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 :| H- 
 
 

 LABORATORY 
 
 OF THE 
 
 INLAND REVENUE DEPARTMENT 
 
 OTTAWA, CANADA 
 
 BUT.T.ETII^ >q-o. ?^ll 
 
 OIL OF TURPENTIISrE 
 
 5026—1 
 
■ii 
 
 
 
 Ul:i 
 
 f . 
 
 ,^^i 
 
LABORATORY 
 
 or THE 
 
 INLAND REVENUE DEPARTMENT 
 
 OTTAWA, CANADA 
 
 BULLETIISr No. Qll 
 
 OIL OF TURPEKTINE. 
 
 
 W. J. Gkbald, E«q., Ottawa, July H, 1910. 
 
 Deputy Minister of InUnd Revenue. 
 
 a , A ^r no residue lemainini' ". ' 
 
 100 u. (JU.S F. . whicii IS the figure iriven in the BP Tim Pr .1 "' *"^".'' 
 distils completely between 16.5' and 162"C Tsi" and 3036 P TK R P 1 .''"'V '* 
 It should distil almost entirely telow 80°C 3.56-F? Thf. f'^' ^^ ^'^^ *****? ^^"^ 
 
 tTrr5?r "-r^r ^. ^--«yrat!'thl^r;tlon" •suit vary nX^Tti 
 + 14. A 52 lb. quantity when fractonallvHUmin^ /on 'An :: ,i. >",*', "^°'" 1/ '" 
 
 the R P th« tV<sV '.u''^;^'"' ''?''''»« point, namely from -0 
 
 the B.P the F.S.P. nor the P.O. refers to the optical rotation. 
 6026 — I J 
 
 ana 
 hich 
 Neither 
 It is officially stated 
 
■IT" 
 
 H\ 
 
 ti. l)c soluble ill its own volutin of Oliiciiil Acetic Aciil. This lent hiin Ih-iii »Ii<..mi 
 (I'.J. 'I'L'. i.r)0:t) l>y thf iiuthor iitid ('. M. CtiiiieK to hr jTiiclically <>/ lui viil,f an a test 
 for Oil of Turpriit'ine, altlioiiRli useful nt i» tost of the strfiiKth of (iluci.il Acctio Ai i.j. 
 An iicid coiifoiininu strictly to tli.' H.K titration test (which r«-<|uir's a il'linite ti;,'un') 
 cjinnot 1* t'xiM'ctiHJ to form" 'i clmr solution with all - pU's of Oil of Tin i.«ntine « l.fii 
 niixfd in im|Uii1 voIuuk-s. t'oiiiinerfiiil Hanipk-s of tJliuirtl A<elic Ariil which re(|uirc 
 more than the li.R hf{urf will mix rcinlilv without Hul>st(.|uciit si(..4rnrii)ii. ami most of 
 the couiuw icial acids (5i\e a hi;.'lier tijjure than thn ll.l'. With such samples of Oil of 
 'I'lirpentinc as ha<l up to thai time h»fn examine<i the mixturi' of any of them in eijual 
 volumes with (ilacial Acetic .\ciil. temperat'ue 14.4' to Hi. 7 C. (5,s to iii" F.) iH-canio 
 a delicate test for a streii;.'h of U'J.") p. c. acid or stronger. The test is also referred to 
 under Acidum Aceticum (Uaciale. 
 
 The more (^eneially oceurrin;^ impurities arc Petroleum, I'uratHn (hU, ISottiri, Rosin 
 Oil, I'ctrolcii.u Itenziii, Kei(is<'iie Oil or similar liydrwarltons. Petrolcuiri, ParalKn Oils 
 of Honin, if present, may Im' detected hy the residue lest. Kerosene or Ho-in Oil, if 
 present, hy the evaporation test. Petroleum llcn/.in, Kerosene and sinular hydro- 
 i-arls>n8 hy the Sulphuric Acid test, each of which tests is de»crH)ed in small type Iwlow. 
 Some work done in the laUaatory of the Canadian Iidand Hevenue department (CD. 
 'dj, i.9.''t.")) has resulted in the following ilefinition of Oil of TurfK-ntine, which mi:»t, 
 however, ho rei;arded as provisional, and 'lubject to corre.;tion and ainplihcaliun ; it 
 should l)e cohmrless, in thin layers, clear, hut niaiie di'cid.slly opn<|ue hy shaking with 
 1.0 p. c. of water, anti Jjivinj,' an opaque distillat* of one tenth volume w!,ich .settles 
 clear in a few hours. The peculiar and characteristic (slour i)uite distinct from that of 
 (iasolene, Uosin Oil, or Acetone. It has u sp. ^r. between O.lstiO and O.Hf<() (usually 
 about t<70). Samples which have Ixfii long exposed to the air have a hi^;' r ilensity. 
 The first 10 p. c. fraction has a sp. gr. of Iwtween (>.8.'i<) and 0.870 (usually al,out 0.8(i(») ; 
 the residual tenth should not exct>ed D.'JOO. '1 he boiling point should lie between l.")4" 
 and I')?* t'. (WJ.-i and 31<;.4 F.) ; nine tenths should distil below IfSO C. (.JOC. F.). 
 Fixed residue should not exceed 2 p. c. Hash point about .32' C. (.•*9.6 F.). The optical 
 activity of the first fraction should increase in a plus direction by oxidation. The 
 refractive index at JO C. should lie Ixslween l.t607 and 1.4722, that of the first 
 fraction should not exceed 1.470. Moistened Starch Io<iide paper should U'come blue 
 when suspende«l over Turpentine exposed to the air, free Bromine in solution should be 
 decolorised. Strong Sulphuric Acid should polymeri/.e and char the sample at a boiling 
 temperature, a rise of temperature should result on mixing with Sulphuric Acid. " 
 
 The above may l)e taken aa summing up all that is known of commercial turpentine, 
 and it is amply evident that definitions and limits of variability are much needed. 
 Reference is male to work don<' in this laboratory in 1901 (Bulletin 79). This consisted 
 jn an examination of .^0 samples of commercial turpentine, having regard to the foilow- 
 jiig properties : — 
 
 Physical characters — 1. Colour. 
 
 2. Clearness. 
 
 3. Odor. 
 
 4. Taste. 
 
 5. Tensity. 
 
 6. oiling point. 
 I . Volatility. 
 
 8. Vapor density. 
 
 9. FUsh point. 
 
 10. Viscosity. 
 
 11. Solubility. 
 
 12. Solvent power. 
 
 13. Rotatory power for polarized light. 
 
 14. Refraction. 
 lr>. Fluorescence. 
 10. Oxidisability. 
 
 Chemical characters — 17. Bromine absorption. 
 
 18. Rise of temperature with sulphuric acid. 
 
in t,.n Uy».^ ami l,«vi,.« u v,.||„w r" t „» " '•'' ^'"•P-'f ""•"<• li'|ui<l. <-„/„„r/,«_ 
 
 .l-.k.ilyopa.,u.. by shaking liih^i^^tr^l^Ti'^'^ '""«• ^^''^'-''-t ma.le 
 '.f onefntl. >olu.,.e. winch «.,tleH Hear i„ ' ' ' /w''"'' »" ''^'"7'"-<<i''tillat.. 
 
 t.r..t.,.. .,ui.o distinct fro,„ tim «f «««! i^" „ I* "i"" '''"'"■ ~ r"'"'^ ""'' ''"'"'c- 
 in« tl„.se .xJours to .1,,, extent of K^^ '1'/"" "' ""■ ""^""'.•".J cpHbl. of .|,H«ui, 
 
 ».!>U0. 
 
 n.nrly l.L'.tO (water I.OOO) McWifr^sc;.!^,', -r J''; ""■""'^; "' '" ^'- "^ouM 1« 
 (AI>H instrument). Hh.. Id rf.JoL ? .'/"-/'/'»•'" ..houlH Ik. abo,' .(:< C 
 
 _sl.o..ld not IH, rondei,.,! translncont by diktion ,„ V..„ "' """'-^ '» ""o" of .isphultun, 
 /y comparison with a -M.ple yif„„;rp"r "v ^t"''":- < l^"'^. '-^ '^ »>^-.t n.ude 
 tr«,t,on should increase in. i .li«Htiri"y '^x lain TlT*'?^^ '.r'-Vy - of the Hm 
 ^hould Imlwtween 1.40.!; .nd 1 17'> lL? J .r « ^^'y"-"'"'-" '"de..- at I'O C. 
 '•■*.<»(). Moi,tenc<l i.Hiide of .tarJh" paper !houd^" ' ?*■"""■ *'""'''' ""' "^ "•"I 
 turpentine t-xt^oned to air jw //i' • "''■"""" '''"'' "'"'" "■"•P'-nded ove- 
 
 decolorized, ivn,,,, 1: J^W. '.^T-S^uir J" :?*"^ <r T''"' '7) ^''«'"'d '>e 
 
 T..pS::r;:riSL!ra:^- tLrb^-^^^^^ ^--^'« ^ --'- 
 
 ..at., portion, of the oi.re.in. r^^;:i:zr ^^lEr.rLi: :iv:r 
 
 Of later years, owin,, to ti^T^ro: ^"sc^^c ["'"oro'lne f""" "/ '"''T'""* '""'"''" " '''"' 
 "f the fact that, by treatnen'^t in the d.^ ly oTliH ^ ' "^"""?«" ''»" »-«" tak.„ 
 pi-.xJuct resembling turpentine is ol.tJ Zw ^f ""P'-rheate.l sU-am, a volatile 
 
 -..aterial). This ^U<^ir^:^.X^^^,!:;iSr' '"T: ^''''P^'*"" '•^•- ^-t^ 
 •substance Inking called gum turpen ine re llnhl I *"<.'dK'rpentine, (the original 
 with turp..„tine in «o mfny reZu tlL Tt S^^^^ ""^ '" «-«» "Wti- «1 
 
 the same name. ^ ^ ' "'"' '* ''*^' ''^" ^"""'1 easy to market it under 
 
 -t rSiViSi^rSl-'S/tci^:;^^';:!' j '-'^^ true turpentine i 
 
 the trade ; and .son.e of the che, caTdiffe-n . ^ ''■''" *!""*" '"' ""'^ recognize.1 I. 
 paper by me. -ntributed to thT*^ ctfv o? rhii: "?? 1''" '*" "^" f'"""^'' °"t 
 Indust., Vol. XXVI (1907) p 847) ^ of Chem.cal Industry. (See Jour. Soc. ( 
 
 IS 
 
 by 
 
 in a 
 
 Chem. 
 
 in<iu,t:voi:xxvro907);"84^: 
 
 (Lond'^^.Tgird) '^bTj.Tl'crtfri riXo'^'^^V'^' «T«*^ »' ^^^^- Analyst, 
 ..W. character fr.L that ^JS f^^ ^^ ^'^ ^^S^l^^ai-i^ -- 
 
 The literature of this suWect verv vol!?i ''''T '" ''"" '^''" '" ""^ "the" way. 
 
 contradictory ; many TrK clIimTL t" aT ' T""^ T"*^'^'" ^^ "• ™"'««V'"-. very 
 
 the various iubstitut^es fo t^rtntine^ itUe'if r".! *'■%""' '" ^'""'^ ""'^ ^""■^''-^ 
 It remains, however that the »„„ r ! ^ ' • "' ''"• '"f'"""" '" *''- genuine article 
 
 doHnite Product; a;d:j.o:iTteSsS'"sr, ':oT'^'r' I" ^"'"'' ^"L certain^'ati 
 wuh crtainty to distinguish betwtn^-^pl^ra^'XtbsSteTotiSitrn.^ ^^'^ 
 
t't I 
 
 ■ir 
 
 Th« report now iuliiiiitu<(l ctiriUioH naalU olttained in Uip »n«lyiii« of 73 RiimplM 
 of tur(H>ntino |iiirch«Med in tb i markflii of th« DomiDion, and «»f '^n (10) «amplM, 
 furniilnMl liy iuiport*r»i iiml oth»rit. TJm-w iMt are in.Jii»t«l by letU-i*. Table I (paru 
 1 and 2) k<vm »h« iwurc.- of the wmplfMi, and the rcm\tn of analytin. Table II make* 
 H Milection of 29 Mmplm which art- upparently genuine tfum torwfntine a» judinxl by 
 the whole reaulu of analyHiii. 
 
 In connection with tiie rPNulta here «huwn it ia important to note a« followi : 
 
 1 The pervcntnge weight of Iodine Uken up, .tpproximHtea 370 ; which namb«r 
 wan regarded a« ijrpical by Womtall (Jour. H«io. Chero. Indust., 1904, 302), 
 and corroboraU-d by mytelf (J.H.C.I. XXVI) the Hubl tolution Ix-inji 
 employed. 
 
 2. The undiw(olve<l (un|K»lymerij*d) residue, on treatment of 10 ce with 40 cc, of 
 
 a Rulphuric acid containing 20 per cent of the fuming acid, neldoni exceeds 
 10 per c«'nt of the xainplu. 
 
 3. The refractive index of thii rcHidue liea b«'twt-ti 1.49SO and 1.5000 ; read at 
 
 4. The refractive index of the tampld ix aliout 1.4700 at 20 C. 
 
 5. ThfHp< tic gravity (13.50.) i» about 0.870. 
 
 6. The initi.il lioilin){ p«)int in not lower than 160°C. under ordinary preMur« ; and 
 
 the greater part (at leaat 73 per cent volume) diitiis below 160 C. 
 
 7. The middle fraction of 50 per cent volume, distiU between 156° and 159'C., in 
 
 iiiiMt iamples. 
 M. Ninety per cent by volume distiU Iwlow 165" C. in most Mmplea. 
 
 9. The refractive index of the second fraction of 25 per cent volume, i« between 
 
 1.46N') and 1.4700 ; and that of the third fraction of 25 percent in practi- 
 (illy 1.4700. "^ *^ 
 
 10. The flanh point lies between 310. and 34'C. 
 
 Table III contains the reHult'i of examination of nine (9) Hamples, furnished by 
 variouH intereNted parties, and suspected, for one reason or another, to be surrogate. 
 It IS unfortunate th»it very small quantities were supplied in most caM*, hence the 
 recor.1 is less complete than could be wished. So far as it goes, it may be noted, in 
 contrast to the g. neral conclusions reached for genuine lur^wntine, that. (1) the Iodine 
 nuinlK-r H decidedly below 370 ; (2) the unpolymerized residue in the ^i.st 7 sample* 
 fail>, within the limit for turpentine, while in I it K, the residue exceeds 40 per cent 
 (.5) The lefruotive index for the first 7 samples, falls within the limiU for turpentine, 
 Willie simples 1. 1 K, .show a much lower refraction. (4) The same holds true of the 
 refraction of the samj)le itself. (5) The specific gravity of the first 5 samples is indistin- 
 >;uiMhablo from that of turpentine ; for samples F .t G it is quite too hiKh ; and for K 
 It IS almoimally low. (t!) Initial boiling point and teraper*tuie for distillation of 
 I'ViJ '^!' '"''"^*''' " viiriat on from true turpentine especially notable in samples 
 1 A K. (( ) The limits of t«'nii>erature for distillation of middle fraction of 50 p c are 
 pronounce<llv different from those for genuine turpentine. (8) Limit temtierature for 
 JO per cent distillate is too high. {'.» The flash point does not serve to distinguish 
 troni genuine turpentine. 
 
 This study, interpreted in the light of our knowledge of wood-turpentine and of 
 petroleum, justifies the conclusions that the first seven .lainn'e.-. in this table (A to O) 
 are e,s.sentmlly wo<xl turpentines; while samples I Sc K, are mixtures containing con- 
 suleuihle amounts of petroleums. 
 
 Tins rejM.rt shows that a considerable amount of adulterated turpentine is found 
 on the market in Canada. The adulteration chieHy consists in additions of petn.leum 
 tractions ; but, in some instance'^ it is due to substitution bv, or addition of wood 
 turpentine. 
 
 W.Hxl turpentine is apparently more closely related to turpentine than are petro- 
 leums. It IS claimed that certain substitutes for turpentine have etjuai value with the 
 genuine article, for use in the arts. With this aspect of the question, we have nothing 
 to .lo. It IS the duty of this Dep.irtment to recniire that nothing else thon true turpen- 
 
•a Uullotia No. 211. I beg to recommend iu pablimtion 
 
 I lidve the honour to [tf, nir 
 
 Your obedient nervant, 
 
 McGILL, 
 C\U/ Anoint, 
 
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 'J E 
 
 as! I . •? 
 
 2 ' - fc- .§ 
 
 5 I i ■# 
 
 a. .Us 
 
 •s C ^ 
 
 *• - = 
 
 I X . J3 
 
 ( 1 
 
 IS 
 
 » 
 
 miwo 
 
 5 1 -yinu""? I , -. 
 
 S i S < - a: 
 
 -- - - ^ <; 
 
 S S S 5 (f^ 1^ 
 
 <-2 
 _ a 
 
 Midiimy ji) '"X 
 
 •uoilMll'O J" •'>«a 
 
 O O '-" ^ irt 
 
 Z 5 -# S I- 
 
 - X ■> 
 
 pi 
 
 i 
 
 s- 
 
 
 a: 
 
 : 
 
 < 
 
 
 ■• 
 
 
 •< 
 
 ts 
 
 o s 
 
 ^ : J "• 2 ^ •=• ij 
 
 ^,5 5 t a V = » 
 
 £ > 
 
 H, a s 
 
 - ? s 
 
 ^ = F- 
 
 a: ^ IS 
 
 
 - ■ i = t ? i 
 
 Si « -a S >- i •. 
 
 ^ ?. 
 
 ?i ^ 
 
 ? ? ii 
 
 * 5. S 
 
 
 4r S 
 
 = » 
 
 5 ^ = 
 
 J O r- r" 
 
 r: f-: R ff 
 i i i i 
 
 t-i ►J u 
 
 5S S % 
 
13 
 
 ? 5 
 
 ?5 ? 
 
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 •: t 
 
 a: 
 
 if 
 
 13 
 
 
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 /'. 
 
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 _ = - :^ 
 
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 1 
 
 6 . 
 
 rf 5 : J 
 
 
 1 : 
 1 -^ 
 
 9 ? 
 
 ll 
 
 I v. - 
 
 I J _•=_ 
 
 
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 « i; c 
 
 1-2 ^ 
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 |0 
 
 S 
 
 e 
 
 -. : > 
 
 T. I 
 
 % 
 
 tc a 
 
 t 
 
 S *i 
 
 S .« 
 
 
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 o 
 
 a 
 
 ■S 
 
 s 
 
 u 
 
 
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 : ta 
 
 .i 
 
 O 
 
 > 
 
 Ph & 
 
 S -3 -S 
 
 
 5 < 
 
 ■O _ - 
 
 Se & te 
 
 i: a5 ^ 
 
 * * d 
 
 - . o 
 
 6 6 -x 
 
 a c 
 
 
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 « <e a'-c 
 
 S C C f -Jfc 
 
 C O O 
 
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 5S2|3<a5oawik,cS- 
 
 
 55 N N Fi S 
 
14 
 
 TABLE I, (PART II) BULL. 
 Rksults ok 
 
 Name of 
 Iiwiiectoral Umtrict. 
 
 l)\ 
 
 1'f 
 
 Nova Scotia ■ ■flOtl 
 
 ' 41'.HL' 
 41943 
 41944 
 41945 
 
 PriiiueKilwaiil Island 3>«!2(> 
 3802; 
 3m>2H 
 
 New Brunswick 3'.><i40l 
 
 31IK41 
 ;«»642' 
 ;«W43; 
 
 ;«>o2:t 
 
 3B524' 
 3lii-)2i> 
 
 ;«i.')2t> 
 
 3tK->27 
 
 I25<) 
 
 l'i->7l 
 
 1258J 
 
 1259 
 
 12liO| 
 
 404421 
 
 40413; 
 
 4()414| 
 
 '40445; 
 
 4014f! 
 
 42'.I42 
 
 42943 
 
 42944 
 
 4294.') 
 
 42'.t4li 
 
 44201 
 
 44202 
 
 44203 
 
 4420-> 
 
 4425<i 
 
 413! (9 
 
 4141NI 
 
 41497 
 
 4149M 
 
 41499 
 
 i 44731 
 
 1-44733 
 
 447;« 
 
 I 41745 
 
 i+4474S 
 
 I 42,501 
 
 I 42502. 
 
 42r-0.3 
 
 i 42504 
 
 42,505 
 
 Quebec . 
 
 St. ilviicintlie. 
 
 Moncreal . 
 
 Ottawji. 
 
 Kinp.HUm . 
 
 Toronto 
 
 Ijorion. 
 
 Windrtor . . . 
 
 1 
 
 29" 4 
 293 4 
 303 1 
 377 5! 
 
 2.51 5 
 o72'3 
 223 
 351 2 
 :«ti 9 
 3t>9 2 
 :).(5 5 
 3tW 9' 
 363 5 
 3«i3 4 
 200 7' 
 ;130 2 
 2M!P ti 
 2!)5S 
 ;a;.'rs' 
 2<H» « 
 2.5« 2 
 :V!5 (P 
 
 350 3 
 24fi 5 
 2)1 2 
 :M4 1 
 373 S 
 36.5 4 
 3iJ9 1 
 
 :w;s 9 
 
 lUUi <i 
 
 :*j<t 
 
 27l> o 
 37li >< 
 295-7 
 3tio 4 
 .W 3 
 2.50 H 
 373 2 
 •MK) 5 
 
 3.52 2 
 3K5 3 
 
 351 tj 
 2;i7 3 
 395 
 35S 1 
 3.5S 
 »i3 9 
 375 1 
 
 ;560' 1 
 393 7 
 392 1. 
 XV) 5 
 375-6 
 
 , ?. i' 
 
 h 
 
 ^a 
 
 
 
 
 
 
 
 
 'II 
 
 w 3 
 
 .l"^ 
 
 i 
 3 
 
 'a 
 
 • r 
 
 
 .IS 
 
 I 
 
 1 
 
 
 1 
 
 • d 
 
 o « 
 
 • o 
 
 ■m\7ii 
 
 46S7|1 
 -4K9t<l 
 49671 
 4643 1 
 49941 1 
 4596; 1 
 4849; 1 
 49'.Kn 
 
 4991 ;i 
 
 4«tSl 
 5(iOt; 1 
 4874 I 
 4820 1 
 4678 1 
 49<k5;1 
 •4483 1 
 46IM1 
 50<10 1 
 4524 1 
 46.521 
 49S01 
 49.521 
 46731 
 41!<1 1 
 49:«i 1 
 49971 
 4826 1 
 
 v.m 1 
 
 -4887 1 
 .5012 1 
 4695 1 
 
 - 4I»< 1 
 
 -50.0 1 
 46!i6 1 
 
 - (894 1 
 49.5(il 
 46.531 
 4984 1 
 5000 1 
 4977 1 
 4914 1 
 1977 1 
 46011 
 .5IH»0 1 
 50O8 1 
 4987 1 
 .5014 1 
 49.52 1 
 
 46681 
 4678; 
 4720 
 4719 
 4<MiO 
 4703 
 4646, 
 4»i92 
 47' p8' 
 1717 
 4686 
 4710 
 468t) 
 4ti88 
 4658 
 4714 
 4559 
 4657 
 470ti 
 4.5;5:i 
 
 -4628 
 4714 
 4731 
 46.55 
 4654 
 -••731., 
 4718i 
 
 •47(Kli 
 4702 
 4tl87 
 47o:i 
 4660 
 4(i61 
 4716 
 4t>57 
 4704 
 4714 
 46.58 
 
 ■471-11 
 4711 
 4701 
 4697 
 4715 
 4643] 
 4703 i 
 4714i 
 469ti 
 4718 
 4716 
 
 8.594 1.50 
 86;M 1,54 
 >ifa; 1.59 
 
 8746 153- 
 8576 154- 
 87101,50- 
 8d74 14S - 
 86.52 154 - 
 .s«)84 152- 
 87591 IM 
 8670 145 
 8718 154 
 8(M>3.149- 
 8(w7il45- 
 8.589 1,52- 
 
 8747 152 
 -8:«)6|110- 
 
 8.589 152- 
 .S692!,53- 
 83:19; 120 
 8<>07 1,53- 
 87;iO 154 
 8870 1.50- 
 8.579 154- 
 8576 151- 
 8674 1.52 
 8735 152- 
 8IM<3,150 
 8707 1.50- 
 81 mo 1.52- 
 8«itl 149 
 86C^ 150 
 8615 1.52 
 8ti81 1.55- 
 8595 152- 
 S706 1.55 
 87.54 152 
 8.576 1.50- 
 .8748 150- 
 .Si^i6 1.55- 
 81 " 1.5;i 
 Him 152 - 
 .S720 l.V) - 
 H,"4<2 145- 
 Ht 188 1:53 
 8705 151 
 
 8(i92 
 
 8819 1.53- 
 8681 15;i- 
 
 160160 
 KiUlOO 
 162 162 
 157 157 
 K1OI6O 
 15til5ti 
 1.58 1.W 
 1.57 157 
 l,5(i 15t) 
 157 157- 
 1,56 153- 
 
 16516.5- 
 164 164 
 164 UH 
 158 1.^>8- 
 166 im> - 
 157 1.57 - 
 
 166 1fiii- 
 1.58 158 
 
 157 157 - 
 
 158 138- 
 157 1.58 - 
 157 1.57 
 
 157 1.57 - 
 1.58 1.58- 
 164 164 
 1.58 158 
 
 154 154 - 
 161 161 - 
 
 158 158 
 152 152 - 
 ItU 163 
 
 155 1.58- 
 
 159 159 
 
 167 167 
 
 168 168 - 
 
 160 Ilio 
 1.5t; l.")6 
 
 156 1.56-^ 
 1.58 1.58- 
 
 - 1591 1.59 
 
 -l,59ll59- 
 
 -16U IIW- 
 
 -158 158- 
 
 1.58 158 - 
 
 165;165- 
 
 -l.'-rft|l.58- 
 
 -1.58 15^'.- 
 
 1,56 l,-.6 -^ 
 
 158 1.58- 
 
 158 158- 
 
 -166 16ti- 
 
 l.V) 1.55 
 -158 158- 
 
 1631 
 
 8 1 49-23 r 4702! 8698 1.52- 
 •60 14994 1 4706, 
 •7 1 4997; 1 4700 
 -65r499:!l-47<k5! 
 
 6 1 4974 1 4700; 
 
 1.56 im - 
 
 156 156 - 
 
 157 i57'- 
 155 1.55- 
 1.56 1.56- 
 1551.55- 
 1.56 1.56- 
 
 157jl57 
 l.->(l!l.-)6- 
 1.57jlu7- 
 1.56] 1.5<)- 
 15t)!l.")6 
 
 1631 
 -1621 
 
 15911 
 -1621 
 
 ....ll- 
 
 4686 
 4686 
 *W7 
 4687 
 4688 
 
 * .Small Kampli- 
 
 t .Sami'le in dirty l)ottlf and therefore not worked. 
 
15 
 
 211— TURPENTINE. 
 
 A.VALY8I8. 
 
 I 
 
 "3 
 i 
 
 Krmark§ ami U|>inion 
 
 uf th» 
 
 C'liitf Aiuklyst. 
 
 1 MOTl 47021-4T27 l-.T<io3: 
 1 46S9r4«931 ■»708 14S3ti: 
 
 1 4(i90 1-4702 1 471)71 4813 
 1 ■ .VW8 1 ■ 470O r 4713 r 4«Wi . . 
 I 4«00 1 46<»8il 4710 1 47iXi . . 
 
 1 4«!ll 1-46<»h:i 4713 1 4878 
 
 1 4ti91 1 47(H)I 1 4740 
 
 41'.l4r Contain* iietroleimi. 
 
 41842 
 
 4HH;) \V(i<k1 tiir|icntin)>. 
 
 4im4 (ipniiiiif. 
 
 411l]o Cnniains iietndeum. 
 
 38<J2*> (renuinp. 
 
 3.S027 C»ntain« iictruleum. 
 
 3H62K Doubtful. 
 
 3«i2!l (Jenuine. 
 
 38H30 .. 
 
 3!H;40;i_)<)ubt,ful. 
 
 3i»642 iJoiil.tful. 
 
 3!)ft43 
 
 3II644 Cuntaiim tietroleuro. 
 
 3(»23 Douhtfu:. 
 
 36524 Cuniains (letroleum. 
 
 3«525 
 
 3*)52f> Koiiuine. 
 
 3i>527 Ccm'ains iietnileum. 
 
 125(i 
 
 1257 (Jenuine. 
 
 125X I>oul)tful. 
 
 12")9 Contains pftmlfuni. 
 
 1261) 
 
 40442 Uoiihtfiil 
 
 40443 Ofniiin . 
 
 40444 Doiihttul. 
 
 40445 ( If inline. 
 40441! 
 
 !2!)42 Dniibtfiil. 
 42!t43 Containn jH-ti-oleiim. 
 42914 
 
 42945 fienuinp. 
 42941) Contains ix'troU-um. 
 44201 houbtful. 
 44202 
 
 442<Xi Containrt [K'troU iiiii, 
 44205 (ienuine. 
 442.")« 
 4139!) 
 41400 
 
 414S7 Doubtful. 
 4141IH Cuntainx |ietioI.'Uiii. 
 414-*9 (feniiinf. 
 41731 Doubtful. 
 44733 
 
 4473li (funiiine. 
 44745; 
 
 44748 Not workifl. 
 42.501! Doubtful 
 42502'<tenuin»'. 
 4250.3 i 
 425041 
 42.505; 
 
16 
 
 TAJILK r, (PAHT M) BULL. 
 
 
 1=1 "i|^ 
 
 3/-, is 7. t^ ^ti^ 
 
 i 
 
 •c a 
 = * 
 
 ~ r 
 
 
 MaiiituU 
 
 ''ul(r'i''V 
 
 VaiifMivt-r 
 
 \'ictoi-ia 
 
 j ;t<is;i 
 ' ;viH7i> 
 
 I :i:»H7i 
 
 ! Siwrr. 
 
 * .•l-iii:i7 
 
 j 3r>ii:;s 
 
 ! 3.-xi;«t 
 
 .■iTs.-.:*; 
 
 :t7N;V); 
 S7n.")<; 
 
 .I7«;-)T 
 
 41(171 
 41i;7.". 
 4Iil7ii 
 41(i7; 
 41c;7H 
 
 Hi 
 
 A 
 B 
 f 
 1> 
 K 
 V 
 
 (» 
 
 H 
 
 I 
 
 K 
 
 a7;t 2 
 
 ,111 I 
 
 :Ci!i 
 
 :«i! 7 
 
 ;tsii i» 
 
 ;t>« 3 
 
 .■i-.4 u 
 
 .•«)!( H^ 
 
 .•f i7 \ 
 
 2!W ti 
 
 3iW 1 
 
 272 :. 
 
 34.') 1 
 
 aw ,s 
 a;7 I 
 .r.L' CI 
 
 21l!l(l 
 2KI (P 
 3'!ll (i 
 
 i 314 4 
 317 1 
 
 3;fin 
 
 3411 1 
 21III 3 
 247 H, 
 372 5 
 2:W0i 
 211 4{ 
 
 i 
 
 !) 1 
 -,.-, 1 
 li I 
 
 a"ii 
 
 I 
 
 15 1 
 
 4 1 
 
 41113 1 
 4)IK« I 
 4!l4t< 1 
 48X4 1 
 4117 1 I 
 4!I47 I 
 5III3 I 
 5003 I 
 4tiOi) 1 
 4«)4 1 
 
 4704 
 
 4<i7K 
 WMW 
 4ti7« 
 46MH 
 
 4H0ri! 
 4702] 
 
 4ii:<i 
 
 4<>.')l 
 
 
 ^ 
 
 - :i 
 
 
 I 
 
 1 1") 1 \'X« 1 ICIHI 
 
 !'.■ I 4'.I22 1 4«9il 
 
 II.") 1 4!K)0 1 4702 
 
 W) r4!i.v.tr.-)7»-> 
 
 !• t 4W2: 1 47IM 
 
 1^ \ VX,A 1 47i>7 
 
 !I5 I 4!»3(il 170.' 
 
 «fl 1 4!t34 1 4703 
 
 10 ,1 4IIIH 1 4(il)4 
 
 ll.') 1 4IM.M 1701 
 
 2 I 4I)."KI 1 4li:)0 
 ft") 1 4!t!IO 1 J7(i3 
 
 3 3 1 4.Mk; I 4031 
 7 ;i 4ltS4 1 47<W 
 T.5 1 4!I7(; 1 4702 
 7 1 4S04 1 4r,«t) 
 i« 1 477!i I 4I)M2 
 
 2 K."i 1 4Kl."i I 4114.% 
 
 3 2 141121 1 1 4IJ.17 
 
 Hr. r4m4 1 4(;.'«i 
 
 HtWl I-)2 
 
 wiir? 1,52 
 
 WliW I. 52 
 .S720 150 
 H732 1.52 
 t*722 140 
 H(»)2 14M 
 .'<720 1.52 
 K(X5 140 
 ■H7ini.52- 
 .h."kS'1I46- 
 NW4 I."k5 
 «U'140 
 S«!U 152 
 W)7!tl.52 
 Stitil 140 
 H(m3 140 
 K54H 140 
 »«;« 145 
 H0.53 140 - 
 
 157 157 
 15,5 iai5 
 I.V)|,V) 
 1.-.5 hV) 
 l.'i«i|5(i 
 I.".*l'l.-Ki 
 1,").". 1,55 
 157 '157 
 15«:|,5ti 
 1.5«!1.5<) 
 157 157 
 1.57 1,57 
 1.5H 1.5M 
 1"^1 l."ito 
 1.55 I, ',6 
 1,52 1.52 
 1;".;5 l.Vi 
 157 157 
 1.5S l.W 
 155'l.-)6 - 
 
 i 
 
 I 
 
 Kkiiults op 
 
 i 
 
 ! 9 
 
 2 i fa 
 
 8705 
 
 WiSlI 
 NIU>4 
 8070' 
 H7WI 
 
 1I28K 
 
 157 157 
 
 1.58 1J8 
 
 iC):ir4«7!t 
 
 15«i V.*\ 
 
 15- 
 
 157 
 
 l«-.':i 4073 
 
 IN) 1,50 
 
 - 1.58 
 
 1,58 
 
 - 16011 4076 
 
 INi IttI 
 
 -158 
 
 1.58 
 
 164:1 4<)07 
 
 1.57 1.57 
 
 1.5!1 
 
 l.')!l 
 
 157 I 4076 
 
 l.V. l.')6 
 
 I.5!» 
 
 
 . . 1 4668 
 
 157 157 
 
 1")8 
 
 1.".8 
 
 168(1 4«,-)8 
 
 1.''>H 1.58 
 
 160 
 
 tlHI 
 
 167 1 4672 
 
 157 1,57 
 
 1,50 1,50 
 
 167 1 4676 
 
 1.57 157 
 
 157 157 
 
 167 1 4fi«7 
 
 161 H!l 
 
 160 170 
 
 225 1 4.584 
 
 1.57 1.57 
 
 l.">8 .. 
 
 .. . 14687 
 
 102 102 
 
 175 175- 
 
 210 1 4570 
 
 \-*\ i.-x; 
 
 1,W .... 
 
 . .. 1 46»0 
 
 1.50 1.5t!- 
 
 1,57 .... 
 
 ... 1 4674 
 
 1.54 l.'>4 
 
 !,■>« .... 
 
 ... 1 4606 
 
 158 l.W - 
 
 150 
 
 
 ... 14610 
 
 Itil 101 
 
 172 
 
 172 
 
 215 1 4570 
 
 1112 102 
 
 174 
 
 174- 
 
 220 1 4,572 
 
 167 157 
 
 150. 
 
 i5!»- 
 
 11.5 1 4602 
 
 \K> 160 160 102162 
 
 4677 
 
 8.562: 
 
 l.V) -1,57 1.57 -167 157 - 
 148 -I.5!l;15!)-lft5 16,5 
 
 1.51 -16l!l61- 164 165- 
 
 Mil! 
 
IT 
 
 6 
 A 
 
 t 
 
 ^- z 
 
 211 TURPENTINU 
 
 ANiiLraiH. 
 
 i 
 
 \ 4om\ 
 1 «mi 
 1 «>8:u 
 
 1 ' 4liMi I 
 
 1 4«!i:i 
 
 1 46!I01 
 1 46.X8 1 
 I 44iMl 
 r4«H71 
 1 46921 
 1 KUM 1 
 1 4«lf. 1 
 1 46431 
 1 461U1 
 1 46861 
 1 46&')1 
 1 46771 
 1 46481 
 1 46361' 
 1 4877 1 
 
 1 461C 
 1 4624 
 1 464(1 
 
 1 4704 1 4713 1 4786 
 I 4646 I 4ti«3 1 4776 
 1 46fi6 1 44i<.f* I 4830 
 
 Rrniarka, »nd u|jinion 
 
 •if thr 
 
 Cbirf Anuyit. 
 
 39«71 C.TOuine. 
 
 39872 
 
 39873 Doubtful. 
 
 39874 
 
 38875 
 
 SS637 Cpnuinf. 
 
 3n638 IVnibtful. 
 
 3B63» 
 
 38640 
 
 36641 (ifnuine. 
 
 378A3 ConUina petroleum. 
 
 87854 Genuinv. 
 
 378S6|Contaiiu mtruleum. 
 
 378.161 Doubtful. 
 
 37H%7if!«'miin»». 
 
 41674 Doubtful. 
 
 41675| 
 
 41676iContaiiu petrolfum, 
 
 41677 ., „ 
 
 416781 Doubtful. 
 
 Wood turpentine. 
 
 Genuine. 
 
 Containii petmleum. 
 
 .'■)02C -2 
 
 lis 
 
18 
 
 Z 
 
 is 
 » 
 
 as 
 
 •iui..,| l|.»|,^ I ti:j3iJup.i.'?:Hh'fi5;P.SfiS«?Jh'SWSH«?J«SS 
 
 I 
 
 2 
 
 sS I 
 
 lilil '>'«1V 
 Wil"l 
 
 mi "I 
 \»i "I 
 r,:i"> 
 
 I Hill '» 
 
 Mil '•> 
 I 8UI -^ 
 
 Wl_^1 
 
 I "icjl ""l-tl 
 
 , < : 
 
 ~«« •64 
 
 !-•» KlOi* 
 
 - «^ • I*' • I* abiA w iv 
 
 )M or^t-i 
 
 
 
 ^^1 
 
 T 
 
 "nir^s 
 
 ■••npi<i^}{ 
 
 n 
 
 •M ■.■8 pjg I 
 
 I 
 
 •>■' S? I'".' 1 
 
 I 
 
 •■^1 gS >»t ! 
 
 iPlli III liiii rll^lilil 
 'iiaiiiiiiliiiliipii|iiip 
 
 iiiiiiiiiiiiiiiiiiiiiiiiiie-E-i 
 
 "iiv-siiik-iiitiKiiiiiiiii-iillli 
 
 ■3^32s^ r-^££ ;sl££l£2 ; iui JsSSS 
 
 •»j(lum>; till I 
 JO x.»i)U| rf.\!iOTJj^H ; 
 
 JO x.ipui JAijoBJJsa 
 
 lIHPiHiHsliiiliMHiiiHI 
 
 •'OS 
 ' II ui ->(<inio«ui 
 
 "pfi'5£Si'y3S3¥£l 3 S ? SfeS IS S S?-S"8 S S 5 f- i 
 
 "y. 7? * 00 ?1 X ?) S OI- — •« "^ ^ M 
 
 ^^ -r X — x'ci'r:^ai«»oo»^ 
 
 
 mmmmMmmnuMmmm^\ 
 
19 
 
 'H ui J[qn|rMiii 
 M 01 "ioJJ rfn[iiiiiy 
 
 JO uopimais^ J 
 
 «i.3>s-.la!oi{12» 
 
 ■.-:•>■ — ..- — n X o T