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Sir, — I have the honour to submit herewith a report upon eighty-two sampl i purchased as Arsenate of Lead in June, .July and August of last year. Consequent upon many complaints regarding the character of this article as offereii on the Canadian markets, a collection of 26 samples was made in 1910 (see Bulletin No. 206). Upon the work then done, and further study of the subject, the following standards were recommended and are incorporated into tlie fourth schedule to the Adulteration Act, l)y an amendment dated June 6 1913. Arsenatk of Lead. — 1. An insecticide, containing at least 48 per cent of its weight of of solids as a residue when dried to constant weight on the steam bath ; and these solids must essentially consist of the pentoxide of arsenic in combination with the monoxide of lead. Water-soluble arsenic (expressed as the tri-oxide of arsenic) must not be present to more than one per cent of the weight of the in.secticide as sold. 2. Arsenate of lead shall lie regarded as adulterated if any substance has lx?en mixed or packed with it so as to reduce, lower or injuriously affect its quality or strength. The results obtained by analysis of the S2 samples now reported must be judged in accordance with the legal standards quoted. The great majority of these samples are sold in the form of a paste, this being the form in which the article is most readily available for use as a spray. In order that the article may not dry out on the shelves of the dealer, it is usually put up in glass or tin con- tainers, and hermetically sealed. Forty-one (41) samples of tliiscollection were furnished to the analyst in the original container, and these are specified in the table. The remainder were furnished in glass bottles or in tins which had been filled by our inspec- tors from the larger packages of the dealer. Owing to the great difiiculty of sampling a paste of this kind, some uncertainty attaches to the determination of the water content 11 these cases ; and where the conUinern used by our tors have been imperfectly ,:l,>-f Vend'ir. N'aiim itnil Addmw uf Manufacturer or Furnisher »» niv.'n by the Venilor. 1 ^ S B Manufacturer. Kurnisher. DISTRICT OK NOVA SCOTIA 1913. ! I July SjAraenateof I Lead. 15! 16| l(i' 17 17 'J 28i M112 N'iiti.mHl DruK Co.. .'til » j llalifi.x, N.S. 54143j.I. A. Craig, Yarmouth, 3 ■ I N.S. 1 54miT. 1,. H..rv.v, Wolf li , I ville, N.S. ' ■ 54) 45:\V. W. K.«:kwell.Kent 3 . i ville. N.S. 5IUr, Wilcox liroH., Wind 14 J f^ttr, N .s. j 54147, !•'. H. .\I,innin(f, Fal-lu ., mouth, X..S. j SlllSiHalifax .S.«l Co., HuU-:3 .. fax, N.S. ! .-.4HlliK. (i. Mo.\on, Triu. , 1 ., N.S. .M15tl'(i. .1. Kiiihy, Lunen- 3 ., i hurK, N.S. I ■'ill51 Hrown lirns., Halifax, 3 .. : N.,s, «>5 Unknown . Canada Taint Co., Montreal. I Nil Vemlor . N. D. ft C. Co. Montreal. Canadian lir.:g Co. , kSt. John, N.B. I i 2(1 Corona Chini. Co., Newwark, N .1. Canada I'aint Co., Montreal. M*'rrimac Cliein.Ctj., ; lioston. .May A Kaker. Lon- don, Kng. Oheuiical LalH>ritie», 75 7.5 Ltd. Manufacturers. Capt. Allun.Kent- ville, NS. K. B. Sutcliffe, Halifax, N S. N. I). & C. Co., Halifax, N.S. N. 1). & C. Co., Halifax. I DISTRICT (»F NEW BKUNSWICK- .fune July I., 60652 The Nat. Dru>,'&Chpm.'31l».. I Co., Ltd., St. John, N.U. 5lHa3W. H, Thoine f;o.,!3 „ I Ltd., St. John, N.B. 50«54il'. Naw & Son, St. 3 .. John. N . H. mWThi- (':in.vlian Drug, 3 „ ! Co., Ltil., St. John,i • I N.B. I r>()ti5li!.r. .S. N.'ill & Son,i3 ,, I'rederictjm. N . IS. ")0fU)7 K. H .Maik, St. .John, 3 N B. 506.W Wade Urui? Co., Perth, N B. rMW.> Dicki».)n & Troy, New- ciwtle, N.B. .'kifiliOl.L 1). B. F. Mackenzie, Chatham, N.B. !Dow Chem. Co., Midland, Mich. The (iraNHelli Chem, Co., Cleveland, Ohio. The Canada Paini ' Co., Ltd., Monti eal The Canada Paint Co., Montreal. .S h e r w i n - Williams Co., Ltd., Montreal The Nat. Drug & Chem. O)., Ltd., St. John, N.B. Nat. I )niB&Chem. Co., Ltd., St. John, N.B. LIOAI) ARSKNATE. t Reaulta n( Analyaia. Kf'Xi lUcu fui;4tMl (in thuiry I'ercentaifc 1 c Rainiil^. Wriifhtii in Original Sample. i Roma'ka and Opinion rii.|»-ct.>r'iil{<'|>ort. s. 3 s IS i ij {"^ ^ 9 ||. 11 .t un fX(in-»- .1 III (if 0|iini(m. 3 1 1 4 it 5 .a o 5 1 ll 4. 1 •s d of tbo Chirf Analyst rfi e. fi i^ j> i& > -< Ji ■< a K .1 WAIGH, INSl'ECTOK. p.C. : 1 ^ 1 !>. c. p. r. 'p. c.lp. c. p. cJp.c. P.C. ] .c. ! 4127 28 76 60 5!t 1 5 12010 1'3H ' 1 i 16 87 30 11 No. 64142 8« IB 27 31 1 71 (WJ lo'o.iao 38 S3 17 « 46 88 Yen. 54143 44 4H ' 1 '. »i 111 m -AH fioii-720 724M1 Ifi 75 35 75 No. 54144 I.,,l..ll.-ll'<.W(ilT«l \ 1 liunntf of Ijt'ud U-2II 2SIW 31 (i2 05 30i 50 12 018 30 1 ! 30 1»| «7 14 200 1211 18 1 70 1. 21 71 ' No. 48 21)' No. 54145 54146 l.al.llrd Swiffi. Ar>inattMif Li-ad 35 M 8 2 11 1 1 25 88! 6H M, 2 31 !«• Gl'iti 15 II 1211 18 1 70 1 ! 0120 001 88 18-53 44 70j No. i Y«,. 54147 54148 .54149 Tin container ■\ „„.,•• linmd.. 12 1 001-38 r 18 34 1 36-21 Yto. ru>ted through ,. 45 05 2«"5 0'408 15 12 18 1 20 1 16 80 37-0O Yp». 54150 44 M 31 07 W 22i 2 24 n ()0l 70 17-25 36 75 No. 54151 I' KERliUSON, INSPECTOK. 4!l 10 31 H2| 65-49 1 00 24 43-65 47 05 •|»i'iilly prt-iiand' 43-64 I"!- c. 1). Co.,; i.t.i. ' 47 -80 ' \ :inco " Brand . . I 4470 27 311 69 110 I 00 24 25 88| 71-92 1-5012 I 25 15! 72 11, 2 0,0- 12 i I 2:) Oo 72 60 3 00 12 I 27 31 69 13 1 0,0 12 N' iitral Arsenate: 47 06 25 8S 71 00! s 5048 nl 1,,-ud. ! ; i'i.,l,ict of Canada: 39 65: 2! 37 88! 15-11! 38 1 I 661 13 47 36 38 16 22 41 43 :*i Y«t. 50652 39 Yes. 50653 08 Ye,. 50654 64 Ye». 50656 86 Yes. 50656 23 Yen. 60657 95 No. r>0658 25 Yes. i 50669 61 No. 60660 t' i i BULLETIN No. H84- Name m»I A>Mrew of Mannf*ctur<>r C, GO Unknown ..I 3:o7«L. K. Mattel. .M Rue J lb.. ' .St. '^wwiih, t^u**!!*^. I 37077 J. K. i.HiTnui.H, Cimil- 3 llw. ' l»rJ, St. .Ii'an. ! I :t7"7tt Dr. Kil M.irin. 113 3 ., J. K. liivernois, 4aCaiia. .t C. Co. I Montreal. .30 .. .. . DISTRICT OF KA.STKRN TOWNSHIPS- July 28 Arsenate of Lead. 1645|H. Neven, St. Ctnaire 3 box'» 1 i l.20iThe Canada IVint 1 Co., Ltd., Men- 1 tri'al. » 30 IWfiP. H. HeWrt, St. 1 jar. Hilairt>. 75 The SherwinWil. liaiiiH Co., Ltd., Montn-al. DISTRICT OF MONTREAL - June 24 Arsenate of Lead. ,. 24 1. 2»i Aug. 21 1 .. 22 >. 22^ ,. 27 .. 28 58701 58702 mm 58704 587(e 5870ti 58707 58708 iioHton. 1.05 Canuila Paint Co . l..->0The Grasselli Co., Ltd., Hamilton, Ont 75 Vendors Dupuy 4 Frrgiiwiii, 3 pK9.ll.05 MerriuiacChem. Co., .Jac(iue(*Square, Mon- treal. H. L. Dery, 21 Nutre 3 „ . . Uaineeast, Mmtreal. Wm. Rennie A Co., 3 •. . . Ltd., lOitMciJillSt., Montreal. The Canada Paint Co., 3 lbs. Willian. St., -Mou tre i. \at. Liru^ & Chein. 3 i, . , Co., ;)4 St. (Jabriel St., Montreal. The Lyman Knox Co. , 3 .i . 374 .St. Paul .St., Montreal. Lynianx, Ltd., 474 St. 3 ,. . , Paul St.. .Montreal. The Dr. Leduo Dni>; 3 ,i . Co., Chaboillez Square, Montreal. I Dow Chem. Co., Midland, Mich. Dow Chem. Co., Midland, Mich. Nat. Drug & Chem. Co. [,KAU ARSENATE. Iti-l'K'iiir'aKeiKirt. (In not Ml t MAitm ti( >|iinion). liiiin KMulta of An»lT>i*. a i I KvtulU CftleuUu^d na the Dry 8*in|>lr. i i 1 'i I i=3 ^ 'jt a j2 * # ,!S ,# PrroenUfe W .fihtii m 1 I 1 ^ RanatK9 •od Opinioo ii( thfi Chi«f Analyst. F. X. W. E. BKLAND, INSPECTOK. p.0. 0-40 .V)Oi) 1.-) 41 12 P.C. ■ , 31 |>. 0. I p.0. p.0. ' p.c. I p.0. 70 8?! 1 "0 240000 78 27 .•» 71 liO 1 f)0 1203<1 25 HX 72 «!l to 27 31 1 02 12 IM.O 70 71 (K'l 100 120 IWO 70 I ! ' ! p. C. 13 65 16 OH p 0. 36 5u 41 9(1 No. No. No. Ym. S7W5 37076 3707' 37018 Tin opnt»inet runted through. 11. V. V LAVALLEK. INSPECTOR. 29 12 15 28 03 30 19 65 49 60 96 1 00 12 I 1 0iO36 18 70] I 18 48 i; 73 46-39I Ni, No. 5^6; 58958 I f. ROULEAU, INSPECTOR, 40 35 I 46 112 27 31; 71 00 25 88 72 11 05,012000088 16 82 i 150 1210:16102 13-74 42-42 Yen. ] 38-28 No. 1645 1646 l>. .1. KEARNEY, INSPECTOR. ! 45 26 27-85 46 53 47 79 41 39 4016 46 33 38 90 31 62 65-85 2 0,0 12 ■ 1 26-60 71 OO 31 62 27 81 3162 26 45 30 19 65 49 70-27 64 66 70 67 67 69 30 19 66 9t> 18\ 70 l-6;0 120 . 2 5'0 120 362 02 1 5iO 12 i 1 0:0 12 018 0-18 1 20 070 17 31 19 Itfi 36 05 YcM. 't-24i Ye». 16 91 35 02 Ye*. I 17 96 36-69 Yen. 18 63 1 OiO 120 SeiO 64 i7 84 No. 2 00 120 361 52 I I ! 1010 120 180-70 18 49 16 83 41 33 Ye«. 16 89 37 Oil Yefc I 40 9l| No. I 58701| i 58702 687031 58704 68706 68706 68707 68708 lUW. •' § Nature Naiiifand Ar 1 of of V'tndo Sample. & 6 ^ ■r. H. s = X CoHt. BULLETIN, No. 284— \ame anii Addresn of Manufacturrr or FurninhiT, ax (fiven by the Vendor. Mitntifacturei . Furnisher. DISTRICT OF VALLEYFIELD- .July 15 Arsenate of 1 .•,*)51B..sn,r A Chusl, . Vul ;< jar». -.") Canada Paint Co., I Lead , [ ItyHcld, V.i.}. t.td ' " 2t! .. ..I58052.TM. Fortune. Hun- .-i „ . . l.2(J Slier'win -WilliauiH! I ,„ ., ^ 'i"g'l»n- f'-y. Co., r,t8 W. ,J. Orali.iiii, Sparks St., Ottawa 59159 (JralianL liros., i^ueen ' St., Ottawa 591tiiK!raham liros.. Queen St., Ottawa. i Nat. Dni^f & Clieni. Co., Ltd., Ottawa, 40|Lyniani Ltd., Men 75 The i^anada I*a i n t Co., .Montreal. JJ5May.it Haker.Uatter- : sea, London, Kng. Drug Trading Co. Toronto, Ottawa Drug Co,, Ottawa. Manufai Hirers. . June 23 Arsenate of 57;{,V) 26 Le ad. ; 573r i 573."i2 ; .5735;) i ,".'5.54 DISTRICT OF KING.STON- O. \V. .MahcHrti, Kings-r, tins. 75iThe Canada Paint' w""!- ^r. , o L- ', ^ Co., Montreal. i U. A. .Mitci.ell,king». 3jar8.; 9li;.\ational Drug Co. ' ,''",'• ,, „ ,„ '„,. ' I London, ( )nt. A.(,een,l!ellev,l]e....,311»,.,: 7,5j Drug Trading Co. H. R. Smith, Cohonrg. 3 tins. l.l)5,Sanderson & Peardy' .^.""'."'"' ,,,,.,., i i Co.. Toronto. | .McDerinid .V ,1 u r y , 3 bot.i. 75;C..nada Paint Co.' I •■'*^' •*"■". I Montreal. I LEAP ARSENATE. RfFtultn of AnalyiiH. •3 Resulth calculated on the Percentage Weights m Dry tSauiplF. ■& IiisiN (tor's Report, (N ni>t !in MXpre«- -i 1^ ^ t 1.1 6 s < § Kemarks and Opinion of the Chief "11 )u of Opinion.) ■i % ! . -s <6 I ^ III 1 3 ater Soluble nic as Xn-t O ater Soluble an Pb. <». 3 ii 1^ 11 1 Analyst. H 1 E= S S |S fi «! < a ,r. I. COSTItlAN, ACTIXG ixspkctor. I : p. C 30 02 40-45 39-62 p. e. p. c. ;p. c.ip. c. p. c. p. c. P.O. P.O. 25-88 70-09 2 0,0-12 0- 18 1-70 15-86 42-74 Yes. 58051 25-88^ 71-11): 2 00-24 36 1-40 15 41 42 40 Yes. 88052 25-881 71-37J 2 00 120 00 1-88 15-79 43 00 Yes. 68053 .1 A. lUCKEY, INSPECTOR. Li!«ll,.il, Neutral. r. 1*. Arsenate of L-a-l. 43 ;& 2U-88 1 1 1 71 74 15 i 48018 1 0-84 14 66 40 64 Yes. 59151 7357 Nugent 1) r u g C o . , ;$ „ PeterUi.'o- ! 57358 W. .Ma7461jH. Cooke & Co., Orila „ ; 25 lia. '■ ! ' i ! 57462 Wm. CroMsland, Barrie'3 pkgsi 90 . .1 5741)3 D. Pettit, Pickering . .Il J lb. ..; 57464 G. .M. Rice, Whitby, ilj . i i . . , 57465|Sandfrson, Pearey Co., 2 .. I 65 .Adelaide St., Tor-j 30 20 iThe Sherwin-Wil I lianis Paint Co. 1 Toronto. 40 jCanada I'nint Co., I Montreal. Unknown Lyman Bros. 4 Co., Ltd., Tor- onto. The Drug Trading Co., Ltd., T..r onto. Nat. Drug i Chem. Co., Ltd., Toronto, •).4()6The T. Katon Co.,i3pkgs 51 Interstate Chem. Ltd., Toronto. i Co., Jersey City, ! I N.J. :il DISTRICT OF HAMILTON - July !) Arsenate of I 58825,Parke & Parke, 17!3 tins.' 60 |Gr.a«selli Chem. Co. l*ad.| Market .S.iuare,Ham-i I Hamilton. I ilton. I ^ ..! 58826 GrasscUi Chem. Co., i3 jars. 54 i Vendors I Ott.awa St., Hamil-i j j ton. 10 I 58827 Niagara Brand SprayjS kegs 4.20 Merimac Chem. Co., i Co., Brant St., Bur- | Boston, Mass. { lington. I 11 LKAD ARSENATE. Resnlta of Analysu. KtMulU calculated on the dry Percentage ■3 Sample. Weighta in •r ^ OriKtnal rt«mi)le. In-iiictnr'uReiwrt- II.4 not iin (■ -^^n-g- 4 1 o 3 1 i 1< i 3 a i ^ 3 ,;■ o S Reniarka and Opinion of the Chief siun 1 rf Upinlon. £ 1 ! s 2 13 X 1 ■^ ■^ 3. Analyst. || o* 2 S !3 x" « ^3 1 -a ^ 5i II 1 'o t 1^' 1 21 a.Si ^3 |l 1 ll d a ■e2 ^ ■5 S # ^ •< ^ •rug Co., Hanukon. Chemical Lalxir- atory, Toronto. mSTKICT OF ROCKY MOUNTAINS- „l •Tuly SJArsenaie of 49917 C. R. Maalonald, Rev- J U, 1 Lead , eLstoki, It.C. ' 49918 Walter I)ews, Revel- v' 11. stoke, B.C. ., 49920 K. W. HazIewo.Hl, jllJ j Trail, 15.C. I 499.S2(;,«,di..e Bros., R„«8- V lb I land, B.C. ^ , . , 49940 I>,x,Ie l)ru« Co., XeLStin,.; 75 The RC. So^m.WWh 4'194'JRi,. !,.'.,» 1 i> ^ .. I 'V ancouver, B.C. ..,4..943R^.,j.J.rd^On,,Co.,3 „ ! ^^VreelandChen,. Co., 3l Hi 16 281 28| 411 .Merimac Chem. Co., I... ISoHton, MahH. 55 \'r RenultH CalcuIatMl on »,!ie Dry Sample. I si' 3 1 J 1 e2 •< ■•■■ -S ;3 » js •i l3 2 .2 ■ [ Percentafre I Weights in ■;'"'ri(rin<»l Sample. .rXd. TALISOT, INSPKCTOR. .aSf a. Remarks and Opinion of the Chief Analyst p. c. p.e. p.c. i p.c. p.c. p.c. p.c. 43 70 26-88 '0-45 1 50120 00 1 38 41 67 25-88 W SO 100120 00 3-88 39 91 35-88 69 3S 1 00120 00 ^ i 88 !'. c. I p. c. 14 56! 39 67 Yes. I 54847 15-Oitl 40-13 Ves. ] .-u; I 15 55! 4i-67i Yes. ; 54878 TH().S. PARKER, INSPECTOR. 26 U-20 "o 16 20 38 47 15 14 1 12 4 12! 1 75 2 5 12 60 Oii'12 5 12 12 0-24 70 17 69 43 14 Na 49917 No. 49918 No. 49920 No. 49932 Yes. 4994(1 58!. ! No. 49943 .1 V. I'OWfiR, INSPECTOR. 0-20 31 62 66 41 200 24 OOO 1 76 . . . 015' 32-34 66-22 1 50 120 ISl-W... Xo. ; ,54911 No. 54912 11. o-siLLIVAN, INSPECTOR. Kl.vir., 28-9«i 16 44 69 33 05 294-! 66-96! 35 I 31 •621 64-93' 28-76i 68-80 ! 23 88; 68-80 2-5 6 12 I 00j3-38i 19 73 12 i8io 20 I 36:0 18|l-96 ! I 12:0 .'WI5 62 15-90 48 91 1 No. No. 38-06 Yea. 1725 4606 No. 57632 57635 57636 57637 I