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Les diagrammas suivants illustrent la m^thoda. 1 2 3 — 1 2 3 4 5 6 r'^'^'wmmmmm 1 ipipppiippi Ifi^i .■1 -!l ' ■ -a ' 4 I.- LABORATORY or THE INLAND REVENUE DEPARTMENT OTTAWA. CANADA BULLETIN No. 367 EDIBLE GELATIN 18646—1 NOTES AND COMMENTS. 1 Under this heading, aa occasion arise*, the Bulletins issued by this Department; will contain, as an appendix, such comment as may seem neceasaiy or advisable upooi matten relating to the woilc of the Department in connection with the administration ' of the Adulteration Act, the Fertilizers Act, the Feeding Stuffs Act or the Proprietary^ Medicines Act. It frequently bappois that correspondeuta ask information regarding the abort; Acts, of such a nature that the matter in question possesses general interest, andi comment upon it would prove acceptable and useful to others than the inmiediatci queationer. In sach cases the reply may find a place in these columns. For oon-^ Tcmienoe of reference theae notes will be numbered in leriea. A. McGILL, Chief Analyst. ' m LABORATORY OF TBI INLAND REVENUE DEPARTMENT OTTAWA, CANADA BULLETIN No. 367 'epartment lable upon inutnition 'roprietary the abore lerest, and immediate For oon- alyst. EDfflLE GELATIN J. TJ. ViHotNT, Esq. K.O., Deputy 3£ini8ter of Inland Berenue. Ottawa, SSod Karob, VH7. Bn, — I have the honour to report upon 187 f t?"? of GMatin, pnrduuwd hf am inspeoton in A^xii, May and Jane of laat y«ar. The report is arranged in thre^ parts. TaU« 1 furnishes the ordinary analjrtkal results upon 67 samplea. Table II givea resolta in greater detail vfoa fiS fMpl— ^ specially examined by Mr. M. Brot of this staff now at the front, somewhere in Tnaat. ''e in gives results for snlphnroos add only, in 2S samplea of so callsd Jelly ' V jrs. These articles are not properly described as Gelatin, ^thoni^ tlwy eontaia ,.in as an ingredient Poth edible gelatin and glue are obtained by treating the ooQageBS of Imim% iendont, cartilage, eta with boiling water. It will bo readily understood that, fnndft- mentaily. they are the same thing. The essential oharaotor of edible f^tin, aa distinguished from ghie, is its purity. Olue may be a perfectly pore article wMlumt ceasing to be glue; but edible gelatin must be a pure article; and, in ordnr to eopni* a satisfactory degree of purity, it should be requirod to meet certain q^emfied ataiuifaHcdB. The treatment which the original material reoaivaa in the iwinufantnTt of gelatin is such as to fairly well aaaure the destruction at organic impurity. But whim we consider the nature of the material available for the manufacture of glue, dead tip^'n nli of all kinds, and in various stages of decomposition, we must raoogniae the dsnn^iiKlgr of giving the consumer of gdatin a goaiantee that only aeleeted and naobjaotimule materials have been used in its production. This can only be done by efioieni iiUKpo- tion at the factory; and for this reason, the inspection of all gelatin factoriea ahooJd be undertakm by Government. So far aa Canada ia oonosniad, tiiis is tlia aamt and the Department of Agriculture, in its administration of the Meat T»ifpy « f fi fn j^ gruarantees the quality of the material used in manufacture of edible gdatin, so far aa meat packers, doing an export besiness is concenwd. I am not however awaia tbai the manufacture of gelatin is anywhere in Canada carried on biqrond the aetiud taqttte»> ments of the manufacturer in his own business. Practically cll of die g^t^ nssd fai Jelly Powder manufacture^ in iosHveam, etc. is of foreign manufacture. Tlw D epartBMmt of Cnatoiu hua kindly fumialMd me with the f oDowinc ttetiatioi oonoernfaif the importation of gelatin and tiinglaM (fiah gelatin) for the fiaoal nar ending Slat March. 1916. '^ United Kingdom ITO.ITS $43,397 Hiina 41 g J^«"» 18,118 8,807 Holland 8,981 460 J«P«» 10,880 8,670 Switierland 18,888 9,684 United Sutea 846,116 »1,08« Total 46431S 1146,891 Gelatin ia thua d^^ned by the Britiah PhramaoopoMa. iwiaion of 1914; "la the air-dried product obtained by the action of boiling water on animal tiaaucs. auoh aa akin, tendona, ligaments and bonea. Characien and TeiU.— In almost oolourlesa, translucent aheeto or shreds. Inaohible in alcohol (90 per cent) and in ether: soluble in acetic acid. A solution in hot water (1 in 60) ia inodotoua, and solidifies to a jelly on cooling. An aqueoua aolution yieMi • iw*cipitate with solution of tannic acid, but not with solutiona of other adds, or with dilute aolution of alum, solution of lead acetate, or test solution of ferric chloride. Ash not more than 2 per cent." Gelatin finds extensive uses in the arts, and most of its applications require the article to possess a high degree of purity. The definition above quoted haa primal/ regard to its employment in medicine, where it is used in the manufacture of capaoles and otherwise. It is, however, with its use aa a food material that we are immediately concerned. Aa a food, gelatin enters into the manufacture of so-called jelly powders, in jellied meata, aa a sti£Fener in ice cream, etc. Investigatory work. Having for its object the fixing of definite distinction between edible gelatin and glue, as used in the arts, has for a considerable time been carried on by the Department of Agriculture at Washington. I am not informed of the completion of the work referred to, but by correspondence I learn that the most important characters consid«-red to establish the distinction are odour, turbidity, jelly strength, fat and aah. Colour is of necessity, a matter of importance, although the bright colours given by coal-tar dyes to most jelly powders, reduce its importance so far as these are con- cerned. Where select materials are employed in the manufacture, it should not be necessary to use bleaching agents to give edible gelatin desirable lightness of colour. Our standards require that sulphur dioxide (sulphurous acid) shall not be present in solid foods above 1 part in 2,000 parts (60 parts per 100,000). This limit is exceeded in 11 samples of Table I and in 10 samples of Table 11. Traces only of sulphurous acid are found in the jelly powders enumerated in Table m. A«A,— The British Pharmacopoeia fixes 2 per cent, aa the ash limit in gelatin. This limit is exceeded in 27 samples of Table I, and in 10 samples of Table 11. Odour. — This is observed by soaking in cold wat«r for 4 hours and then i?ifi l H"g into a jelly by heating with water. 0' ^d samples yield no offensive odour. Thirteen samples of Table I and 14 samples ot Table 11 gave more or leas unpleaaant odour when thus treated. Of this number 6 samples were decidedly objectionable, and ahould undoubtedly be classed as glue. TurHditv of • M par oMit, tolution wm obMrmd ia tlM MnplM amnfed in ruble II. Of the total number (09 Mmplea) IS uunptet gare more or leat diadnot turbidity; in 9 of them the turbidity waa yery marked. Viteoniy.—ThiB may be determined by the method of flow, wUdi hov et we Imve found to be Tery unaatiafaotory and aubiect to large experimental error. D«ter- minationa aa recorded in Table 11 were made on S6 per cent, aolntiona at M* 0. In >\ general way the rcaulu ouiroborated those aicerUined by the uae of the DooUttle Viicosimeter, bat theae laat are much mora truatworthy and dnplioataa in eloae agree- tiii-nt are eaaily obtained. The inatrumeiit ia standardixed in terma of augar aolutiona made aa per inatmo- tMinit accompanying it. We have not yet been able to formulate ipccifio atandarda for gelatin, but it ia li' '|)ed that this may be done in the near future, and the information fumiahed herewith ^^■ill bo helpful to this end. I would reapectfnlly advise publication of thia rvport aa liulletin No. 8«7. I have the honour to be. Sir, Your obedient aerraat, A. IfoGILL, 18645-2 ^ BULLETIN No. 867- •m , N»tun fhmpi*. ! i •A Nanw nnd Addreu ••( Vowlur. Cut. Nrnnr and AdilrcM o( Munufaclurar (« FurninhM M irii'm bji Ihv Vndur. In<|)•otor^i J •3 1 i llMiuf*uti>r*r. ruraUlHT. R»|nrt. (ta nut Ml U|>muuin(i u|>iiuofi. ) DIHTKICT OK NOVA MCOTIA 191& (ieUtine. . MSHl Muir'i, Ltd., lUliUx. KnUt.- 1 » .. 46 50 Unknown .... M. Michu-I k 8i> n, N f> w York. J. M. I>oi»l» ft Co.. Mun. tmU Mfr 8hwn, P.E.I. .lenkini ft Son, Char- lottctown, P.E.I. J. H. Myrick ft Ca, Tisni«h, P.KI. •Hpkga •i .. 3 M 3 M 3 .. I lb. Spkg* 3 .. 3 .. S .. ChariM h. Kaox ft Co., MoB' treat J. A O. Cox, EdinburRb, 8ootland. Chui. 11. Knox ft Co., .Montreal J. ft O. Cox, Edinburgh, Scotland. W P. Uownoy, Montrral. Chaa. U. Knox, MontiraL MoLarrn'a, Ltd., Hamilton. J. ft (). Cox, Edinburgh, ScotUnd. Chu. B. Knox, Montreal. Knox. « i Oox 1 Knox. Cox... Knox. i McLann'i.^ Cox J Knox. DISTRICT OF NEW BKUNSWICK- May 3 5 5 .. Ifl .. IB Gelatine 69402 6»t03 60404 60406 .1. L Davia ft Son, St. .John, N.B. M. K Gnwa, St. .John, N.B. H. L. Alitxander, St. Tohn, N.B. A. E. Trentowaky, at. John. N.B. M. K Graw, St. John, N.R Spkga 8 .. 3 „ 3 .. I lb. .1. ft G. Cox, Edinburgh, Scotland. Chaa. B. Knox Co., Montreal. •I. ft G. Cox, Edinburgh, Scotland. Chas. B. Knox Co., Montreal. Coignet, P^ ft Fila ft Cie, Pari*, France. Cox... Knox.. Cox... Kiiox. (lELATIN— TABLE I. KatulU irf Ankljraiii. ■s ill Oduur ul \% Hiilutkin. Aftrr Aftrr 4 bcHirm. Sdajri. Rnwtioa with I Phylnl ChwMMrbtioik Litmiu. Alum i CuliHir. Muti.M. Tt»nrf- lamiojr. t 1 i I i K J. WAUUH, INHI'KOTOR. |>.C. .IIW »' + Uliwy. Very ucy. Nwitnl. I'M IS + Normal. N. rni»l. Buio. Iterk brown. Y-II..W. Uh brnwn. CiMr. Brok>n •hi«tii. 8hn«l- dwi. A. J. I,. 54381 U9«j lOHX C. FKROITSO!*, ACTING IN8PK0TOR. I'» 1 M 1 00 1 5« 2 03 2 Ot5 1 M 1 60 2 34 M II BA 47 NormiU. (Jluajr. Nurnul. SliKfatly »lu#y. Normal BlighUy gluey. Normal. Nurmal. Badly dreoin- powd. Normal. Slightly gliwy. Normal. Slightly gluey, Aoid. Neutral Aoid. Normal I Veik . ill. tint I tear. Powder A.J. u 00451 Shred- ded. •• 69403 Powder. .< •»45t M " 89405 '• " (»4M Leaf. •• 60407 Powder. .. 60406 " " 60400 " " 60460 n " 60101 KHIN C. FERGUSON. INSPKCTOB. 2 29 1 38 2 10 1 14 52 8 11 5 V Normal Normal. Aoid. 18646— 2 J Oolonr- leie. Clear. Powder. Leaf. A.J. L. 60401 KB403 00403 69404 69400 BULLETIN No- 36:— ll ill ^ 1 ■ Natom of i. Sample. S 4 •5 1 0! •s i.1 Name and Addteu ol Vendor. Cost. I Xamo and Addraiw of Manafacturer or Kurnuher as given by the Vendor. Manufacturer. Furniaher. Inspeotor'i Ii«|iort. (U not an expreMion of opinum.) DISTRICT OF NEW BRUNSWICK- 1916. May 2S " 26 II 26 June 6 Gelatine 69406 G»407 C. H. Bunt, Frederic too, N.B. WatMm & Trice, Woodstock, N.B. G9W8^Yerxa Grocery Ca, Woodatock, N.B. 6!*40HMill Eveleigh Ca, Ltd., Sunex, N.a 69410 H.T.Brewster. Munc ton, N.B. 3p!tK» 3 „ 3 .. 3 » S „ McLarem I m perial Cheeae Co., Toronto. Pitre «oid Mfv Co., Ltd., Trti ronto. Litater Pnr« Food • Co., Ltd., Toronto. Chu. B. Knox Co , Montreal. ■1. * O. Oix, Kdinburgh, ScotlanH. McLaren'i. Pure Gdd. Litater'i... Knox Cox DISTRICT OF CjUEBEC CITY- 16 May 15 Gelatine. ., 1.'. .. IC 6C761 iS6762 667U 56756 I F. LfUiKloia, 1176 St Valier »t., Quebec. J. N. Rmdeau, 6 Lachevrotiere, Que boc. Sboit* .3 ,. 3 pki 3 ,. Unknown Cox Unknown Knox N. Turjotta 1. B. Renaud. Lady Char- lotte. Cox Lady Char- lotte. Knox. . ... DISTRICT OF QUEBEC PROVINCE- &Uy 1 Gelatine. | 4905 M ' 4986 Kobin Jone?, Paiipe- biac, P.Q. Ferdinand Laudry, Caileton, P.Q. 3 pkn. Georgie Mi 111, EdinburRh. Cox. .DISTRICT OF MANITOBA - April 2^ (relative May ™l » 2)1 .. 3l> .. 30 II 30 I. 30 71809 7184!) nsyo 7lb51 718S2 71853 71894 Swift Cii„(C»nttliaii) KUnwuud, Ont. KobiiiHon & Co., Main Ht., Winniiieg. TheT.EatiniCu.,WiD- nijieg. Crtwient Cnmnery Co., Bunnell it., Winni|ieg. MoLaren'n, Ltd., \V iiiitipiig. Gordon IronHideg k Fari'8, Logan ave., WinuiiM^. Hudnon'x Bay Ca, Winniiwg. 1 lb. 1 .1 1 I. 1 ., 1 „ 1 .. 1 M Peabody Co., The Gelatine Agent Co. Francr. French Co Vendom . . . Unknown . F. H. Wyley, Winni|)og. Blade in SwitKiland. (iELATIN— TABLE I. Remit* of Analjrti*. 3 ■aas Odour of 5% Solution. After 4 honra. After 2 days. Reaction with. Litmuii. Alum Solution Physical Characteriatioa. Colour. Trana- parancy Agpre gation. t 1 i i\ 3 Cunclvdei. p.C. 22* Trace. + Xomial. Normal. Aoid. - Powder. A.J.L. i;»4a6 1 76 3S + 69407 046 19 + ..- " .. - u •1 69406 1 23 + It >• H Powder. 6940* 1 86 .... " It " " " 60410 F. X. W. E. BELAND, INSPECTOR. 1 SO 2 46 \'\ 1 10 Normal. SliKhtly sluey. NomiaL Normal WiffaUy gluey. NormaL Neutral. Acid. NeatraL Acid. A. PELLETIKR, TEMPORARY INSPECTOR. a 44 »'04 40 Slightly fluey. Normal. Sligfady NormaL Neutral Acid. Red. Shrad- ded. Powder. Shred- ded. Ftnrder. A.J.L. 80761 067B3 66706 66756 Mired- ded. A.J.L. 4966 4986 I. B. COSQROVE, INSPECTOR. 1 54 128 11 6 Po.- itive. NormaL Neutoal. 11 Neg- ative. White. Yellow white. Powder. Sbeeta. E.L.C.F 71809 7I84» 208 77 " » » JSvown* iah white. Yellow white. , II 71860 »00 16 ti H Aflid. •• Powder " 71fl61 2 10 44 1« " >. Nmtnl. M It M White. „ M 71861 7U6I 1 ii M 1 W 77 •■ II It II Btown- iih white. Sbaeti. tt 71864 10 BULLETIN No. 367— Nature to "a. of Sample ^ o d '< Name and Addrma of Vtndor. Ckwt. i I f Name and Addren of Manufacturer or Fumither an given by the Vendor. Manufacturer. Fumiaher. InHpector'a Report. (!• not an exprensionof opinion.) DISTKICT OF ALBKRTA- 19Ui. May 30 ( .June 13 13 14 15 IS 15 15 15 Gelatine 62427 5343-> 5242!) 52430 52131 6213.> 52133 52434 52435 52436 'O. W. Buck, High River. > Carlisle Dairy Co., Calgary. I HudsonV Bay Co., Calgary. Ilochon'a, Ltd., Cal- gary. I Campbell k Griftin, Ltd., Calgary. '. Tuxedo C.ffee & Spice Mills, Ltd., Calgary. IL.T.Mewburn*Co., Calgary. Ltd., Louis Petrie, Calgary. Jamee Findlav Drug Co. 6 or... I lb 1 I I 1 1 1 I 30 55 90 55 66 1.00 80 90 75 1.26 Coignt-tPAreKiU ft Co. Ht'ghea Gelatine *Co.,Chie'ago. Siniington ft Co., Calgary. F. W. Wiley, Winnijjeg. Imperial FiXtract Co., Toronto. T. H. Wiley, Winiii|ieg. J. A G. Cox, Edinburgh, Slot. Chas. B. Knox Co., Montreal. Tellier ft Koth well ft Co., Montreal. Grouud . . Made in Swit^erlan.i Ground . Powdered. . Instant PoW' dered. Sparkling . Made in Switxerlaud. DI.STRICT OF ROCKY MOUNTAINS- lli'til May 5 6 Gelatine.. 68217 68219 F. H. .lacks. >n, Cres ton. Cmston Mercantile Co., Creston. 3 pks. 3 .. 45 46 .1. ft a. Co». Edinburgh. C. B. Knox ft Co., Montreal. ■■ 5 '- DISTRICT OF VANCOUVER- June 26 .. 26 Gelatine . 27 56622 Empress Mfg., Co.. Ltd., 1106 Homer St., Vancouver. 6562.5 Mmmey Biscuit A Candy Co., Homer ft Drake Sts., Van 55626 556S7 5.5828 KhIIv f5nnfnrtinn»»r Co., 1106 .Mainland St., Vancouver. Nelson, Shakespeare, Watkins Co., 136 Water St., Van- couver. 1 lb. 1 ., I „ t .. 60 Tellier, Rothwell ft Co., Mont real. W. A. .lames, 318 Homer St Vancouver. 40 56 fin 45 Patten, McKen- xie ft Co . , Yokahama, •Tapan. ITnknown. W. A. .Tames. .HIS Homer St., Vancouver. Sold as .Tap- ■neee Gela- tine. 11 GELATIN— TABLE L ReaulW of Aiulyris. 3 Odour of 6% Solution. After 4 faoura. After 2 d»y«. Reaction with. Litmua. 6% Alum Solution Phyaical Characterittic*. Colour. Trans- parency. Agfrw- gation. -a A. W. R. MARKLEY, INSPECTOR.- i is i's 1 11.0. 92 rca 2 12 2 !M 1 fiO 1 80 24 1 .52 2 18 2-22 60 27 82 5 33 11 S3 16 22 1 43 Poui- tire. Normal Faint. Normal. Neutral. Acid, Neutral Nega- tive. Red. Light brown. Mica coloured Light brown. White. Light brown. Mica coloured Clear. Clear. Clear. Sheet*. Powder. Sheet!. Powder. SheeU. W.A.D, 53437 62438 53429 634S0 82431 S34S2 S24S3 62434 63436 63436 TH03. PARKER, INSPECTOR. 306 1 50 49 8 Normal. Normal. Acid. Kega. tive. White. Clear. Powder. J.A.D. 68317 68219 I E. .T. MORGAN, INSPECTOR. 2-95 60 Gluey. Gluey. Acid. Nega. tive Yellow white. ' . ran*- lucent. Powder. J.A.D. 50683 3-65 76 " •■ " " Amber. II Grain*. " S0OS5 4 16 None. None. Alka tl White. " Sheet*. of Analyaig. i a 6 Remaiks and Opinion of the Chief Anal>«t. V CADIKITX AND T. OENDRKAU, TKMHORARY INSPECTORS. .Swfet . <»ood , Ve Very rood. Clear . Very clear. :o 7 73 6 78 7 Soft hard. Hard. 1 30 1-78 1 24 109 None M. B 398 670U 73209 T. J. COSTIGAX, INSPECTOR. Ciwd . , (;iuey . Clear... Turbid . 23 18 2u 26 23 21) ffi- Soft hard. Soft,.,. 1-90 1 70 80 82 .M. B. 678»/) 67881 V^erv good. Clear,.. 27 20 30 71 6 Ha>d .. 1 18 19 H 67862 ( I w)d . . 24 6 34 27 70-2 Soft hard. 1 74 13 " 67883 1»H. V, P. LAVALLEE, INSPECTOR, 'umiiih«r, as given hy the Vendor. Mannfacturer. Fumiaher. Inapector'i Keport. ( In n. A. RICKEY, INSPECTOR. i^xid... Clear. . . 3fi 27 28 70 7 Hard. 1 12 13 M.B. 73141 A< rid . . Turhid.. 21 19 20 66. Soft hard. 2to 18 " 73142 Bad. Shpf py , Clear . 27 40 32 726 Hard.. 1 22 13 „ 73503 ■^wert . Turbid.. 19 27 20 69 Soft... 1 70 32 „ 73604 iJfHid . . Clenr. . . 26 2S 32 72-5 Hani.. 2 38 32 •• 7SS06 A. RICKEY, ACTING INSPECTOR. i;i)od. . Clear... 21 3t 24 69 25 32 32 725 (Hwd I'litacrid Sweet . . .. . . 28 20 29 21 31 21 72 668 Soft hjird Hard.. Soft hard. 08 2 14 1 16 1 80 32 13 13 32 M.B. 73157 78163 73166 73170 18 BULLETIN No. 367- S I C Natiim of Samiilc 6 V. Nikme kntl Addre'i o( Wndor. Cent. Naniv and Aildma uf MftnufactuiM or Kuniiahf-ru iciv«n liy tin" Vendor. ■t 14 Manufacturer, i Fumiabrr. Ini>|iector*i Ke|H)rt (In not an MxprHfliium of iitMniun). UISTIUOT OK TOKONTO- laHi. May 2 (lelatint; 727«H 727t«» 72770 72772 72n8 72774 72775 72776 72777 72778 72779 72780 727SI 72782 72783 Swift Ciinadinn Cu. We«t Toronto. (iiinna Ltd., Wnt Toronto . .McLaren > Iiniierial Cheeae Co. Toront*) Thf BowpK Co., Ltd., 711 Kront street, E. Toronto. I lb. R. B Hayhoe&Co 4i Colbome atreet, Toronto. The T. Baton Co., Ltd., Yonpe and ijiipen HtK. , Tortjiiti Matthews Lainc Ltd. liathurnt and Kront ■treeta, Toronto. McLan-n'a Inirieriiil CheeaeCo. , 8f» Front atreet, E. Toronto. Rnffer a '">., 268 Pape ai • ' oninto. Imperial Kxtract Co. to Matilda atreet, Toronto. Wm. Ncilson, Ltd., ^>J liladatune ave., Toronto. Pure Go;d Mfg. Ca. Ltd., 381 College at Toronto. Liater Pure Food Co., 12'.>7 Queen at , W. Toronto. The White hwan.S. ft C. Ltd.. LV. Pearl atreet, Toronto. Kaaex Itt'lntint Co. Iloaton, II H..V. Ven'lora McLaren* Ltd. Hamilton. 10 Venilora 60 fK) Unknown Vendor Unknown. . Canada Glue Co., Itrant. foni. Tellier Roth- well,M ■•»l'l""»f< J" '••K 'i I ■aonoj,,.)0 JO i^»ti o a. 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