons, a gain of 125 per cent over 1906. There are two seams, No. 7 and No. 5, underlying the northern two-thirds of this county and much of Gallatin on the east, each approximately 5 feet thick and lying 90 to 150 feet apart vertically. (/) Fulton and Peoria Counties. Fulton County produced more than 2,000,000 tons in 1907 and Peoria about half as much. Here the principal seam, called No. 5, is from 4 to 4.5 feet thick. Shafts reach the coal at from 75 to 150 feet. In all, seven beds are present. (g) La Salle, Bureau and Grundy Counties. The La Salle district includes three principal counties and produces more than 5,000,000 tons yearly. The largest production is by long- wall mining from seam No. 2, or the Third Vein. The coal averages 3 feet thick and is of good quality. About 140 feet above it, lies seam No. 5. It is about 4 feet thick. About 40 feet above No. 5 is seam No. 7. This is extensively mined by room-and- pillar methods. 2. The samples tested were procured from 5 of the 7 districts described in the preceding paragraph. They were furnished by the several coal mining companies of the state free of cost, and were shipped to the fuel testing laboratory under the supervision of an expert inspector whose chief care was to secure a sample for test- ing which fairly represented the normal product of the mine. The cars were numbered consecutively in the order of shipment, and this number has been retained as the laboratory designation of the sample. When two or more car lots consisting of different grades, such as lump, nut, etc., were shipped from the same mine, each lot was designated by a letter. For example, Illinois 11A is screened coal, 11B run-of-mine and 11C No. 5 washed coal, all from the same mine. A complete list of the car-load samples of Illinois coal re- ceived and tested is given in Table 1. In this table the location ILLINOIS ENGINEERING EXPERIMENT STATION r N Min gger Hollow No CCCO-H <y M < -2? OOO^ 66066 'S OO rr a ^ Co :6 o-o a : og o :: : s 2O -3 o :J ' bl o o : ZH : : : : d^- gW: - Sm ?l! : iS| SSv^to SS'S "?3 ^5- .2 '^ |: I O I. g :s S"S&|f- I PU!Z; 's I130O S 'O 'S 'H ;^^^^2: FUEL TESTS WITH ILLINOIS COAL a d >- . . . g|l, . g. d. |g or s"3 Jc/}> S a? occ ' b : : : -S -S |tf a da : S ^^c'B es ^a be ^sCa5 fl . ^^ : - c : |-a-g : <j X < ffi < S < 23 FUEL TESTS WITH ILLINOIS COAL 9 of the mine, the geological bed or seam and the name of the mine or its depth are given. Referring to the table it will be seen that fifty-three car samples from thirty-three different mines were tested, and that the mines are distributed throughout twelve of the principal coal mining counties of the State. The location of each mine is plotted on the map, Fig 1. A comparison of the coal output of the several localities de- signated in paragraph 2, with the number of mines submitting samples, shows that the coal tested is fairly representative and while it is true that two comparatively important coal producing localities are not included, the results of tests should be accepted as characteristic of Illinois coal in general. 3. The plan of the tests as adopted by the United States Geo- logical Survey included a complete chemical analysis of samples submitted, an investigation of the advantages of washing, an in- vestigation of the coking qualities of the coal, and a series of boiler and gas producer trials. In carrying out this plan each sample was tested under conditions as nearly identical as possible, and every effort was made to secure results which would admit of di- rect comparison. IV CHEMICAL PROPERTIES OF THE COALS TESTED To determine the chemical properties of the coals tested, samples were taken both from the working face of the mine and from each car-load shipped. 4. The mine samples were obtained as follows: After a gen- eral inspection of the mine to determine the variations of coal in thickness and in quality, two representative points were selected in opposite parts of the mine. The face of the coal at these places was cleaned in order to remove any weathered coal or powder smoke, and a cut made across the face of the coal from roof to floor, including all the benches mined and such impurities as were not removed in ordinary work. The coal obtained, amounting to 25 or 30 pounds, was pulverized and quartered down according to generally accepted rules, and the sample placed in an air-tight iron can. This was mailed to the chemical laboratory where it was received and analyzed within two or three days. 10 ILLINOIS ENGINEERING EXPERIMENT STATION 5. The car samples were obtained during the process of unload- ing at the testing plant. A quantity never less than 200 pounds and often as great as 600 pounds was collected, a shovelful at a time from every part of the car. This was thoroughly crushed and quartered down until 25 or 30 pounds remained , placed in an air- tight can and immediately shipped to the chemical laboratory. Here the sample was pulverized and again quartered until a con- venient amount for analysis was obtained . 6. The chemical work included calorific determinations, and ultimate and proximate analyses. The calorific value was deter- mined in duplicate for each car sample. A determination was also made for one of the two mine samples corresponding to each car- load. An ultimate analysis was made in duplicate on each car sample. The approximate analysis and the determination of sul- phur were made for practically every sample that came into the laboratory, and were made in duplicate for all car samples. 7. The results of the chemical analyses are given in Tables 2 and 3, (p. 12, et seq.) Column 1 gives the laboratory number, Col- umn 2 the U. S. G. S. number, Column 3, the coal bed or seam and Column 4, the location from which the sample was taken. Column 5 gives the designation of the sample. The proximate analysis is given in Columns 6 to 14. These results are given both for air- dry coal (Columns 7 to 10) and for pure coal (Columns 12 to 14). The calorific value is given in terms of dry coal in Column 11 and in terms of pure coal in Column 15. Referring to the latter it will be seen that the maximum value is 14900 and the minimum 13900, a range of about 6.7 per cent. The average, however, is 14319 and but few of the recorded values vary from this by an amount greater than two per cent. The ultimate analysis is given in Col- umns 16 to 21. For convenience in comparing the results this is put in terms of dry coal. Columns 22, 23 and 24 have been calcu- lated from the ultimate and proximate analyses. The combustible volatile is equal to the difference between the total volatile (Col- umn 12) and the inert volatile (Column 23). The inert volatile is equal to 100 minus the total carbon, the ash, the water, the sul- phur and the available hydrogen all divided by 100 minus the ash and water. The ratio of the volatile carbon to the total carbon (Column 24) is equal to total carbon as shown by the ultimate anal- ysis minus the fixed carbon as shown by the proximate analysis divided by the total carbon. FUEL TESTS WITH ILLINOIS COAL 11 The values included in Columns 22, 23 and 24 have been cal- culated in order to make possible a classification based on the ratio of volatile carbon to total carbon. This is the classification suggested by Professor S. W. Parr, and, in brief, is as follows.* VC Anthracite Proper Ratio -^- below 4% VC Anthracite Semi- Anthracite Ratio -~- between 4% and 8% VC Semi-Bituminous Ratio -^ between 10% and 15% VC A \ Ratio -^ from 20% to 32% ( Inert Volatile from 5% to 10% COAL Bituminous Proper Black Lignites Brown Lignites VC B j Ratio -~ from 20% to 27% Inert Volatile from 10% to 16% VC Ratio -^ from 32% to 44% Inert Volatile from 5% to 10% VC D _j Ratio -^ from 27% to 44% Inert Volatile from 10% to 16% Ratio from 27% up Inert Volatile from 16% to 20% VC* Ratio -^ from 27% up Inert Volatile from 20% to 30% It will be seen that in this system of classification all samples of Illinois coal tested fall in one of two divisions, bituminous B and bituminous D. In Table IV (p. 18) they have been arranged in the order of their volatile-carbon total-carbon ratio. Referring to VC Column 2 of this table the minimum value of the ratio is 20.9 o and the maximum 33.4. The inert volatile calculated on the pure coal basis varies from 12.5 to 16.3. The classification of the several coal beds or seams of the state as used in the state coal reports has often been questioned; nevertheless it is of interest to note that in so far as the present tests can be taken as an index, seam No. 7 falls in Class B, and seam No. 6 falls in Class D. Furthermore if, as has been pointed out, (paragraph 2, section b, Chapter II) certain of the Blue Band Composition and Character of Illinois Coals, by S. W. Parr, Illinois State Geological Sur- vey, Bulletin No. 3. 12 ILLINOIS ENGINEERING EXPERIMENT STATION f O CO O Oi O Ci C^ -OCO . CO 1C CO CO * & . -r-< CD Oi -t-Oi . . I- ?o - co ** . cot-coio^ I-GOQ sana jo punod jad-n ^ 'g Proximate Analysis of Pure Coal (Ash and Moisture Free), Per cent jnijd^ns UOQJ'BQ PSXT^ J831T?J^ ["BOQ Ajp-JTV jo punod aad -h "j -g Proximate Analysis of Air- Dry Coal, Per cent qsy - 9mT3^Oj\ 8Jn5SIOJ\[ -JTV ui aanisiOH ui SSOT; 0) "S O a s3 c bj) 'w O Q a ui'Bas jo pgg \V.OQ ON 'S '0 'S 'n o N , MJ0 .,oc l ^ cocorooi-<MTf<o SS^^ro' QO aocceo -MO ^ os -coco .ae-sco-^<N -i^oo co .^^iO 'O(M - -iCO -ino cO<l~'--!> -Ol^C- ooeO"tij^!- it^os osoo-rHTt<^-*--. t^ccwaoosooOi-io> i c " N 1-1 (M 66: 66 - 66: 66 (M . 66: 111 Illl 111 II l I " CCW " a- - * c* * CQ KQ FUEL TESTS WITH ILLINOIS COAL 13 g :23 = g :$o ;S3 ;S2 :S38 :gp :|8 :? :S :S :g2 :? :j? :g : :SS * ' ' : ' ' o t 66:66:60:66:06:66: 6:66 iz;^; : ^^; . : !z;^ :^;^ : ^^ : ^;J?; :66::66::66:66:66:6 wS'&w cficn s x'. - ccc/3 ^0:7: --yix --/ice csxx rsr.x * zx-s.'Ji'S. 2 * r s. * 5 ^a! aQOQ ^c Smao aiajcWCW ca>^aja;^oo^c>(i)^<ui)^ua)^^aj<ija)a)^^ocJ/ic/3ajajy3y3<uc/3a)a>c/2a)>c * 14 ILLINOIS ENGINEERING EXPERIMENT STATION jo punod aad I n !} - g 05 W.S'J jntidjng !-*= <lg UOqjfBQ p9XI l J Proximate of Pure Cc and Moistu Perc S? A jo punod jad -h ; -g (Hi qsy Si M *-= si II noqa^o paxi.g <*a 8{15'B'[OA 26 || 2 8jn^sioj^ auao ja<i -Su -Jiy UT aanqsiojv ui SSOT; 0) Pi s JB o a o '5 a be CC s d-o .22 2s ll a 6 m'RSS JO P9Q fROO 'N S 'D 'S 'H wxuwom coco <N IO3O .-* in m T-, T-+ ~ ~-aor~iot~-<*i-<ticoaoeoiot^io<oa3Coaoasusc<5-'*iaoo OO -OiC^COCOt^Ci -OiO5 -COCO -CD -COC^OC S8 : :8 : ;S^S^ oo _ eo ; oor-m<ri r-i et i~ et rn 04 : aJJ G o.^ p."p.<i> <u ^'E'. s a a a s a && aag-aag-a aa cc acccn esco ir.i e8. 3. . w. S SccoQS FUEL TESTS WITH ILLINOIS COAL 15 UOQJBO 81T1BIOA JO OtlBH ysis of Dry Coa cent) loo aanj) aiqpsnqtaoo qsy areas J Psa T^OQ oos ** -eo . .posqeo eo ffi *i 'eowcoco . 30 l^. -OO -OS O 3O OOGO30 Oi OS 00 < .** . .M . .* -o -in -2?-t~- .oeoi^-o .-xi -ta -so -co - -o~ r^ os in I : O1CO -CO ; .CO - ; : ^ -cQ | \ ' '-oS ' -o ' -6 : : : D '6 : CQ Q3Q 16 ILLINOIS ENGINEERING EXPERIMENT STATION uoqji3Q iieaOiL oa uoqa'BO 9U11310A jo omn coot- . .iftwt-t- . .t- . .CD -m -os . .00 -oo """ '* - ... - - ... (sxsT?a 11300 ajnj) 3 3 i 1-1 (N ; M CO <N <N -CO -<N -CO ; ;(N _ ;W ; ;CO^n (sis^g IBOO QJtidD os m 1-1 - - 1- 1- o os - -o .m . .0 <w IN . t- 1-1 W W (M M IN W (N (M CC -CO <M -CO <N M Ultimate Analysis of Dry Coal (Per cent) qsy CQ ^Hffioo -Tti^He^i^i i-i -co *c -o -o -oci S -^H O < .OiOO^nCO . -OS . .5> -O in !> . -H N ^t-OO -I^t-J-t- -CD -5> -CO . -Ji -COO w.r4 -coc^iriiN TH --^ -Tti i-I -TT ' i-i ~ 2 t-t-QC -QOOSOOOO '00 '00 'OS 'OO -OS ' -Oil- ~ co., . :S8ga ::S : - : - : :S : - ; .gg i-l i-l i-l -i-l.^-^H i-l -^ -H r-< _ r-, r- " t- INOO 06 o o - < - t- -co -co ' m ' -cc-^ to co t- * - . m * ' .m . t- . . -co - . o <M o os CD oo m !> m CD -co CD -co co * co "E "o a o I I H! mi M hlM Miin : : : : ; ; ; : : : '. 6 6 ' ' <]ffld : <ifflfflpq '.".'. ' & v<n a> a> <D I cpaiaiiii '.'. 2* ' ' ' aJ '3, I Q.<t't> ftftn' oftftft 'ft' ft - ft -ft' ftpflao, ||| : Hi! j| : :S : | || ; ||||| 600 : 6606 '6 i -8 : o -8 : 6iioo urB9s ao pgg \V,OQ CO CM ON 'S 'O 'S Tl <Jmo <HCQ = CQ ;pq , N ..0 WOW oo-.^^,ncD-oooso. N co^,co^oooso. N co^mcD FUEL TESTS WITH ILLINOIS COAL 17 os . r- cc -*" e<i cs oo o . ~- oo i ec c :88 : :2 -O -O?O -I- <&5 -oco TO * .1-1 . o -<M -ow -t 10 -t-- 'ftoo 6 -66 -66 -66 -66 -do -66 -6c> '.66 -66 ' ' '66 166 '.66 '.66 ^O! r3 sXX cJ X 'V. -CT. O 18 ILLINOIS ENGINEERING EXPERIMENT STATION coals of Sangamon County in reality belong to Seam 6 instead of 5, Class B would also include all coals tested from seam No. 5. The single sample from Seam No. 2, (U. S. G. S. 18) falls in Class D, well up towards the lignites. TABLE IV CLASSIFICATION OF ILLINOIS COAL ON THE BASIS OF THE VOLATILE-CARBON AND TOTAL-CARBON RATIO U. S. G. S. Number Ratio of Volatile Carbon to Total Carbon Inert Volatile (Pure Coal Basis) Class Coal Bed or Seam 1 2 3 4 5 28 20.90 12.50 B 6 22.20 13.35 B 5 3 22.50 12.20 B 16 22.90 12.50 B 7 19 23.00 12.30 B 7 12 23.63 12.20 B 7 21 23.70 16.30 B 6 13 24.70 13.00 B 11 24.77 12,00 B 7 34 25.40 12.90 B 5 10 26.20 13.30 B 7 24 26.90 12.50 D 6 20 26.90 13.60 D 6 29 27.13 13.50 D 5 31 27.60 13.10 D 6 4 28.30 12.36 D 6 9 29.00 13.00 D 6 22 29,20 12-70 D 6 23 29.30 13.30 D 6 25 29.20 13.40 D 6 15 29 50 13.20 D 6 26 29 80 12.50 D 5 27 29.80 13.50 D 6 8 30.30 12.70 D 6 14 30.60 12-40 D 5 30 31.00 14.00 D 6 33 31.00 12.80 D 7 18 31.80 12.70 D 2 7 32.80 12.95 D 6 1 & 2 33.40 12.95 D 6 V WASHING TESTS 8. The equipment for the washing tests of Illinois coal consists of one modified Stewart jig and one jig especially designed for the laboratory, a Cornish tooth-roll crusher, an adjustable-mesh bumping screen, and bins of suitable capacity for storing the coal. The Stewart jig, shown in Fig. 2, provides for the washing of coal not exceeding 1J inches in diameter. The special jig may be used for larger sizes. It is of the center- plunger type, that is, the plunger is directly beneath the screen. Its upward stroke causes the pulsation, and its downward stroke, by an arrange- ment of valves at the side of the jig body, admits the water sup- FUEL TESTS WITH ILLINOIS COAL 19 ply. The screen is 4 feet wide by 5 feet long and is constructed of No. 10 wire set 1-16 inch apart. The length of stroke and the depth of the coal bed are adjustable. FIG. 2 STEWART JIG (PROF. PAPER 48, p. 1460) 9. The tests involved the weighing of the raw and washed coal, and the refuse. Samples of the coal were collected before and after it was fed to the jig. These were sent to the chemical lab- oratory for analysis. Altogether 31 tests were made on 24 kinds of coal. 10. The results of the tests are given in Table 5. Column 1 of this table is the U. S. G. S. coal number, Column 2 the jig used 20 ILLINOIS ENGINEERING EXPERIMENT STATION spanod 11300 PJUSU i re spunod w 'S . ^r9 ^[91T5J'Bd9S) anqd[ns ^T3g g2 S^ Ju| qsy X'' (p9UltU.I919C[ A'[9JKJT?d9S) jnqd[ns S-H O .2 a 02 a; qsy >> o o| < . < ^ a P S I 3 R S?A CH <W 1-H C* 1 ' 1 I T I <M ^1 (71 ^ li ^- G^ CM <7J T (T-^T-H^-T I (M CO CM T I I OQUiirtOOQO r i -.-TI- -oi-r 1 ': : : I o Ut lO -- CD CC ?O iO OO 1C ^O ^ J -* rf Ci ifs <M t- t- oc x ;e C5CiCS>fl=;CC CC rt 1- ON 's ' ~s -a ^i ^ t^ eo c <*-,-<* ; ; ;-- Sl!mi!l: IldSv 11! SrJ ~^ : : :3? sssssssssss gg^S? ?55 ^i2 S2g -s w -o^^j,'^:^;^;"^^^ o ;; '- 1C * 7' ~ g$ |w : 1^6 o eo oi oo ao i os od ffi * " re :c in :2^ !^ 1C ^-' 05 Slack Run of Mine No. 5 Nut Run of Mine crushed to 2 in. Slack Run of Mine crushed to 2 in. Slack Run of Mine crushed to 2 in. Egg crushed to 2 in . Lump crushed to 2 in. Lump & Egg ( crus:rud to 2 in. Lump crushed to 2 in Screenings crushed to 2 in. Lump crushed to 2 in. Nut & Slack crushed to 2 in. Lump crushed to 2 in. Screenings crushed to 2 in. Nut crushed to 2 in. Run of Mine crushed to 2 in. Lump crushed to 2 in. Screenings crushed to 2 in. Nut crushed to 2% in. Nut crushe i to 1 in. Screenings crushed to 1 in. vart modified "sS as | % ..B 3< ^ c - ^ 12 ~ !2 Z . & ^ i* iri ci w 75 5Sw w <M ?; %%%% FUEL TESTS WITH ILLINOIS COAL 21 and Column 3 the size of the coal. The proximate analysis of the raw and washed coal is given in Columns 4 to 11. The weight of raw coal tested is given in Column 12 and the washed coal pro- duced in Column 13. Column 14 gives the refuse expressed in per cent of raw coal fed to the jig. 11. The improvement in quality of the coal effected by wash- ing is well shown in Columns 4 to 11. For example the percent of ash content is, in every case, decreased by washing. This is shown graphically in Fig. 3. In this figure the per cent of ash in the washed coal is plotted against per cent of ash in the raw coal. The average line shows that by resorting to the process of washing, it is possible to reduce the ash content from 22 per cent to 8.7 per cent and from 10 per cent to 6.9 per cent. Ex- pressed in per cent the amount of reduction is as follows: When raw coal contains 8% ash, the reduction is 20%. When raw coal contains 12$ ash, the reduction is 30%. When raw coal contains 16 % ash, the reduction is 43%. When raw coal contains 20 % ash, the reduction is 53%. 210 a 5- in c < 6 < 43 z: O 4 6 8 10 12 14 16 18 20 Per Cent of Ash in Raw Coal FIG. 3 REDUCTION OF ASH DUE TO WASHING 22 22 ILLINOIS ENGINEERING EXPERIMENT STATION In a similar way the reduction in sulphur due to washing is shown in Fig. 4. Referring to this figure it will be seen that: When raw coal contains 2% sulphur, the reduction is 13%. When raw coal contains 3% sulphur, the reduction is 17%. When raw coal contains 4% sulphur, the reduction is 22%. When raw coal contains 5% sulphur, the reduction is 28%. 73 4 o 12345 Per Cent of Sulphur in Raw Coal FIG. 4 REDUCTION OF SULPHUR DUE TO WASHING In bringing about this improvement in the quality of coal by washing, much good coal which can not be recovered is carried off with the refuse from the jig. For example, the tests show that, based on the average of all tests, the refuse amounts to 16.8 per cent of the raw coal. The ash in the raw coal is 12.6 per cent, but in the washed coal this is reduced to 8.34 per cent, therefore 12.6- 88.2X8.34 or 5.7 per cent is the ash content in the refuse. It appears, then, that the material thus discharged is made up of about | pure coal and i ash. FUEL TESTS WITH ILLINOIS COAL 23 VI COKING TESTS 12. The ovens in which tests of the coking qualities of the coal were made are of the regular beehive pattern. Originally they were arranged in a battery of three, two of standard size, 12 feet in diameter, by 7 feet high, and the third 12 feet in diam- eter by 6 feet 4 inches high; later, however, one of the standard ovens was removed. Since the two remaining ovens may be con- sidered as end ovens, that is, those placed at the ends of the bat- tery, the results obtained are directly comparable. 13. The tests. To prepare the coal for test it was finely crushed in a Williams mill. It was then placed on the larry and delivered to the oven. The larry used when the work was begun had a capacity less than one ton. This necessitated the filling and emptying of the larry six or eight times before the charge was complete. Each portion thus had time to emit a large amount of gas and often to burst into flames before the next portion of the charge was added. This resulted in much injurious cross lami- nation of the coke in many of the earlier tests. Afterwards when a larger larry was installed and the time of charging reduced from one hour to less than seven minutes the laminations and cross-breakage disappeared. Directly after drawing the charge the ovens were closed for a period of one or two hours during which time they were allowed to gather heat for the next charge. A sample of coal was taken at regular intervals as-the charge was emptied into the larry. The total weight collected was 40 or 50 pounds. A sample of coke was taken from 5 different parts of the oven, one piece 2 feet from the oven floor, one 2 feet from each side on a line drawn from the center of the oven, one from the center of the oven, and one 2 feet from the back wall: The separate pieces of coke extended the whole height of the charge and were as nearly uniform in size as possible. 14. The results of the tests are given in Table 6. Column 1 of this table is the test number, Column 2 the U. S. G. S. number, and Column 3 the size as shipped to the laboratory. The proxi- mate analysis of the coal and coke produced from it is given in Columns 4 to 13. Column 14 gives the weight of coal in the charge. The coke produced in per cent of the weight of the coal charged is given in Column 15, and the per cent of breeze in Col- umn 16. The total yield as given in Column 17 is the sum of the coke aod breeze produced. A brief description of the physical 24 ILLINOIS ENGINEERING EXPERIMENT STATION .in -co in ^f Tf t- r- c<i . ^H co - . I-H in O3 r- T+H r- (M o o oc r- 02 oc . t- T-I . . Cft IN ^ t- <M .0 !> -CO 5 00 00 -OS CO OO -3< Ol in - ^ Ajad'ea'Bdas anqdins of Coke qsy , Analysis - & 1 -- Aiai'e.i'Bdas jmiding s of Coal qsy e Analysi Proximal SS^A 1 "o oj 'S*o's - n , N , SS , -cow -^ -co * m co o co co > Tt<O5 . D - '-I'-I --^i - i- w -e .t~CO - - -ioo . ' o o : ' TJ< cc o ~ n -i * M * m >n . i-^OTjiTt<Ni-Tj<ineoint''ff - x>cc^cO' ccoooscc ^ i- <N m -* 1-1 x i^- oo tt> M i FUEL TESTS WITH ILLINOIS COAL 25 .fitctfi 26 ILLINOIS ENGINEERING EXPERIMENT STATION properties of the coke produced is given in Column 18. In reviewing the results of the tests as set forth in Table 6, it should be remembered that the necessary routine work involved in the testing of so many coals made it possible to make but few tests on each coal. The data presented, therefore, show the results obtained under conditions which of necessity had to be controlled by observations made from time to time as the coking proceeded, a procedure which tended to make the conditions of operations by no means ideal. Of the 37 tests made with Illinois coal 9 resulted in the pro- duction of comparatively good coke and 14 in the production of a poor grade of coke. The remaining 14 samples apparently proved to be non-coking coals. Referring to the approximate analyses of the coke produced it will be seen that in a number of cases the quality of the coke is by no means inferior, though in all cases the ash and sulphur content is slightly greater than is desirable. Seven samples (11D washed, 13, 13 washed, 16, 22B washed, and 29 washed) were successfully used in a foundry cupola. VII STEAMING TESTS 15. The apparatus comprising the plant for steam-ing tests con- sisted of two standard Heine water- tube boilers equipped with hand-fired furnaces and an Allis-Chalmers Corliss engine oper- ating a 200 kilowatt Bullock generator. A plan and elevation of one of the boilers and its setting are shown in Fig. 5 and the general appearance as set up in the laboratory in Fig. 6. The equipment used for testing the boilers provided conveni- ent and accurate means for measuring the coal and water and for making all observations of pressure, temperature, etc., specified in the boiler testing code of the American Society of Mechanical Engineers. It consisted principally of water-weighing tanks, scales, charging cars, sampling cans, apparatus for analyzing flue gases, pressure gages, calorimeters, thermometers and draft gages*. *This apparatus is described in detail in"Professional Paper No. 48" United States Geolog- ical Survey. FUEL TESTS WITH ILLINOIS COAL 27 28 ILLINOIS ENGINEERING EXPERIMENT STATION i FUEL TESTS WITH ILLINOIS COAL 29 The principal dimensions of the boiler and furnace are as follows: Length of drum feet 21.58 Inside diameter of drum inches 42. Number of tubes, 11 tubes high by 11 tubes wide 116 Outside diameter of tubes inches 3.5 Width of furnace ' feet 6.16 Length of furnace feet 6.58 Mean height of furnace inches 26.00 Grate area square feet. . . 40.55 Ratio of grate area to air space 40. 17 Water-heating surface in tubes square feet . . .1897 Water-heating surface in water legs square feet ... 91 Water-heating surface in shell square feet. . . 43 Total water-heating surface square feet . . .2031 Ratio of heating surface to grate area 50. 1 16. The Tests. Since the establishment of the fuel testing division of the United States Geological Survey, more than 500 boiler trials have been made, and of these, 112 involved the use of Illinois coal. Tests were made with each of the 34 samples submitted, the coal being used either in its natural state or in the form of briquets, or both. A number of tests were also made with washed coal. A summary of the principal observed and derived results of tests with Illinois coals is given in Tables 7 and 8. In these tables only such values as have a direct relation to boiler performance are included; additional data, however, may be found in the reports published by the United States Geological Survey.* 17. The description of the coal tested given in Table 7, Column 1 , of this table is the serial number of the test and is useful as a means of identification. Tlie number describing the location from which the sample was taken, is given in Column 2 and the number of the coal bed or seam, in Column 3. The size of the coal is given * Bulletin No. 332 and Professional Paper No- 48. 30 ILLINOIS ENGINEERING EXPERIMENT STATION in Columns 4 to 9. The size as shipped (Column 9) was not always the same as that used in the tests since in some cases it was crushed or screened after it was received. The actual size as determined from samples taken during each test is given in pre- cise terms in Columns 5, 6, 7 and 8, and the average diameter calculated from these data is given in Column 9. The proximate analyses (Columns 10 to 14) were made from samples collected for each test and are given in the tables in terms of coal as fired. Calorific values were not determined for every test. The values given (Column 15) were calculated from the proximate analysis and the calorific value determined from the car sample, on the assumption that the B. t. u. per pound of pure coal (ash and mois- ture free) is the same for each car load shipped to the testing plant. 18. The performance of the boiler and furnace is given in Table 8. Column 17 gives the average boiler pressure in pounds per square inch. The standard pressure was 75 but it will be seen that the values given vary from 68 to 81. The draft above the fire (Column 18) was measured in inches of water. In some tests it was as great as .3 inch; the average however, is a little less than .2 inch. The furnace temperature (Column 19) was observed with a Wanner optical pyrometer. The results .given are averages of a number of readings which varied over a considerable range throughout the test. The lowest temperature recorded is 1887 and the highest 2829 F. The rate of combustion in terms of dry coal fired per hour, per square foot of grate surface (Column 20) is, for most tests, about 25 pounds. This rate, it will be seen, is sufficient to evap- orate, in most cases 5i pounds of water from and at 212 F. per square foot of heating surface per hour (Column 21) or 100 per cent of the rated horse -power (Column 22). The evaporative efficiency is given in Columns 23, 24 and 25. In Columns 23 and 24 the equivalent evaporation per pound of coal as fired and per pound of dry coal, respectively, is given. The values given in Column 25 represent the over-all efficiency, that is, the ratio of the heat absorbed by the water in the boiler to the potential heat in the coal fed to the furnace. It is evident, therefore, that this is the best measure of the value of any parti- cular fuel for steam generation since it expresses the exact pro- portion of heat purchased in the form of coal which can be con- verted into useful energy in the form of steam. Referring to the FUEL TESTS WITH ILLINOIS COAL purio<j~jad r n -a 31 sgqoni ' of C cen T % o-j qoni i 01 qoai i J9AQ ON -s '0 *s r* i ^ o . . .<M . O'-*csot-ffi- / 5 -< ICCCXl-t-^r O >oso " ! ITS iO 30 I II cc-^ Xt- . ?o acac ceo o ac so 35 030 <N ; : 2: : 2 ^^^S^si:^?,?? 'g :^x c3 bl & a 3 33 " <D 4D <D F t> t> l t t> 00 00 Ok <3 Oft Ok Ok Ok O O O O O 32 ILLINOIS ENGINEERING EXPERIMENT STATION rBooA-jci 4 i rh IBOO ui gXSSSMSSesSSSS^aSSSeSXSSgeSloCiSSSS alysis of ired it usv SSSPSSSSSSSSSSSsSSSSSSSSSSSSeKSSSiS noOT * M CM S3SS838?82&SSS!25S23Sgg38Sg;838|2g COOOOt-OOOOTOlCCDCOTht-^-OI-COOOO <NW<Ni-ii^OOCi Proximate Ar Coal as F per cer . S?A - SS8883Si8888S88&88885&$58%88S COWCOCOCOCOCOCOCOCO(WCOCO*JCOCOCOCOCOCOCOCOOOCOfWCOCOCOCOWW<NW 0) S>g>g2g23gS288c3Sc38c333S3c ODcot^dcodoJoJco^oJcoddcDoioioidi-ie-iiftd oi -hi-cowcowco sgqoui 'IBOQ jo -O-CDO ^sgggg ^psggggggsssggggasB Size of Coal per cent qoat ^ J9pufi oo O 9* 1-1 CO O CO CO CD Ifii TH CO O . -* CO CO O <M r- Ci 1ft Tt< CD CO * CO CO J^ <M CD ^ 3381S3SS5 .Balsas .5s*ss8;i3,HS3i*83$5;i8 qoui %oi % to CO <N (M CO Tfi CO CO 1-1 CO CD O5 1-1 CO O CO O 1-1 CD t- O I-" OO CO OS CD O5 CO O <N t- CO t-COOCDt-COlft !><N <0 S> T(H -100C500it-lO WLOWt-OOW^T^jH qoui I 01 % COOCOCCWift^ .^W^COCOOT .QOl>NI-<05t-t-t-W ^Z^Z :%Z^%% :^^^^^^ U.OUT I J8AQ U3 OSCD-r-CO-^CO 00-*iCC-'*ilftCO .OCOO<MCO-<*"<MCiO^CO>O t- S^S^SS : 8S8^ isliSeJSiciScSSlS^^ffi ' : Size of Coal as Shipped * : : : : : : : : : : : ':':':': ': : i :::::::::::: i : 1 : : ::::::: : : : : : : : : :::::;::::::: : 1 : : j i i i i j -a : : a) : ! : -S i : : ': : i . 58 . aj : : . ; i : *: : : : - - : i i'S : : : : S : : g -^ :^ : : .2 d s3 fl . ; i 2 * "* " S ' 'ii '^ r.s 'a : j ' ' -g > i^l ' "o, . &- - SSp. - - o. 0- ^^ P. - . a&opi&fi. .- - - g: : g - - 00^- - - i- |S= o- S- - - SSSSSSC s s ^'C s s 'C^j ^ s ^ s y 3 3 3"" P5 j ^pqas Di P3^ ^ J j^jjjj^ ureas JO pgg I'BOO CO CM ON -s -o -s *n CQ CO CO 3D CQ CO O O CO ^<5j<J< 'ON 5S9J, *c r- 8 J5SsS)SgS g 5S 5 ; 5 ag 5^ 8SS s5 : $s8S8R ^^^^^^^CO-H^- ^ FUEL, TESTS WITH ILLINOIS COAL SSS2?3?* = 2Si2j = S88 -"2S*S.H.i-228 w S""' < *8 -- : ->2 . : a i. 2 a i ...ii. - S- - S- c- 5 5 S i! gc- - C333 -r- - ~ ~. ~ ~. ~. 34 ILLINOIS ENGINEERING EXPERIMENT STATION TABLE 8 STEAMING TESTS PERFORMANCE OF BOILER AND FURNACE u S Equivalent Q .r- Q2 C3 S Pounds of t- <U cB <D ?- a 88 Q g'5 'O P <D O Water Evap- [s 3.g 3 in PH en C&n"c/2 g || orated from and at 212 F. pqO ^ )>3 CM > fl o fe It Is 1| IP f} 3'! - 2 Per Pound in 0) G III 09 H 2s 3& ^n 7^ S o^g u a v |*KS i| ^-d c2 &fi f-i fl G 0) .SS^H O^_, - &! I 5 03 O 6-9 f- 1 i s a r !2|*S 3|* * kg 85 fe P 3 o W f ii **s w 3 K 1 16 17 18 19 20 21 22 23 24 25 18 .18 1887 24.90 3.59 100.7 6.51 7.21 58.73 4.85 19 .15 22.36 3.57 100.1 7.16 8.00 61.47 4.38 38 .21 21.23 3.41 95.5 7.35 ! 8.04 60.39 4.34 48 .16 19.84 2.92 81.9 6.38 7.34 57.27 4.73 50 .21 23.13 3.36 94.2 6.36 7.27 56.36 4.80 73 .... .23 22.34 3.30 92.5 6.43 7.40 61.64 4.72 106 75 .25 22i3 25.94 3.39 95.3 5.56 6.56 49.64 5^32 313 72 .17 17.24 2.81 78.7 7.03 8.16 65.51 314 68 .07 2359 21.81 3.42 95.9 5.99 6.91 55.14 122 72 .30 20-08 2.19 61.4 5.44 6.08 58.71 5.74 129 73 .24 19.92 3.19 89.6 6.70 8-02 60.84 4.36 142 81 .16 20.07 2.97 83.3 6.65 7.44 61.39 4.70 143 79 .18 18.74 2.69 75.5 6.46 7.20 62.01 4.85 146 67 .22 20.21 2.68 75.2 6.64 7.40 64.45 4.72 516 79 .13 31.99 3.70 103.7 4.95 5.79 54.38 6.03 101 83.5 .32 28.82 3.21 90-1 5.39 6.22 49.86 5.61 102 78 .25 38.36 3.62 101.5 5.58 6.39 51.41 5.46 103 81 .27 22J8 26.53 3.61 101.1 5.94 6.81 52.59 5.13 104 80 . 19 2155 23.22 3.01 84.4 5.70 6.50 50. 2S 5.37 105 78 .25 2220 30.26 4.08 114.3 5.93 6.75 51.92 5.17 113 75 .20 25.60 3.05 85.6 5.68 6.66 49.67 5.24 121 75 .19 26.60 3.57 100.0 6.69 7.49 58.15 4.66 492 76.5 .16 3.50 98.2 6^65 7.79 62.50 4.48 107 76 .32 2229 2li()0 3.20 89.9 6.76 7.65 59.44 4.56 108 76 .21 22.24 3.13 87.6 6.39 7.04 53.60 4.96 109 78 .29 21.46 2.96 83.0 6.90 7.70 60.10 4.53 110 75 .26 20.66 ! 2.48 69.6 6.08 6.71 50.12 5.20 114 75 .21 24.23 3.52 98.7 7.16 8.11 57.82 4.30 137 74 .16 20.98 3.17 88.8 7.76 8.42 64.51 4.14 138 74 .18 2376 19.94 2.97 83.4 7.68 8.32 66.08 4.20 139 77 .18 2435 19.70 3.06 85.9 8.02 8.67 68.33 4.03 141 79 .15 18.81 3.11 87.3 7.66 8 29 64.02 4 21 111 73.5 ! .28 24.35 2.93 82.0 6.15 6.70 51.18 5.21 112 80 .27 22.36 2.90 81.2 6.59 7.23 54.65 4.83 115 76 .26 22.89 3.42 95.9 6.83 7.49 58.71 4.66 116 76 .22 24.19 3.61 101-3 6.94 7.48 55.85 4.67 117 75.5 .20 23.80 3.42 95.8 6.71 7.19 55.38 4.85 118 77 .16 23.16 3.32 93.1 6.74 7.19 54.26 4 85 119 75 . 25 25.70 3.75 105.0 .84 7.31 53.97 4.78 120 72 .23 25-41 3.55 99.5 .08 7.79 56.27 4.48 312 71 .11 2400 19-38 3.40 95.4 .96 8.80 63.60 127 73 .19 21.49 3 35 94.0 .15 7.81 63.04 4.50 128 75 -19 21.45 3.51 98.3 .54 8.19 65.07 4.26 131 74 .19 20-87 2.91 81.50 .04 7.74 64.08 4.49 133 81 .22 22-91 3.15 88-2 ,00 7.67 62.51 4.55 135 74 ,18 23.09 3.62 101.3 .86 8.75 64.48 3.99 136 75 .21 20.77 2.91 81.5 7.00 7.81 63.56 4.47 463 81 .11 2490 18-67 3.20 89.7 7.98 8.58 64.44 4.07 132 76 .13 22.06 3.37 94.5 7.67 8.52 65.67 4.10 134 78 .18 22.55 3.39 95.0 7.58 8.39 63.96 4.16 144 79 .10 20.42 3.70 103.8 8.20 9 . 08 66.12 3.84 145 75 .13 20.14 3.38 94.7 8.37 9.36 67.93 3.73 123 73 .28 23.60 3.10 87.0 6.49 7.34 59.03 4.76 125 74 .20 20.30 3.08 86.2 6.62 7.58 60.37 4.61 130 77 .14 21.63 3.33 93.3 6.49 7.71 58.48 4.53 126 69 .18 20.44 3.11 87.2 6.86 7.62 62.62 4,58 FUEL TESTS WITH ILLINOIS COAL 35 TABLE 8 STEALING TESTS PERFORMANCE OF BOILER AND FURNACE (Continued) 8 s ^ Equivalent Test No. Boiler Pressure Ib. per sq. in. Draft above Fire inches of Water mperature of Furna< Degrees F. )ry Coal per sq. ft. ol Grate Surf ace per hour, pounds niviilrnt. Kv;i]iui'nt.i( Dm and at 2!2F. pei ft. of Heating Surfa Per Hour, pounds Per Cent of Rated orsepower Develope Pounds of Water Evap- orated from and at 21 2 F Per Pound Efficiency of Boiler ncluding the Grate Per Cent s|J 1 3? 5f-> | & i i &i w o s M 3 1 16 17 18 19 20 21 22 23 24 25 152 75 .13 2439 19.63 3.36 94.3 7.57 8.59 63-30 4.06 150 74 .11 .... 19.63 3.56 99.8 8.24 9.08 68.11 3.85 140 75 .18 18.51 2.86 80.1 -.60 8.61 64.20 4.06 147 72 .17 19.53 3.12 87.4 -.57 8.91 63.48 3.92 148 73 .19 18.86 2.99 83.9 -.06 7.94 59.02 4.40 149 74 .14 2060 17.83 3.29 92.2 -.70 9.23 66.36 160 77 .14 2428 18.47 3.07 86.1 -.27 8.33 61.71 4.'i9 161 77 .20 2080 17.77 3.12 87.6 -.62 8.80 65.82 3.97 163 78 .17 2227 20.79 3.57 100.2 7.50 8.61 63.63 4.06 170 79 .16 2039 20.22 3.10 87.0 -.42 8.56 64.29 4.08 171 77 .17 20.08 3.23 90.6 -.79 8.97 67.06 I 3.89 175 74 .09 2470 20.54 3.73 104.7 8.13 9.10 67.50 : 3.84 204 72.5 .11 2447 20.69 3.50 98.2 8.54 9.45 69.93 3.70 205 .12 2448 20.38 3.38 94.9 8.32 9.27 68.86 3.77 420 79.5 .12 .... 19.95 3.35 93.9 7.67 8.40 65.26 ! 4.16 423 78.5 .14 .... 16.94 2.89 81.0 7.73 8.53 65.92 I 4.09 424 83.5 .12 18.67 3.18 89.1 7.81 8.53 66.35 4.09 425 81 .14 19.33 3.32 93.0 7.87 8.61 66.73 4.05 421 82 .11 19.46 3.30 92.5 7.70 8.48 65.76 4.12 422 78.5 .12 19,46 3.39 95.0 7.88 8.73 67.03 4.00 292 70.5 .10 2020 15-49 2.37 66.3 6.55 7.66 64.75 4.56 301 69 .30 24.61 3.54 99.3 6.71 8.04 62 08 4.34 302 76 .17 2708 25.69 3.81 106.7 6.91 8.27 63.65 4.22 315 74.5 .16 2499 20.05 3.27 91.6 6.94 8.16 65.97 4.28 316 69 .15 2401 20.05 3.19 89.3 6.76 7.96 62.80 4.39 318 69.5 .04 2508 25.30 4.11 115.3 6.73 8.14 63.04 4.29 324 71.5 .20 2850 23.08 3.60 100.9 6.91 7.81 65.67 4.47 325 72 .18 2828 22.61 3.60 101.0 7.14 7.97 64.81 4.38 328 71 .14 2829 26.73 4.34 121.8 6.97 8.14 60.82 4.29 306 67 .13 2402 18.50 3.01 84.3 6.97 8.15 66.93 4.29 317 70.5 .13 2397 19.63 3.23 90.4 7.02 8.23 62.12 4.24 321 70.0 .27 23.75 3.78 106.0 6.89 | 7.97 59.22 4.38 322 74.5 .16 24.54 3.80 106.6 6.71 7.76 57.66 4.50 335 74.5 .22 2708 20.49 3.30 92.6 7.09 8.07 63.68 4.33 336 73.5 .26 21.48 3.29 92.3 6.71 7.67 58-68 4.55 337 72 .20 23.63 3.82 107.0 7.00 8.10 62.71 4.31 338 71.5 .21 21.36 3.10 87.0 6.38 | 7.28 56.16 4.80 339 73 .21 23.63 3.54 99.1 6.63 j 7.50 60.25 4.66 341 76 .34 20.91 2.84 79.7 6.56 7.58 60.85 4 61 342 77 .30 2264 23.02 3.16 88.6 6.47 7.67 60.42 4.55 353 78 .18 2360 19.83 3.14 88.0 6.66 7.93 64.73 4.40 354 76 .17 2162 19-26 3.08 86.4 6.75 8.02 66.12 4.36 459 80 .15 2601 18.72 3.13 87.7 7.75 8.36 64.29 4.18 457 81 .16 2606 19.85 3-42 95.9 8.13 8.64 64.99 4.04 448 79 .17 2862 22.52 3.88 108.8 8.21 8.63 64.50 4.05 452 82.5 .14 2833 21.97 3.94 110-5 8.35 8-98 66.35 3.89 465 75.5 -15 2665 20.35 3.62 101.5 7.65 8.91 65.58 3.92 460 81.5 .18 2759 21.38 3.44 96.3 7.16 8.05 65.08 4.34 461 80.5 .18 2816 22.32 3.72 104.2 7.31 8.34 63.28 4.19 466 79.5 .16 2784 22.32 3.90 109.2 7.87 8.74 66.14 3.99 511 79.5 .19 .... 20.94 3.59 100.7 7.76 8.60 62.58 4.06 489 74 .14 21.16 3.49 97.7 7.06 ! 8.25 64.76 4.23 491 82 .20 21.65 3.56 100.0 7.35 i 8-24 64.51 4.24 513 82 .10 2465 26.41 3.23 90.7 5.43 6.13 53.34 5.69 509 82 .22 21.50 3.79 106.2 8.24 8.82 62.53 36 ILLINOIS ENGINEERING EXPERIMENT STATION values given, it will be seen that but few fall below 55 per cent or above 65 per cent, the maximum and minimum efficiency recorded being 68.11 and 49.64 respectively. In reviewing the results set forth in Tables 7 and 8 it should be remembered that they apply only to the performance of a hand-fired water-tube boiler of the Heine type and that any con- clusions which may be drawn are thus limited. Had it been pos- sible to provide a furnace especially adapted to the burning of each particular coal, the relative efficiency as established by the tests might have been slightly different. The results obtained, however, may be accepted as fairly indicative of the value of the coals tested. With this in view, then, it will be of more than ordi- nary interest to study the effect of the physical and chemical prop- erties of the fuel upon the performance of the boiler and furnace as set forth in the tables. 19. Furnace temperature. It will be seen that while the results do not show any exact relation between efficiency, furnace temperature and rate of combustion, nevertheless they clearly indicate that as the rate of combustion increases, the temperature increases, but that efficiency is only slightly affected by change in combustion-chamber temperature. A comparison with values representing capacity (Column 22) shows that as the combustion chamber temperature increases the capacity is increased. 20. The evaporative efficiency as affected by moisture in the coal is not well defined by the results of the tests. While they seem to indicate that coals high in moisture generally give low effi- ciency it must be remembered that high moisture is often accom- panied by high ash content or by poor mechanical structure, either of which properties has a more deleterious effect on effi- ciency than moisture. That this is true is emphasized by the fact that the heat required to evaporate the water in Illinois coal con- taining 15 per cent moisture is but little more than 1.5 per cent of its total calorific value. 21. The effect of sulphur and ash upon evaporative efficiency. Sulphur is an undesirable element in coal. It generally occurs in combination with iron, as pyrites, and in combination with cal- cium as gypsum. Of the two sulphur compounds, the former is generally contained in larger quantity in coal and is harmful be- cause it increases the tendency of the coal to clinker. The clinker- ing is especially bad if the percentage of ash is small in proportion to the sulphur. In such coals the pyrites and the ash fuse and form- a thin layer of solid clinker, which effectively stops the FUEL TESTS WITH ILLINOIS COAL 37 passage of air through the grate, thus permitting the grate bars to become heated from the hot fuel bed just above. The heat warps the grate bars and the clinker has such corrosive action on the hot iron that destruction results in a short time. When such clinkering occurs, any attempt to slice the fire fails and only slow and very difficult cleaning of the fires will remove it. Most Illi- nois coals having a large sulphur content are also high in ash so that the injurious effect of sulphur is not so pronounced as in some other coals. In making the tests it was found that the use of steam served to prevent the clinker from melting into the grate when the ash and sulphur content is large . Referring to Columns 13, 14, and 25 of Tables 7 and 8 the decrease in efficiency with increasing ash and sulphur will be read- ily seen. In Fig. 7, which shows this relation graphically, efficiency is plotted against per cent of ash plus sulphur based on dry coal, for all tests run with lump, egg and nut coal. Although many of the plotted points lie at a considerable distance from the average line, its position and direction are rather well defined. It shows that the efficiency drops from 66.5 per cent when the ash plus sulphur is 10 percent to 55 per cent when ash plus sulphur is 30 per cent. For increases in ash and sulphur beyond 18 percent the drop in efficiency is relatively rapid. 22. The effect of size on evaporative efficiency. The discussion in the preceding paragraph does not take into account the fact that size has much to do with the efficiency with which coal can be burned, and this is one of the chief reasons for the poor alignment of many of the points. The efficiency shown by the same tests together with those made with slack have therefore been plotted against size, expressed in percent of coal under i inch in diameter. The resulting relation is shown in Fig 8. Here, too, the points are widely scattered but the slope of the average line is fairly well fixed. Thus a coal giving an efficiency of 66 percent when 10 percent of it is under i-inch in diameter, will give an efficiency of only 62 per cent when 60 per cent of it is under i-inch in diam- eter. 38 ILLINOIS ENGINEERING EXPERIMENT STATION 6 8 10 12 14 16 18 20 22 24 26 28 30 32 Ash -f Sulphur, Per Cent of Dry Coal FIG. 7 EVAPORATIVE EFFICIENCY AS AFFECTED BY ASH AND SULPHUR 10 FIG. 8 50 60 20 30 40 Size of Coal, Per Cent Under i Inch * EVAPORATIVE EFFICIENCY AS AFFECTED BY SIZE OF COAL FUEL TESTS WITH ILLINOIS COAL 39 90 80 B H 70 o 1 60 g 50 I" iS 30 20 10 10 20 30 40 50 60 Size of Coal, Per Cent Under J Inch FIG. 9 COMBINED EFFECT OF SULPHUR PLUS ASH AND SIZE ON EVAPORATIVE EFFICIENCY Fig. 9 has been drawn to show the combined effect of sul- phur plus ash and size, on the evaporative efficiency of Illinois coal. In it lines have been drawn showing the decrease in effi- ciency with decrease in size for coals having 10, 20 and 30 per cent ash plus sulphur based on dry coal. There are, of course, other factors which affect efficiency but the results of the present tests seem to point to these as the most important. The lines given therefore, may be accepted as defining with considerable accuracy, the performance of Illinois coal when burned in a hand- fired furnace under a water-tube boiler. 23. Comparative efficiency resulting from the use of washed and unwashed coal. It has been shown that the process of washing Illinois coal is effective in reducing the ash and sulphur content. That the evaporative efficiency of the coal thus treated is increased follows directly from the facts just developed. The extent of the 40 ILLINOIS ENGINEERING EXPERIMENT STATION improvement is set forth by Table 9. In this table tests are grouped in the order of the size of coal used. A comparison of the average values given shows that where slack is used washing effects an increase of 4.2 per cent in evaporative efficiency, 2.3 per cent where nut is used, .7 per cent when run-of-mine is used and .6 per cent when lump is used. The extremely small gain for TABLE 9 COMPARATIVE EFFICIENCY OF WASHED AND UNWASHED COAL U. S. G. S. Coal No. Size Efficiency Unwashed Washed 1 2 3 4 1 7C 10 Slack Slack Slack 58.73 58 71 50,12 61.47 60.84 57.82 60.04 Average 55.85 9A 12 R. o. m. R o. m. 50.28 62.51 49.67 61.48 57.08 Average 56.40 13 13 Nut Nut 65.67 63.96 67.93 66.12 Average 64.68 67.02 23 A 18 18 Lump Lump Lump 66.93 64.20 J.9.02 63.38 62.12 63 48 66.39 64.00 Average the last two sizes named is explained by the fact that, in the pro- cess of washing, the coal was crushed to a size under 2 inches, a size which has been shown not to be so well adapted to the kind of grate and furnace used as the larger size. 24. Comparison of efficiency resulting from the use of raw and briquetted coal. Of the 112 boiler tests made, 15 tests were run with briquetted coal. Comparing the results shown in Table 8 with the results of similar tests with raw coal, it will be seen that in most cases where the raw coal is in the form of screenings or FUEL TESTS WITH ILLINOIS COAL 41 slack, briquetting improves the evaporative efficiency, but where it is in the form of egg, nut or lump, but little difference in perform- ance results. As in the case of coal in its natural state, effi- ciency decreases as the ash and sulphur content increases. This is shown graphically in Fig. 10. The rather close alignment of the plotted points in this figure is due principally to the uniform- ity in size of the fuel. H 7 2 O 60 8 10 12 14 16 18 20 22 24 26 28 Ash + Sulphur, Per Cent of Dry Coal Fi(*. 10 EVAPORATIVE EFFICIENCY As AFFECTED BY ASH AND SULPHUR IN BRIQUET 42 ILLINOIS ENGINEERING EXPERIMENT STATION 25. The evaporative efficiency of Illinois coal compared with that of coal from other states, as shown by the United States Geolog- ical Survey tests, is presented in Table 10. Only tests with bitumin- ous and semi- bituminous coal are here included and the average values given are based only on tests which were made under simi- TABLE 10 COMPARATIVE RESULTS OBTAINED FROM COAL FROM VARIOUS STATES % a ,. || ll ! o i S " ^ ^ ^ T^ 3 ,3 *o > Ofe Q Is a en c3 43 <D ~o o O 3 ^ 'cd o> O p Q > ^ ^ Q, O State Kind of Coal ^ ^ * 0> H^Q "o^ K O CD c _, ^3 >>i P. ^ 6 6 Pt O ~ c s P-* ,JQ fa fc o>T "3 c3 O S^ ^ w > r) P. 'S'5 43 P p H M pq 1 2 3 4 5 6 7 8 Alabama Bituminous 10 4 91.9 8.43 64.31 12656 Arkansas . EJituminous 8- 89.3 9.03 63.54 13707 Colorado Bituminous 1 1 71.9 7.21 55.36 12577 Illinois . Bituminous 52 25 89.6 7.95 62.66 12249 Iowa Bituminous 5 5 90.7 7.13 59.55 11650 Indiana Bituminous 24 11 89.5 8.23 63.76 12549 Kansas Bituminous 8 6 83.4 8.10 61.26 12780 Kentucky Semi-Bituminous 8 3 91.0 9.77 65.41 14417 Kentucky Bituminous 3 3 88.9 8.37 62-82 12883 Missouri Bituminous 9 92.2 7.73 60.18 12246 New Mexico Bituminous 6 3 104.3 8.28 64.68 12507 Ohio Bituminous 18 9 92.2 8.82 64.88 13130 Pennsylvania Bituminous 18 9 89.9 9.75 66.22 14248 Tennessee Bituminous 24 9 102.3 8.81 64.18 13261 Virginia Semi-Bituminous 10 4 94.2 9.73 65.07 14436 West Virginia Bituminousand Semi- Bituminous 36 21 95.5 9.86 65.89 14451 FUEL TESTS WITH ILLINOIS COAL 43 lar conditions of operation. Column 1 gives the name of the state, Column 2 the kind of coal, Column 3 the number of tests included in the average, Column 4 the number of samples of coal, Column 5 the average rate of power developed, Column 6 the efficiency in terms of equivalent evaporation per pound of dry coal, Column 7 the efficiency in per cent and Column 8 the heating value of the coal in B. t. u., per pound of dry coal. The values given in the table show that the average evaporative efficiency of Illinois coal is 62.66 per cent. This compares favorably with the results from any other coal tested and in fact is nearly identical with the gen- eral average, 63.1. VIII PRODUCER-GAS TESTS 26. The prod ucer-gas plant used for the United States Geolog ical Survey tests of Illinois coal consists of two Taylor pressure producers arranged to discharge into a single scrubber, a Westinghouse three-cylinder vertical gas engine rated at 235 horse-power, and a six-pole, 175 kilowatt Westinghouse direct current generator. Auxiliary apparatus was provided for meas- uring accurately the coal and gas, the steam used by the producer, and all temperatures and pressures necessary for a complete determination of plant efficiency. The general arrangement of the plant is well shown in Pig. 11, and a section through the pro- ducer in Fig. 12, (pp. 45, 46). The principal dimensions of the producer plant are as follows: Producer Capacity, horse-power 250 Outside diameter feet 7.0 Inside diameter feet 6.5 Height feet 15 Area of fuel-bed square feet 38.5 Diameter of gas delivery pipe inches 22 Type of feed, Bildt automatic continuous feed. Economizer Diameter feet 3 Height feet .... 16 . 5 Number of 7 -inch tubtt... 6 44 ILLINOIS ENGINEERING EXPERIMENT STATION Scrubber Diameter .feet ... 8 Height feet. . . . 20 Material used in scrubber, gas-house coke. Tar extractor Speed, revolutions per minute , 1500 Purifier Length of sides feet 8 Height feet.... 3.25 Material used in purifier, oxidized iron filings and wood shavings. Gas holder Diameter feet 20 Height feet. ... 13 Capacity cubic feet. . . 4000 27. The tests were conducted alternately on the two pro- ducers, one being charged while the other was in operation. The schedule adopted involved two sixty-hour runs per week. The first eight or twelve hours of each test were used for bringing the fuel bed to a uniform condition. During this preliminary run- ning, observations were made as in the regular tests, but the record data include only the last 48 or 50 hours, when the run- ning conditions were maintained as uniform as possible. Special attention was directed to the accurate measurements of the coal actually used and charts and checking devices were introduced for this purpose. Owing to the lack of reliability in the operation of the gas engine, many of the tests made at the beginning of the series were only of a few hours' duration; later, however, no difficulty was experienced in starting the engine and continuing it in opera- tion for a period of 120 hours. During this time two different coals were tested. Altogether 30 tests were made involving the use of 23 different samples of Illinois coal. 28. Results of the tests. The more important observed and calculated results of the tests are given in Table 11. Column 1 of this table is the laboratory number of the test, Column 2 the U. S. G. S. number of the sample tested and Column 3 the size of the coal tested. The proximate analyses of the coal as fired are given in Columns 4 to 8 and the heating value in B. t. u. per pound of dry coal is given in Column 4. The brake horse-power given in Column 10 is the power delivered by the gas engine. Column 11 is the cubic feet of gas delivered by the producer per hour, in terms of standard gas, that is, gas at atmospheric pressure and 60 F. temperature. Column 12 is the calorific value of the gas expressed in B. t. u. per cubic foot of standard gas. Column 13 FUEL TESTS WITH ILLINOIS COAL 45 QQ 46 ILLINOIS ENGINEERING EXPERIMENT STATION FIG. 12 ELEVATION SHOWING GENERAL ARRANGEMENT OF PRODUCER-GAS PLANT (Prof. Paper 48, p. 983) FUEL TESTS WITH ILLINOIS COAL 47 -9S.IOH a^Jg *sd patnns -UOQ IOO -JQ IOQ ^JQ jo panod iad st?o at pgaiBiaoo -n * -g IBOQ AJQ jo panod igd s^o pj^puBig jo 399J ojqno jo :jooj oiqno aad -n ^ g anon J9d SBQ pa^pa^^s JO 589J oiqno jo panod J9d - n 5090 jgj ' Proximate Analysi of Coal as Fired, per cent qsy ox -S.--D - s -a os T* TJ. to oo tt cs < i- o ec -<N^- . ec r- * ^ oo m <o o o - eo ~* * -o oo mow to e> o t^ t--* oo^* 01 ao o -osor-^ooi-imosooo*Jme*-* ill i o o o o M oo aooo IN oo -?? ?i -M ?! OS 05 CD r- t^ 00 i-iOO" t-t-0(M eCOOO>0^0'-05C<5COiOICffC5 <ncn . Q M fl ^ 3 G T3; :::: gc3 . 3 T 1 & ? 48 ILLINOIS ENGINEERING EXPERIMENT STATION is the cubic feet of standard gas per pound of dry coal. Column 14 is the B. t. u. contained in the gas per pound of dry coal fired. This value divided by the heating value of the coal (Column 9) equals the thermal efficiency of the producer. Column 15 is the pounds of dry coal consumed by the producer per brake-horse- power available for outside purposes. In comparing the results of the producer tests as set forth in Table 11, too much emphasis can not be given the fact that they were subjected to absolutely no refinements. With the exception of three coals one test only has been made on each kind and grade, and the result of each test has, to a great extent, depended upon the ability of the operator to discover the best methods of handling a given coal within the 8 or 10 hours allowed preliminary to the offi- cial test. Moreover, all tests were made on one type and in one size of producer, a type designed primarily for anthracite coal, and in carrying out the plan of the tests more effort was made to develop the required power than to observe the proper relation between the gas producing qualities of the coal and the area of the fuel bed. In spite of all these restrictions it is the opinion of those who were in charge of the tests that certain general relationships have 100 90 80 70 60 50 3 40 30 fe 20 o 10 10 1(1 18 12 14 Ash Per Cent FIG. 13 CUBIC FEET OF GAS PER POUND OF COAL AS AFFECTED BY PER CENT OF ASH IN DRY COAL FUEL TESTS WITH ILLINOIS COAL 49 been fairly well established. They may be subject to modification in the light of future investigations, but the conclusions to be drawn from them are sufficiently significant for presentation. 29. Efficiency as affected ~by ash in the coal. The cubic feet of gas delivered by the producer per pound of coal fired is, perhaps, the most convenient measure of efficiency. Referring to Column 13, Table 11, it will be seen that in general as the ash in the coals increases this quantity decreases. The exact relation for all tests made at full load is shown graphically in Fig. 13. In this figure, cubic feet of standard gas per pound of dry coal is plot- ted against ash expressed in per cent of dry coal. The average line is drawn so as to include as many of fche plotted points as possible. It shows that when the coal contains 8 per cent ash the output of the producer is 67 cubic feet per pound of dry coal fired and that when ash is 20 per cent the output is decreased to 50 cubic feet. 30. Efficiency as affected by calorific value of the coal. The cubic feet of gas per pound of dry coal plotted against B. t. u. per pound of dry coal for all tests made at full load is shown in Fig. 14. Since the heating value of Illinois coal is very nearly inversely proportional to the ash content the relation shown is merely a restatement of the facts brought out in Fig. 13. The points, however, fall in better alignment. It appears from the curve that the output of gas in cubic feet per pound of coal increases from 49 when the calorific value is 1 1000 B. t. u. per pound of dry coal, to 65 when the calorific value is 13000. Fig. 15 shows the efficiency expressed in per cent plotted against the heating value of the coal. Here the same rise in efficiency is again shown. The average value at 11000 is 58 per cent and at 13000 it is 76 per cent. 50 ILLINOIS ENGINEERING EXPERIMENT STATION 100 o 90 O 80 7 - B 10 o 11000 12000 13000 B. t, u. per pound of Coal 14000 FIG. 14 CUBIC FEET OF GAS PER POUND OF COAL, AS AFFECTED BY CALORIFIC VALUE OF THE COAL 100 W 10 11000 12000 13000 B. t. u. per pound of Coal 14000 FIG. 15 EFFICIENCY OF PRODUCER AS AFFECTED BY CALORIFIC VALUE OF THE COAL FUEL, TESTS WITH ILLINOIS COAL 51 31. A comparison of Illinois coal with other bituminous coals. A condensed summary of the more important items relating to Illinois coals compared with those relating to all other bituminous coals tested, is presented in Table 12. The average values given TABLE 12 A COMPARISON OF ILLINOIS COAL WITH BITUMINOUS COALS FROM OTHER STATES FOR GAS PRODUCER SERVICE Average of Tests with 111. Coal Average of All Tests with Bitum- inous Coal Composition of fuel, per cent: Moisture 10 84 6 82 Volatile matter . . 33 06 33 06 Fixed carbon 44 06 49 80 Ash 12 04 10 32 Sulphur 3 15 2 41 B. t. u, per pound of dry coal ... 12000 13150 Composition of gas, volume per cent: Carbon dioxide . . . 9 60 9 84 Oxygen . . . 03 04 Nitrogen 56 81 55 60 Hydrocarbons 3 21 3 30 Carbon monoxide . ... 18 31 18 28 Hydrogen 12 01 12 90 B. t. u, per foot of standard gas 146 5 152 1 Cubic feet of standard gas per pound of dry coal 59 1 64 7 Pounds of dry coal per brake horse power, hour 1.36 1 26 are computed only from tests in which the producer was operated at its rated capacity. It will be noted that while the analysis shows that the Illinois coal contains 4 per cent more moisture and 2i per cent more ash the quality of the gas produced is but slightly inferior. Thus the heating value is 146.5 B. t. u. per foot of standard gas when Illinois coal is used and 152.1 when other bituminous coal is used. The output of gas, measured in cubic feet per pound of dry coal, is 59.1 in the one case and 64.7 in the other. Comparing the efficiency at the engine it will be seen that it requires 1.36 pounds of Illinois coal to develop a horse- power and 1.26 pounds when other bituminous coals are used. This comparison is by no means unfavorable and consid- ering the lower selling prices which prevail for Illinois coals the very slight difference in efficiency is almost insignificant. 32. Relative results of steam and producer-gas tests. From theoretical considerations it may easily be shown that it is pos- sible for the gas engine to utilize a much larger amount of the ILLINOIS ENGINEERING EXPERIMENT STATION RELATIVE AMOUNT OF ILLINOIS COAL USED BY STEAM AND PRODUCER PLANT POUNDS PER BRAKE HORSE-POWER HOUR OQ Steam Plant Producer Plant Ratio *7A 11C 7C 27 *7B 190 21 *23B *6B 4 9B 26 8 3 23A 29B 22A 16 15 14 13 18 30 25 10 24B 19B 11A *11D *11D | i 01234 * No producer test. FIG. 16 RELATIVE COAL CONSUMPTION IN GAS AND STEAM PLANTS. FUEL TESTS WITH nJ#K#ISr-@OAI/- J ' J 53 heat supplied than the steam engine. The results of the present tests show how much of this saving is realized in practice. The ratios of the total coal per brake horse- power hour re- quired by the steam plant and producer gas plant under full load conditions are presented in Fig. 16. The values representing producer plant performance are those of Column 15, Table 11, and those representing steam plant performance are calculated from those of Column 25, Table 8, allowing 85 per cent as the efficiency of the dynamo. It will be seen that the maximum ratio is 3.13 and the minimum 1.50 while the average is 2.61. 54 l iLilNbW ENGINEERING EXPERIMENT STATION UNITED STATES GEOLOGICAL SURVEY PUBLICATIONS ON FUEL TESTING The following publications, except those to which a price is affixed, can b^ obtained free by applying to the Director. Geological Survey, Washington. D. C. The priced publications can be purchased from the Superintendent of Documents, Government Printing Office, Wash- ington. D. C. Jhdletin No. 261. Preliminary report on the operations of the coal-testing plant of the Unit' d States Geological Survey at the Louisiana Purchase Exposition, in St. Louis, Mo., 1904; E. W. Parker, J. A. Holmes, M. R. Campbell, committee in charge. 1905. 172 pp. 10 cents. Professional Paper No. 48. Report on the operations of the coal-testing plant of the United States Geological Survey at the Louisiana Purchase Exposition, St, Louis, Mo., 1904; E. W. Parker, J. A. Holmes, M. R. Campbell, committee in charge. 1906- In three parts. 1492 pp. 13 pis $1.50. Bulletin No, 290. Preliminary report on the operations of the fuel-testing plant of the United States Geological Survey at St. Louis, Mo., 1905, by J- A. Holmes. 1906. 210 pp. 20 cents. Bulletin No. 323. Experimental work conducted in the chemical laboratory of the United States fuel-testing plant at St. Louis, Mo., January 1, 1905, to July 31, 1906. by N. W. Lord. 1907. 49pp. Bulletin No. 3S5. A study of four hundred steaming tests, made at the fuel-testing plant, St. Louis, Mo., 1904, 1905, and 1906. by L. P. Breckenridge. 1907. 196 pp. Bulletin No. 332. Report of the United States fuel-testing plant at St. Louis, Mo., January 1, 1906, to June 30, 1907; J. A. Holmes, in charge. 1908. 299 pp. Bulletin No. 334. The burning of coal without smoke in boiler plants: a preliminary re- port, by D. T. Randall. 1908. 26 pp. Bulletin No. 336. Washing and coking tests of coal and cupola tests of coke, by Richard Moldenke, A. W. Belden. and G. R. Delamater. 1908. 76 pp. Bulletin No. 339- The purchase of coal under Government and commercial specifications on the basis of its heating value, with analyses of coal delivered under Government contracts, by D. T. Randall. 1908. 27 pp. Bulletin No- 343. Binders for coal briquets, by J. E. Mills. 1908. 56pp. Bulletin No. 362. Mine sampling and chemical analyses of coals tested at the United States fuel-testing plant, Norfolk, Va.. in 1907, by J. S. Burrows. 1908. 23 pp. Bulletin No, 363. Comparative tests of run-of-mine and briquetted coal on locomotives, by W. V. M. Goss. 1908. 57 pp. Bulletin No. 366. Tests of coal and briquets as fuel in house-heating boilers, by D. T. Randall. 1908. 44 pp. Bulletin No. 368. Washing and coking tests of coal, by A. W. Belden, G. R. Delamater and J. W. Groves. 1908. 53 pp. PUBLICATIONS or THE ENGINEERING EXPERIMENT STATION Bulletin No. 1. Tests of Reinforced Concrete Beams, by Arthur N. Talbot. 1904. (Out of print.) Circular No. 1. High-Speed Tool Steels, by L. P. Breckenridge. 1905. (Out of print.) Bulletin No. 2. Tests of High-Speed Tool Steels on Cast Iron, by L. P. Breckenridge and Henry B . Dirks. 1905. ( Out of print. ) Circular No. 2. Drainage of Earth Roads, by Ira O. Baker. 1906. (Out of print.) Circular No. 3. Fuel Tests with Illinois Coal. (Compiled from tests made by the Tech- nologic Branch of the U- S- G. S.. at the St. Louis, Mo., Fuel Testing Plant, 1904-1907, by L. P. Breckenridge and Paul Diserens. 1909. Bulletin No. 3. The Engineering Experiment Station of the University of Illinois, by L. P. Breckenridge. 1906. (Out of print.) Bulletin No. 4. Tests of Reinforced Concrete Beams. Series of 1905, by Arthur N. Talbot. 1906. Bulletin No. 5. Resistance of Tubes to Collapse, by Albert P. Carman. 1906. ( Out of vrint.) Bulletin No. 6. Holding Power of Railroad Spikes, by Roy I. Webber. 1906. (Out of print.) Bulletin No. 7. Fuel Tests with Illinois Coals, by L. P. Breckenridge, S. W. Parr and Henry B. Dirks. 1906. (Out of print.) Bulletin No. 8. Tests of Concrete: I. Shear; II. Bond, by Arthur N. Talbot. 1906. (Out of print.) Bulletin No. 9. An Extension of the Dewey Decimal System of Classification Applied to the Engineering Industries, by L. P. Breckenridge and G. A. Goodenough. 1906. Bulletin No. 10. Tests of Concrete and Reinforced Concrete Columns. Series of 1906, by Arthur N. Talbot. 1907. (Out of print.) Bulletin No. 11. The Effect of Scale on the Transmission of Heat through Locomotive Boiler Tubes, by Edward C. Schmidt and John M. Snodgrass. 1907. (Out of print.) Bulletin No. 12. Tests of Reinforced Concrete T-beams. Series of 1906. by Arthur N. Talbot. 1907. (Out of print.) Bulletin No. 13. An Extension of the Dewey Decimal System of Classification Applied to Architecture and Building, by N. Clifford Ricker. 1907. Bulletin No. 14. Tests of Reinforced Concrete Beams, Series of 1906, by Arthur N. Talbot. 1907. (Out of print.) Bulletin No. 15. How to Burn Illinois Coal without Smoke, by L. P. Breckenridge. 1908. Bulletin No. 16. A Study of Roof Trusses, by N. Clifford Ricker' 1908. Bulletin No. 17. The Weathering of Coal, by S. W. Parr, N. D. Hamilton, and W. F. Wheeler. 1908. (Out of print.) Bulletin No. 18. The Strength of Chain Links, by G. A. Goodenough and L. E. Moore. 1908. Bulletin No. 19. Comparative Tests of Carbon, Metallized Carbon and Tantalum Fila- ment Lamps, by T. H. Amrine. 1908. Bulletin No. 20. Tests of Concrete and Reinforced Concrete Columns, Series of 1907, by Arthur N. Talbot. 1908. Bulletin No. 21. Tests of a Liquid Air Plant, by C. S. Hudson and C. M. Garland. 1908 Bulletin No. 22. Tests of Cast-Iron and Reinforced Concrete Culvert Pipe, by Arthur N. Talbot. 1908. Bulletin No. 23. Voids, Settlement and Weight of Crushed Stone, by Ira O. Baker. 1908. Bulletin No. 24. The Modification of Illinois Coal by Low Temperature Distillation, by S. W. Parr andC. K. Francis. 1908. Bulletin No. 25. Lighting Country Homes by Private Electric Plants, by T. H. Amrine. 1908. Bulletin No. 26. High Steam-Pressures in Locomotive Service. A Review of a Report to the Carnegie Institution of Washington. By W. F. M. Goss. 1908. Bulletin No. 27. Tests of Brick Columns and Terra Cotta Block Columns, by Arthur N. Talbot and Duff A. Abrams. 1909. Bulletin No. 28, A Test of Three Large Reinforced Concrete Beams, by Arthur N. Talbot. 1909. Bulletin No. 29. Tests of Reinforced Concrete Beams: Resistance to Web Stresses, by Arthur N. Talbot. 1909. Bulletin No. 30. On the Rate of Formation of Carbon Monoxide in Gas Producers, by J. K. Clement. L. H. Adams, and C. N. Haskins 1909. Bulletin No, 31. Fuel Tests with House-heating Boilers, by J. M. Snodgrass. 1909. Bulletin No. 32. The Occluded Gases in Coal, by S. W. Parr and Perry Barker. 1909. 3 *"? c UNIVERSITY OF CALIFORNIA LIBRARY Illinois State Reformatory Print