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Maps, plates, charts, etc., may be filmed at different reduction ratios. Those too large to be entirely included in one exposure are filmed beginning in the upper left hand corner, left to right and top to bottom, as many frames as required. The following diagrams illustrate the method: Les cartes, planches, tableaux, etc.. peuvent etre film^s ^ des taux da reduction diff^ronts. Lorsque le document est trop grand pour etre reproduit en un seul cliche, il est film^ A partir de i'angle supArieur gauche, de gauche ^ droite, et da haut en bas, en prenant le nombre d'images nicessaire. Les diagrammes suivants illustrent la mAthode. 1 2 3 1 2 3 4 5 6 LABORATORY OF TBE INLAND REVENUE DEPARTMENT OTTAWA, CANADA BUJLLETIISr :N^o. 277 TINCTURE OF IODINE •'56277—1 CORRhCTION. Bulletin No. ii73, Gelatin]). 13, Sample No. 58729 — under the column headed ' Remarkii " the word artificial should be deleted. LABORATORY or Tui INLAND REVENUE DEPARTMENT OTTAWA, CANADA BULLETIN No. 277 TINCTURE OF IODINE Ottawa, February Iti, 1914. Wm. Himswohtii, Esq., Deputy Minister of Inland Itt'vcnun. SiK, — I beg to submit a report dealing with 72 samples of Tincture of Iodine pur- cliased in Septemlier and October last. The following is u statement of rexults : — Samples. Found genuine 62 " adulterated 8 " doubtful 2 Adulteration consists in the use of Methyl Alcohol (Wood Spirit) for Ethyl Alcohol in the preparation of tiic article. Ethyl Alcohol alone is prescribe 1 by iho Pharma- copoeins ; and the Inland Revenue Act, Sec. 2C6 retiiyl Alcohol, in black letters not loss than one fourth of an inch in height, wher- ever it is used. Two samples aro marked doubtful because they do not conform to the formula of the British Pharmacopoeia, nor do they, with exactitude meet the requirements of any other pharmacopoeia. They have, however, evidently been prepared with honest inten- tion, us one contains over 5 per cent of Iodine, and the other meets a demand for a colorless tincture, which however s'lould not be confused with the B. P. Tincture of Iodine. The last examination of Tincture of Iodine was made in 1908, and results are published in Bulletin No. 152. I bog to recommend publication of this report as Bulletin No. 277. I have the honour to be, Sir, Your obedient servant, A. McGILL, Chief Analytt. 66277—2 BULLETIN No. 277- Nkture o( Sam pi*. Name kixl Addnwi of Vendor. 9 d Owt. Namr and Addrxaa n( Manufacturer or Fiimiiher aa Kivtn by thx Veu>tur. Manufacdirrr. Fuminhw. DIrfTRICT OK \OV,\ aCOTIA- 1813. Ocf. Is'Tincture of ; 54311 L. C. Cartlener Co., Yar- U o». Iodine. , mouth, N.S. •. IB „ ..! 61312' H. K. WilKin, Wimi-or, 12 .. ! N.S. 23 .. . . 54:113 r.n.wn Bron. t Co., Hali 12 .. fan, N.S. I 27 ,. .. r.1314 Crowe Bn>»., Tniro, N S. 112 „ 27 ., .. 54315.1. J. Kinlcy, Lunenburg, i 12 i> i i N.S. 76 Vendor . 1.00 90 j Vendor*. 1.00 l.Cin Vendor . DISTRICT OF NEW BRUNSWICK- Srpt. Oct. 20 Tincture of ! iodine 3 I 16 I 22 23! I 60387 Nat. Drug & Clifni. Co., 3 boU. 1.20 Vendor*. . .. Ltd., St. .lohn, N.B. | I 1 .WStWTIiH Canadian Driitr Co., '3 LH. St. Jr.lin, N. B. 503t<9Thp Bttird Co., Ud.,13 V. iXKlatllclc, N.B. ri0.'?90 Leger Drug Co. Ltd.,:3 Moncton, N.B. 50391 C. P. Hickey, Chatbam, 3 N. B. i.aoj 1.20' I 1.20; I l.OOi Vendor, DISTRICT OF QUEBEC- Sept. 22 Tincture of I 50169.1. B. fJiroux, SK> RneSt.'l2 oi. 1 Iodine.' ! .Toxepli, (.^uplx^;. „ 221 .. .. .WUO .los. Maswin, So8 Rue St. 12 .. . I 1 Valier, (Quebec. I „ 23 .. ..I 56171 A. Martimau, 7»IRucat. 12 .. . j .ToMi'ph, (Quebec. I „ 26; " .. 66172 VV. Brunet&Cie, 139 Rue 12 .. . I i St. .l(M*eph, tjtuebec. „ 261 ., .. 56173 L. E. Martel, ."il Rue St. 12 .. . I j Joseph, Quebec. I i 1.80 Vendor . 1.00 1.20 1 20 90 Vendor* . Vendor . DISTRICT OF THREE RIVERS- Sept 24|Tincture of Iodine 25 25 25| 1(7 69740 A. I.,. Bouchir, Joliette. . 12 o*. 597.V1 R. W. Williams, Three 12 .. . Rivers. 59756 J. A. Peltier, Three Rivera, 12 .. . 69767 L. P. Normand, Three 12 .. . Rivers. 69766 J. T. Gaudet, JoUette... 12 .• . 1.26 Vendor. l.OOLj. an8, Ltd., Montreal. Vendor 1.20 1 10 1.25 Btm TINCTURE OF IODINE. Reaulbi of Anklyui. In^iM'ctiir"* llfinjrt. (I. iiirt an fx|)rfw.ii n of O|>iiiion). I "8 •s i II Aloohol. i - i 1 ^ i Renurkif ana OpinioD of the Chief Anklyit. R J WAl'tJH, IN8PECTOK. rmula . . p 0. 894 8M p.c. None 236 pi. 89 80 79 71 Ethyl 13 !0 Mwthyl 75!»7 Kthyl. 51311 54312 Not 11. P. for.nuU. Contain! methyl alcohol. Adulterated. (fonuine. .. 849 3 51 79 71 " 54313 " » 2M 242 79 71 .. MS14 -. .. 265 2 28 76 24 " 54315 " ■r. c. KKKt;usoN, inspector. us. I'har. Formula . B. P. Formula . 819 3 06 81 60 366 2 80 81 60 5 79 None. 86'41 289 3 05 75 21 282 2 80 76 9J Ethyl Methyl (cru'le.) KthyL 50387 lOenuine. C0388 I 50389 jContaini Methyl alcohol. Adul- i tented. 50390 Genuine. 50391 K X. W. E BELAND, INSPECTOR. 561 225 353 226 2-41 None. I 78 ■4« 2 17 ' 80 10 I 2 10 I 80-1I 2-78 I 79 S^ 2-48 75-62 Ethyl /il'i'' 'Not B. P. fonuula. Doubtful. „ 8«!7(i Gem. 'le. .171 .■■6172 i ' 5«1-H ■ DR V. P. lavall£e, inspector. 207 3 32 70-62 2-52 2 65 76-91 236 2 62 78-48 237 2 20 80 10 807 332 68 78 Ethyl 59740 Oei 69755 59766 j 69767 I 69758 I BULLETIN No. 877- NnntM of H»ni|'lf. i i.( V-ndor. Oixt. 9 a i 6 :52 Nanw •ml Adilrew of Maniifactiin'r cir Kiinii«l.>^ »» Kivi-n by tlv Venili.r. MunufftftnrHr. Fiiriit*hHr, DISTRICT OF KASTKRN TOWNSHIP8- 1913. 8<-pt. Oot. 20Timtiiiv <>( ! I ml i IK'. IS 17"i7 H. KiTnm, Ar!h»l)»«li»i!l.. 12n».:l 801. U.W K. C. Fraier, H(ierbr(ioke IS - 1 17ri!>«i. A. Ct«li'TH, M.«K»ntic 12 i 1780: A. VailliHicoiirt, Waterloo 10 . KGliUr. E. .St. JacipiM, St. 12 I Hyaointhp i I I 1 " ' Vendor. 1 80; i ; 1 00 „ 1 2oi .. . DISTRICT OF MO.NTKEAL- N()v. I i ■ I :tTincturcM,( .'>S(i21 .\rtlmr Cluiii'nt. Notre .'iboU. 1 S.'"'; Vendor. I IcKlini". l>ante St., Ijachinf j 3 .. .. BSCL'J Lacliini. I'hariiittiy S70HI. ;j ,. 1 001 ,. .loHfpli .St., Lat'liin**. ■ ! 4 .. .. .\-«i:!3.l. Victor Kii-liin.md, 7013 .. 1 !0 j i Wfllintfrmi St.. Lnchiiif 41 .. ..■ f)J«!21.I. A. AriMi-liii, :il <'.-iitrf 1 (X» ,, i , St., .Montrnal. 41 M .. 5«i2."> l>i. loiiitliii-r, Wi,'! Centrr ... 1 .T5 ,, I , St., .Montreal. DISTRICT OF VALLEYFIKLD- Nov. 20 Tincture of Iodine. ,. 2o; .ISOTI Phartnaoie St. On|r«, V»l Shotii. 1 80 Vendor . Invfinld. i .W)72l)r. .1. t. A. Ganthier,!3 ., 1 3.'5 Valli.yH.'ld. j DISTRICT OF OTTAWA- Sept. 17 Tincture of Iwline. .. 17 Cot. •WKllW. B, Chrk, Druffgi't, j R«*nfrew. 5!>172:D. J. Kitza, Renfrew. I . 591 7.1 Clarence H. Lewis, Bay ; St., Ottawa. . 50174 Fred Brethour, Bronson 1 ' Ave., Ottawa. . i 59175 .\llen & Cochrane, (lru(f- I Rists, Bank and (iilmour ! St«., Ottawa. i I2oza. 12 .. 12 ., 10 „ 12 ., 1 00! Vendor . 1 2o' „ 120j „ .. 100 ,. .. 1 20 Vendor* TINCTUKE OF lODINK. Krwilu I if Aiialjriiii. Ini«|frti»r'ii K- txirl I > lint >D f » I ■■'U'n a<{ CpiniiMi. 1^ fla t. > "B'" ; i •V 6 12 J. C. ROl'LEAU, INSPECTOR. l>.c. j tl.C. P.C. IVittl.- UbrllMl T.ymiin.! "» '? J 20 ; B7 09 Knox k Co., .Montrpti 2 03 ■ 82 4tt I )t'oulourized . 4 43 ' S 2 07 3 79 71 81 2S Kthyl . Kthyl . i Kiniarka anil i|iiMi>n nf t' Chirl Analynt. 17&7:(>»naine. 17.WJ ., •17n!) Not U. p. tirrturc. Doubtful. 1760 lienuine. 17tl' D. .1. KKARXKY, INSPKCTOR. 2 38 i 2 .57 2-97 j 2 09 I 2 38 j 79 78- 78 70 31 79 00 80 26 77- 78 48 lEthyl R8fi22 Ocnuine. [ fixliilc of iMitaKKJum tito low. Adiiltirat<-(i. 5882.'''»;enuin«>. I &8r>24'Iiidii1p of potoMium too low. I Ailulterated.. 68»)2r> C ienuine. ). .1. KKARNF.Y, ACTINO IX.SPKCTOR. 1-65 2 39 2-73 I 78 18 3(>5 76M Ethyl . .1. A, RICKEY. INSPECTOR. * Labelled Tincture of lodino, Deoolonrized. 58071 Iodine too low. Adulterated. S8G72 Genuine. 2 88 2-43 78 48 Ethyl .... 5917l' 2 96 2 M 7809 ., .... 89172 2 80 2-62 7B91 S9173 3 74 263 78-88 ., .... 69174! 3 10 232 81 28 II S9175 BULLETIN No. 277- ,1 6 o I nf Sample. •r. c° Nanif and Adn-?- of \'t*n s o n , 28 12 .. ' .Ma-ket St., Urantford. | 3 „ .. 50894. Walker, Abbs A Co., 29512 ., I 1 .St. Paul St., St. Gather ines. Oct. 100 Vendor. , 120 110 100 100 Nat. Dnig 4 Chem- ical Co., Ltd. Vendor Vendor* . DISTRICT OF WINDSOR- 8 Tincture of 1 Iodine , 8| 54411 J. McRobie, Petrolia. ll2oM. 54413. Tackson & Co., Petrolia. 12 .. 54428 (J. (i. Ingeraoll, Samia. 12 „ B4429 P. T. McGibboo. Samia, 13 „ M434 iH. Robertson, Samia. 12 lOO' Vendor. . I 120 Vendors 100 Vendor. . 100 » . 120 TINCTURE OF IODINE. Innpector'n Reix5 R«mmrkii and Opinion of the Chief Analyxt. J AS. HOGAN. INSPECTOR. p. c. 2 34 2-30 3 12 IttO 3-4!> p. c. 2-59 303 2 68 1-57 2 13 p. c. 77 30 Kthyl 79-71 J i 7809 ' 83-59 i I Kthyl tW jMethv 15 73 79 ^ Ethyl 27 1. 32 60041 Genuine. 60042 60013 I 60014 :Methyl alcoliol pn-iient. Iodine tiHj low. Adiiltnrated . 60045 iGt-nuine. H. J. DAGf;R, INSPECTOR. 66 77 I 2 7 574t7 57498 .1. .r. COSTIGAN, ACTING INSPECTOR. 2-52 2'13 2 46 2-50 3 26 2-39 81-28 Ethyl. . 2 !» 65-« M .... 2-44 70 24 2 tHi 86 44 MKhyl... 2 61 79 32 Ethjl... 508!)0 Genuine. 50891 \ 50.S92 50893 CoutBins Methyl. aUohnl. Adul- teratf d . 50S94 (icnuine. JNU. TALBOT, INSPECTOR 3 03 2 79 75-70 Ethyl .... 54411 2 h2 2-86 81-60 .. ... 51413 ' 2-67 2 44 77 09 ■■ .. 54428 2 69 2 61 82-37 54429 »19 2 86 80-10 54434 10 BULLETIN No. 277- S & Cost. Nanu* and Addrcst* of ManufucturfT or FurniHiier lii* given by the Vt'iidor. Nature of Saiiiplt'. Name anti Address of Vendor. S " 5- d Maniifucturir. 1 Furnisher. DISTRICT Ofc MAMTOBA- 1913. Oct. I 6 Tincturi' 8'Ruth.'ifordDrUKCo.,NeI-il2 «■/.: 180 Vendors. I son, B.C. ! 49'.ltiM Cnadii l)ni(,'& Book Co., ,12 Ntlson, B.f i 499T6 X. K. Sudda . Fernie. . . 12 4997T -McLean Drug and Book 12 Store, Fernie. I 49990 Tlios. Stout, Rossland. . . . 12 135: ., 135 Vendor. 180 ,. ■ 150i „ DISTRICT OF VICTORIA- Oct. l8jTincture of | .-)7«43 HalKV Co., 702 Vates St.. 12 oj, 150| Vendors lotline.' ! Victoria, B.C. ,'>7(>,")8 Ivilsl'harni.icy, 1415(>ov- 12 ermnenl St., Victoria,' I B.C. 5;(;.">9 0ak Bay I'haruiacy, Oak 12 Bav ,1 unction, Victoria, BC. 57lifi,t Terry'n Drug Store, 705 12 j Fort St., Victoria, B.C. 57609 Dean & llisct^k's, 027 1 Yate.iSt.,Vic;t .ri.-i, B.C. l.')0: V'eudor. . 130 { 150 .. i i loO V-ndoix. 11 TINCTURE OF IODINE. In8|iector'8 Report. [ (Ik nut an etpnmion of ! Opinion). I tt«iulti) of Analyaia. ^ ! Alcohol. Ji «^.,>1 c g ► I' = B f. .§ 2 a s 1 Remark! and Opinion of the Ch'ief Analyst. A. C. LARIVIERK, INSPECTOR. lie. 2 42 2 69 2ifi 2 69 2 94 p. c. p. c. ! 245 83 09 Ethyl..., .1 48985 283 8U 49 j u .. . 48936 1 2 97 83 43 i . 48987 2 58 78-48 .. . 48988 2 91 83 43 . 4M9WI Genuine. TIIOS. PARKER, INSPKGTOR. 2 79 2 274 2- 306 2 2-69 2 261 2 2- 79 2-62 ■ 2 83 2-58 2-51 79 71 Ethyl... 1 i . , 49»W 76-65 M . . 49969 77-69 49976 , 75 -.52 11 .' 49977 78 88 . 49990 Genuine. D. OSULLIVAN, INSPECTOR. 2 21 282 3 15 415 2 69 2 40 82 70 Ethyl \ .57643 jUenuine. 2-47 79 71 ! 57658 | 3 36 784-8 j „ ... i Ethyl None. 75 88 58 60 Methyl i 17-28 2-47 I 78-09 I Ethyl.. I : 57669 57663 ^Contains Methyl alcohol. Adul- terated. 57669 Genuine. mtm