• A 13 . i "*" .:.. :: I OFL. ORNL P 2126 . ta 1 • ) " . . in . 1. 0 . . votreberica Y . t . 4 T! . . 1 . . . . . . . 7 11.25 4 1.1.5 MICROCOPY RESOLUTION TEST CHART NATIONAL BUREAU OF STANDARDS - 1963 I . " . . C ORNU 8-21966 Cant-6609an-1 MASTER MAY 10 1966 MODEL AND UNDERGROUND STUDIES OF THE INFLUENCE OF STRESS, TEMPERATURE AND RADIATION ON FLOW AND STABILITY IN ROCK SALT MINES, O R. L. Bradshaw, T. F. Lomenick, W. C. McClain, and F. M. Empson CESTI PRICES Healt}. Physics Division Oak Ridge National Laboratory, Oak Ridge, Tennessee RELEASED FOR ANNOUNCEMENT H.C. $ 4.00; MN_50 IN NUCLEAR SCIENCS ABSERICH I. INTRODUCTION Reprocessing of nuclear power reactor fuel produces a radioactive waste which must be isolated from the environment for centuries. The most promising disposal method for these heat-generating westes is con- version to solids, followed by final disposal in a salt mine. In order to be able to design a radioactive waste disposal facility in a salt mine, it is necessary to be able to predict the effects on mine stability of both supporting-pillar stresses (produced by the superincumbent earth strata) and elevated temperatures (produced by radioactive decay of the fission products in the waste). Research in this area has been carried out in the laboratory using model pillars, and in a 1000-ft-deep (305 m) salt mine in Kansas using reactor fuel and electrical heaters in a specially excavated area. S . . . .. . ... For publication in the Proceedings of the International Society of Rock Mechanics, First International Congress, September 25 to Octo- ber 1, 1966, Lisbon, Portugal. Research sponsored by U. S. Atomic Energy Commission under con- tract with Union Carbide Corporation. NOT ARABoyЕрте р La n gai orientation HEAEG AND HIS the 2. SAIT MOVEMENT IN MINES In general, when an opening is created in a salt mine, there is a flow of salt into the opening. The rate at which the opering closes is dependent won such factors as depth of the mine, percentage of the area extracted, extent of the area already mined, shape and height of the pil- lars, temperature of the salt, and time since creation of the opening. In flat-lying (bedded) deposits where shale is interbedded with the salt, the flow of salt frequently causes separation of layers of salt from the shale layers with resultant floor heaves and ceiling sags. If too much salt is exüracted, if the supporting pillars are not properly sized, or if the thickness of the layers of salt in the floor and in the roof (down to and up to the first shale layers) is not great enough, the floor heaves may be large enough to interfere with the movement of ma- . chinery, and hazardous roof falls may occur. Even in mines where salt flow does not cause trouble during the mining operation, roof falls and floor heaves may occur after an extended period of time, perhaps decades. Sufficient empirical data on existing salt mines are available to: enable predictions to be made on the stability of mines at ambient tem- perature, but no data or experience are available which are directly applicable at elevated temperatures. Recent work by Seratat and Obert . at ambient temperatures has shown that flow in rock-salt mines may be approximated by testing scale-model specimens uniaxially by providing proper horizontal restraint over the floor and roof portions of the model. -... . . . . . . . . - - LEGAL NOTICE This roport me preparod an account of Government sponsored work, Nuither the United Statau, dor ebe Commission, nor any person acting and behalf of the Commiundon: A. Makss way warranty or repromatatha, expressed or implied, with raspect to the accu- racy, completeness, or wofalnou of the information contained in this report, or that the word of any information, apparatu, mothod, or procesu discloved in the report may not infring privately owned richta; or D. Asnimos hay liabilues with respect to the une of, or for damage resulter from the on of any information, apparitus, molbod, or procou dixcloued to this report As med in the above, "parrow nothing on behalf of the Commiustom" laoludne way on. ploys or contractor of the Commission, or employee of such contractor, to the extrat det noch employee or contractor of the Commission, or employee of much contractor preparou, dhiminates, or provides access to, wam laformaatios partient to Me employment or contract with the conaminaton, or his employweat with such contractor. . ni it . .. . 3. 3. MODEL STUDIES ON EFFECTS OF TEMPERATURE AND STRESS , .. We have studied the behavior of scale-model pillers at temperatures up to 200°c and stresses up to 10,000 psi (703 kg/cm?).” To simulate pillar, roof, and floor conditions in mined cavities in rock salt, sample specimens were fabricated to represent scale models of salt pillars and their surrounding rooms. The test, specimens were cylindrical in shape, with a portion of the center ground out to form the pillar and surround- ing rooms (Fig. 1). Steel rings attached around the ends of the samples effectively supplied confining pressure to the roof and floor portions of the models as they were loaded. 1. The following approximate empirical equations have been fitted to the results of these pillar-model tests for times from 10 hr on. € = 3.2 x 10-36 720.9 -3.2 +-0.65 E = 9.2 x 10-36 710.9 23.2 +0.35+ A : where Se ė = strain rate (vertical convergence, 1 in. in.-hr-?), : € = cumulative deformation (u in. in.--), T = absolute temperature (°K), o = average pillar stress (psi), t = time (hr), and A = constant adjusted to fit experimental curve at 10 hr. U · Extrapolation of the rate equation produces predicted creep-closure : * rates which are in reasonable agreement with rates measured in the Kansas mines since 1959.* The relationships between vertical and horizontal closure rates measured in the models also have been corroborated by meas- urements in the mines. 2 5 t . . * . W IK . . :. . ORNL-OWG 65-1543 .. .-> Til Wi; . INTIIMIIMILLUS . LTUMTU . . 'PILLAR ROOF 'FLOOR STEEL RING one ano foi o 2010 sets *** * fig.!.. Model of Salt Pillar REY 5 . wit.* .. . . 1. In a model of the type shown in Fig. 1, 1/8-in.-diam (0.32 ca). horizontal holes were drilled at the top and bottom of the pillar and filled with colored salt before the sample was deformed about 60%. The floor-to-ceiling dimension was reduced from 1 in. (2.5 cm) to about 0.4 in. (1 cm). After deformation, the model was saved in half, vertically, along the plane containing the holes. The result is shown in Fig. 2. ** It is evident that the sait-filled holes are no longer horizontal and are much closer together at the sides of the pillar, thus showing that some of the salt from above and below the pillar has flowed out into 3.1 2. . * ܝܪܫ ܕܝܺܫܺܫܫ * : * ts . I the floor and roof of the cavity. Strain gages attached to the steel restraining rings showed that a horizontal (radial) stress, equal to about 50% of the average vertica). pillar stress, was transmitted to the rings. The model tests have thus shown, in a qualitative way, why floor heaves and roof sags take place. Cavity closures, as functions of time, for models axially loaded to 4000 10/in.2 (280 kg/cm?) and 6000 16/in.2 (420 kg/cm²) at temperatures of 22.5°, 60°, and 200°C are shown in Fig. 3. It is clear that elevated temperature has a marked effect on deformation rates. Note also that the 12 -. . deformational behavior of the pillar loaded to 4000 psi at a temperature 16 Ihr of 60°C is approximately the same as the sample loaded to 6000 psi at . SA roor. temperature. This illustrates that the effects of elevated tempera- ture on deformational betavior are much the same as those of increased stress. However, at temperatures of 100°C and above, the deformational behavior of the models departs somewhat from that produced by increased stress. This is illustrated by the pair of curves for the 60° and 100°C samples at 6000 and 4000 psi in Fig. 3. At higher temperatures, the pil- . . . lars tend to behave more plastically with consequently reduced spalling. V !" Ki -.AFT day. 2. Section that in allen anal After * sonra Domodo .. : : :. RO. memori.....: . . ideo conosna ... siamo i in modo sin tid med hont concise manne and can commodo consenso ai dedicada en musica . w ..... . . . . -- - ' . S 1 W. H Y . . 222 - VY S72TYS Watch 12 بيا ORNL-DWG 65-1542 6000 psi 100 °C VERTICAL SHORTENING OF PILLARS (in.) 4000 psi 100 °C . . 96000 psi 60 °C i 2 . - * 4000 psi 60 °C 6000 psi 22.5 °C 4000 psi 22.5 °C A 3. . i. . . oo 50 100 200 250 300 ET 150 TIME (hr) dia 3. Deformation of models at Different y temperatures and stresses. 422 - ? In many cases salt is mined to a shale. layer (sometimes called a "parting") since these layers are planes of weakness at which the salt will readily separate. The presence of shale partings can have a sig- nificant effect on the rate of cavity deformation, depending on whether the shale is at the top and bottom of the pillar or in the center of it. This is shown in Fig. 4 by the deformation curves of model pillars de- formed both with and without simulated shale partings (greased teflon sheets) in the piilar. The actual effects to be expected in a mine would lie somewhere between the two extremes show in Fig. 4. E ' S. P: t - EXPERIMENTAL FACILITY IN KANSAS MINE TL . . 97 . . . . . - . . 7711 . 15 9,. . 4 The demonstration disposal of high-level radioactive waste solids, initiated in November 1965 in the Carey salt mine at Lyons, Kansas, is known as "Project Salt Vault."5,6 Among the objectives of the demonstra- . .. . . . . _ Lar. tion are confirmation of feasibility and safety of disposal in salt mines, 12 SET . IND . 1.-1! and collection of information on creep, plastic flow, and mine stability which are needed for the design of an actual waste-disposal facility. Since highly radioactive waste solids are not available currently, ir- radiated reactor fuel assemblies with supplemental heaters are used as the heat and radiation source. It might be expected that a logical choice of space for waste dis- posal would be in existing mined-out areas. However, in the Lyons mine, as in most other mines in bedied (flat-lying) salt deposits, the salt be- neath the floor (where the holes for the waste containers would be drilled) contains layers of shale with a few percent water content which is driven out at temperatures above 100°C. This could produce problems of increased Si .. , ' $ E ? " ORNL-DWG 65-10988 . : 0.24 WITH FRICTION REDUCER AT FLOOR AND CEILING VERTICAL SHORTENING OF PILLARS (in.). WITHOUT FRICTION REDUCER WITH FRICTION REDUCER AT CENTER OF PILLAR 0 20 40 60 80 100 120 140 TIME (hr) Deformation of Model Rock Sali Pillars at 4000 psi. dig. 4. affects of Shale Partings on Deformation . i nc MA TY litru MAI Wir 10 corrosion of the waste containers and possible movement of radioactivity out iuto the mine. Also, floor heaves, rocf falls, and sagging roof in LE all but the most recently mined areas (Operating period of the Lyons mine was from the 1890's to 1948.) pose rehabilitation problems which might be as expensive as mining new space. Therefore, it was decided to create a newly mined area at the periphery of the mine, at a higher level and of the most desirable gecmetry, so as to have the purest salt strata in the floor where the radioactive sources will be located. The layout of the specially mined, 300-ft-long (91 m), expérimental area is shown in Fig. 5. In the first room is located the main radioac- tive array which consists of seven 12-ft-deep (3.7 m) holes in the floor. 70 . Seven 7-ft-long (2.1 m) reactor fuel containers were placed in the holes GET in November 1965. For comparison with the main radioactive array, a TRX- geometrically similar array, containing electrical heat sources, is low cated in the fourth room. A third array, duplicating the main radioactive array but located in the original mine floor, will ne loaded with used radioactive sources about June 1966. In adlition, the temperature beneath the center pillar of the experimental area will be raised to about 100°C . by means of electrical heaters in the floor. Since this pillar-heating . test may produce extreme salt movements, it will not be started until near the end of 1966. 5. THERMAL STRESS EFFECTS IN THE MINE At the end of December 1965 (46 days after start-up) the salt tem- perature at the wall of the peripheral holes of the main radioactive { rray was about 120°c, and at the wall of the center hole approximately 135°C. ORNL-DWG 63-774 AR2 DU WO UVOD FEET 50 100 150 . ELECTRICAL ARRAY . 250 30 ft 40ft FEET C AA 118-A-5-17 HEATED PILLAR 109-A-N-2 -111-A-U-3 F. 105-A-U-37 ARRAYS MAIN 100 RADIOACTIVE 50 . SPECIALLY MINED AREA 14-ft ABOVE EXISTING FLOOR- LEVEL WASTE CHARGING SHAFT FROM SURFACE U 30 ft RAMP UP * * C C .: P EXISTING MINE WORKINGS SHOWN APPROXIMATE FLOOR FABIOACTIVE . FLOOR RADIOACTIVE ARRAY 11- DO PEARL . . AN 2 . fig. 5. Layout of Expenmental Area 12 In the vertical cente. planes of the main radioactive and electrical arrays - about 9 ft (2.7 m) below floor level - essentially the entire area with a circle formed by the peripheral holes (that is, a circle of about 10-ft (3 m) diameter) was at or above 100°c. Vertical thermal expansion of the floor in the center of the arrays had reached nearly an inch (2.5 cm) by the end of December 1965. The MO PE cx floor uplift (measured in feet) as a function of time for each array at ". . the center and 10 ft (3 m) from the center 18 shown in Fig. 6b. It may be observed that the rate of rise in and near the array is slowing down. This is due to the fact that the rate of rise of the salt temperature is also slowing down. In Fig. 6a is shown the uplift profiles for room 1 (radioactive array), along the north-south and east-west axes of the room. It is apparent that thermal expansion of the material in the floor extends to 40 or 50 ft (12 to 15 m) from the center of the array. The north-south uplift profile shows the restraining effect produced by the presence of the adjacent ... E pilla-s. c. Figure 70 shows the transverse expansion (in inches) taking place in the pillar which borders the radioactive array room on the north side. The curve labeled 109-A-N-2 is a measure of the amount of horizontal ex- pansion taking place between the surface of the pillar (about halfway up from the floor on the south face of the pillar) and a point about 10 ft in toward the center of the pillar. The curve labeled 118-A-S-1 is the corresponding measurement made from the north face of the pillar. (Lo- cations of the gages are shown in Fig. 5.) The power was turned on in the array at 806 "standard days" (November 15), and almost immediately . ORNL-DWG 66-618 la) 50.050 : FLOOR UPLIFT (ft) NORTH-SOUTH PROFILE EAST-WEST PROFILE CENTER OF al EXPERIMENTAL AREAL . NORTHERN ENTRY TUNNEL EDGE OF ROOM 0.025 SOUTHERN EDGE OF ROOM : . 25 15 5 5 15 25 35 DISTANCE FROM CENTER OF ARRAY (ft) 45 0.100 0.075 CENTER OF ARRAY To FLOOR UPLIFT (ft) 0.050 10 ft FROM CENTER ū0.025 O ROOM 1 (RADIOACTIVE ARRAY) ROOM 4 (ELECTRICAL ARRAY) 0 10 20 30 40 50 60 70 TIME (DAYS) (a) Floor Uplift Profiles in Room 1 as of December 30, 1965. (6) Floor Uplift in Array Rooms. figure 6. Iloor Uplift Due to Thermal Expansion : ORNL-DWG 66-619 lo) 105-A-U-3 ill Co-o-oto-o-o-200 111-4-u STARTUP INCHES (6) 109-A-N-2 20-0°448-A-S-1 -- STARTUP 06288=:=8=:*:- 850 900 650 700 750 800 STANDARD DAYS (a) Movement of Ceiling Relative to Six Feet Up. (6) Transverse Expansion in Pillar 1-2.. dig. 7 Pillar and Roof hovement Due to - Thermal Stresses . : the other that comel.. 1* the expansion rate on the south side of the pillar increased from about 0.15 in./yr (0.38 cm/yr) to about 0.45 in./yr (1.14 cm/yr), a threefola increase. This marked increase in expansion rate halfway up the pillar was due primarily to a transfer of thermal stress from the center of the floor, since the increased rate was detected before any appreciable tem- perature rise had taken place beneath the pillar. The fact that the ex- pansion rate has not tended to decrease with time (as has the rate of floor uplift) is due to the fact that some temperature rise 18 now tak- ing place beneath the pillar (about 10°c at the south edge of the pillar as of December 30). It will be noticed that the north side of the pil- lar has also experienced a slight increase in stress (curve 118-A-S-1). A similar behavior has been observed in the wall on the south side of the room, and the behavior of the electrical array room is also essen- tially the same. The transfer of stress has not been limited to the adjacent pillars, but has extended to the ceiling as well. That this should be so is at- tested by the results of the pillar model tests described earlier. There, it may be remembered, an axially applied load resulted in movement of salt from above and below the piller out into the roof and floor of the 2 opening. Figure 7a shows the movement of the ceiling relative to a point, 6 ft (1.8 m) up into the roof. The curve labeled 111-A-U-3 is the roof- gage data for a point 10 ft from the center of the radioactive array (10 ft toward the mouth of the room, Fig. 5). The other curve (105-A-U-3) is for a point about 45 ft (14 m) from the center of the array, out in the middle of the access corridor (Fig. 5). It will be noticed that almost immediately after start-up (806 "standard days") there was about a fivefold increase in the rate of roof movement near the array (increase in rate of sag from $. y ciutat ciutat *. VES about 0.12 to 0.55 in./yr (0.30 to 1.40 cm/yr), and a substantial increase in the sag rate out in the entry corridor (from about 0.16 to 0.42 in./yr - 0.41 to 1.04 cm/yr). The data for the electrical array room show similar movements taking place. Most of this movement appears to be separation of the 2-ft-thick (0.6 m) salt layer in the roof from the thin shale layer immediately above it. Movement rates would be expected to be lower if the salt layer were thick enough to resist buckling, and a test is planned to determine if the 2-ft-thick layer can be effectively bolted to the 3-ft-thick (0.9 m) salt layer above the shale parting. . Salt flow behavior in both the radioactive and electrical array rooms has been essentially the same. It 18, therefore, concluded that thermal effects on salt flow are much more important than radiation effects. CONCLUSIONS The pillar-model tests have proven themselves to be useful for under- standing the way in which salt movements take place, and it is reasonable to expect that the predictions based on the elevated temperature models will be valid also. No measurable effects of radiation on the flow of salt were expected, and none have been observed during the first 50 days of operation of the demonstration. Thermal expansion of the floor, and increased transverse expansion rates in the pillars adjacent to the array rooms, have been about as expected. The acceleration of movement in the ceiling (separation of a 2-ft- thick salt layer) has exceeded that which was anticipated from the thermal 27 effects in the floor; however, the magnitude of the movement 18 such that no trouble 18 expected from this source during the operation of the demonstration. Even in an actual operation, movements of this mag- trouble se ected from this sourc on of nitude (or even greater) should not cause trouble during the time when a room 18 still being filled with radioactive waste, and, after the room 18 filled, it is anticipated that it will be backfilled with crushed salt. The increased roof movement does Indicate, however, that an extra margin of stability must be allowed in the initinl design of the waste disposal facility. .. 18 7. REFERENCES 1. S. Serata, "Theory and Model of Underground Opening and Support Sys- tem," in Proceedings of the Sixth Symposium on Rock Mechanics, Rolla, Missouri, October 1964, University of Missouri at Rolla, 1964, pp. 260-292. 2. and Potash Ore," in Proceedings of the Sixth Symposium on Rock Mechanics, Rolla, Missouri, October 1964, University of Missouri at Rolla, 1964, pp. 539-560. . 3. 2. T. F. Lomenick and R. L. Bradshaw, "Accelerated Deformation of Rock Salt at Elevated Temperature," Nature 207(4993), 158-159 (July 10, .1965). . 4. R. L. Bradshaw, W. J. Boegly, Jr., and F. M. Empson, "Correlation of Convergence Measurements in Salt Mines with laboratory Creep-Test Data," in Proceedings of the Sixth Symposium on Rock Mechanics, Rolla, Missouri, October 1964, University of Missouri at Rolla, 1984, pp. 501- 514. . R, L. Bradshaw, J. 0. Blomeke, W. J. Boegly, Jr., F. M. Empson, F. L. Parker, J. J. Perona, and W. F. Schaffer, Jr.; "Disposal of High AC- tivity Power Reactor Wastes in Salt Mines: A Concept and Field Scale Demonstration," Nuclear Structural Engineering 2, 438-446 (October 1965). W. J. Boegly, Jr., R. L. Bradshaw, F. M. Empson, W. F. Schaffer, Sr., F. L. Parker, and J. O. Blomeke, "Project Salt Vault: A Demonstra- tion Disposal of High-Level Radioactive Solids in Lyons, Kansas, Salt . Mine," Health Physics 12, 417-424 (March 1966). + - 1 END DATE FILMED * . 2 SE- 1 . - . . . . * N * . N 277 5. 2 W 14 LY! -