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I I C jloured pages / Pages de couleur I I Pages damaged / Pages endommag^es D Pages restored and/or laminated / Pages restaur^es et/ou pellicul^es Pages discoloured, stained or foxed / Pages d^colordes, tachet^es ou piqu^es Pages detached / Pages d6tach6es 1^' Showthrough / Transparence [ I Quality of print varies / n D Quality in^gale de I'impression Includes supplementary material / Comprend du materiel suppl^mentaire Pages wholly or partially obscured by errata slips, tissues, etc., have been refilmed to ensure the best possible image / Les pages totalement ou partiellement obscurcies par un feuillet d'errata, une pelure, etc., ont 6\6 film^es k nouveau de fa9on in obtenA. BULT.KTIN No. 197 IJME FRUIT JUICE (I.IME JUICE) W. J. Gkkali>, Esq., Deputy Minister of Inland Revenue. Ottawa, Jaiiuorv 12, 1910. Sir, — I have the honour to submit herewith a report upon 76 sample^ purchaaed as lime juice, throughout the different inspectoral districts of Canada in December of 1909 and January, 1910. The last examination (comprising 27 samples) of lime juice was made in 1902, and the results are published in Bulletin No. 83 At that time I was supplied with six (6) samples of lime juice, whose genuineness was vouched for by the importers. These samples contained free citric acid averaging 7-74 per cent. A mean content of 7 66 per cent of free citric acid is yielded by the results of analysis of 42 samples of the present collection, which appear to be genuine, except that some may contain small amounts of added water. It would thus seem justiflable to establish at least 7-5 per cent of free citric acid as a normal amount for lime juice. When the article contains decidedly less than this amount, it is reasonable to infer the addition of water ; and as the number 7-5 per cent has been deduced from a list of 42 samples, including 13 which show less than 7 per cent citric acid, it cannot be held that the standard suggested is too high. The present report comprises : — 9 samples, sold as lime juice cordials. 42 " judged to be genuine lime juice. 13 " judged to be abnormal, but are not declared to be adulterated. 12 " adulterated under the Act. In the absence of legal limits for density, citric acid content and other definitive characters of lime juice, it is impossible to declare adulteration in the cases of those "■xmples which I have marked 'doubtful.' Where, however, there is addition of matter (juite foreign to lime juice, and manifestly added for the purpose of taking the place of some natural constituent of lime juice, the article is clearly adulterated under Section 3 («). (6). (")• It is not certain that the addition of a dye to true lime juice can be held to constitute adulteration ; but the addition of a dye to a solution of tartaric acid in water is evidently made for the purpose of concealing inferiority and of enabling the I)roduct to be taken for a true lime juice. This constitutes adulteration under Section :\ (h). 11204~1J Ifffil- '! ^n , t Ouiciod hy the prinripleH lairati<>n conitiiitH in th* atliiitioii c of a dye for the purpose of imitating the natural yellow colour of liiiie juice. Were tha Nainplea in question sold an 'coDipounds,' they could not he declared adulterated, since Section 'J I ('/) of the Act provides for «uch articles. Hut I find nothing on the laliels which could inform the purchaser that he was being supplied with anything else than the genuine juice of the lime frt. ' and our inH{)ec^o^l have invoiceit form of adulteration is evidently the addition of water to the juice This would have the effect of lowering the specific gravity (density), and of reducing the percentage of container! citric ucid. In order to determine whfher or not water has been a(ldercentage content of citric acid therein ; olso to determine the variations from such normal which may l)e exhibited by genuine lirae fruit juice. Aiioiher character of lime fruit juice is its optical activity, and in the subjoined table I have brought tigether the results of recorded work upon sample.) I«'ieve( Samples. i ' Maximum. 1 .Miniiiiiim. Mhsii. , Mstimum. Minimum. Mean. 1 3 3 4 j t 1 0898 i 1 1 iHat 1 1 OSes 1 02HR 1 0266 1 ill 1 8 12 7 68 ; 781 8 82 7 38 » 61 6 36 602 774 7 20 712 7 66 +0^.0 -(f .6) to } + 0°.5) 6 8 4 42 10339 1 1 7 87 1 i w 1 Krom examination of 6 sample> Kunig, Xahrungs and ( ienuwmittel, Bd. I, p. -tT. 8. .■ .. 4 „ „ .. „ p. 1304. It id not certain that the nun.bera quoted refer to lime juii;e pni|>er, and not to Innon juice. 4. Knini fXttiuinatid-.i nf 42 'amplex, rejiortt^ in this Bulletin and probably genuine, but not guarantefsl an ttuch. I. An examination of the tabulated results of analysis, and their comparison with the above means, will show the grounds upon which I have felt justified in declaring thirteen (13) samples to be of doubtful genuineness. The standards for lime juice issued by the Bunde Dentscher Nahrlingsmittel Fabrikanten und Handler (Deutsches Nahrungsmittelbuch : Zweite Auflage) in 1909, recognize (page 286) a first pressed juice (Muttersaft) end a second pressed juice (Nachpresse). This second pressing is the result of addition of water to the residue left from a first pressing of the fruit, and the product is necessarily a very inferior article. When the product of a second pressing is added to tb-^ first pressed juice it is required that the fact should be distinctly stated upon the label and that the article be sold as a mixture (Fruchtsaft mit Nachpresse). It may be that the low grade lime juice samples which I nave characterized as doubtful are mixtures of the kind indicated. If such is the case, they should undoubtedly be plainly labelled in conformity with the facts. LlXB PkUIT JuiCK CoRWALS. OR LlUU JviCt CoRDIAU. Nioe H*mp!u are labelled ai Cm-lialt. Thi* term it apparently applietl to a ililute«l and aweet«ne(l lime juice, and a linm juice cordial differ* from plain lime juice merely by the addition of water and iugar. The amount of water added -ariea much in different brand* ; and for the nino Haropleti now reported, the extreme!) ar" about 43 jier cent, and HI per cent, raiculatctl from the citric acid content. Tbcdmuuntof sugar '■hI varie« from about -'0 [)er cent to over 50 per cent. Since the lima juice i^ ilie characteriatic component of thexe articles, it it evident '»nvi. their value variee K>«atly, and the following conitpeotu* in of interest : - SMn|>lr ■Mm 1 iooa 3)«8H 1 OSM 4(i;«3 1 taw i-jim 1 27tlN 42789 12301 ^IHTS t 3896 44709 13361 37H0I I i:(02 MttSl 1 OIHH 63 81 71 V.I 62 63 43 R4 8' 30 3U 26 ( (No prmurvktives). 3(1 U (N'u pr«H-rvativea). With four exceptions, ihesti articles contain salicylic scid wt a, preservative. No mention of this fact is made on the label. Number 403M1 is exceptional among these cordials in containing a high percentage of citric acid, very little added waUr, no suger, and 7 27 per cent of alcohol e(|uivalent to 15 8.'5 per cent of proof spirit. This article is legally saleable only a.s a drug, or an «n alcoholic beverage. I beg to recommend the publication of this report as Bulletin No 197. I have the honour to be. Sir, Your obedient servant, McUILL, Chief Anali/$t. IKJTrLKO Xatiire I Aiit All upinion. t IHSTUUT OK NOVA SCOTIA tiWt i>m. 7 H .. 7 " 8 ■■ IS • e. FVittlMl Liiiiv 4t7)'>'<'R. n. AiUiiia A r.<.,'3lwU. m IVHiii., Jtlit H;llif»«, X.S 417BliNatiiiiMl llrug t'.).. ; lialifoK, N H. 4l7)l2i\V>-iil»'ll», i.tit., ICaIi I f»x, N.M. 417kiKri- tfii Brand ll.ili \V«.t Imlia . . ID) Nat. DriiK ft CIihiti. SovRrcifrK Uraiiil Ok, IUIifa». N.«. DISTRICT OK I'RIXCK EUWARU I.SLANL* I)ih:. 7 l<«ttl<'il tiiiiir .TKfill A. IV Pwim-l, Smu.-. 3|)t«. . W Kr»mf« Krake, Ncwl Juic*». JO 10' .11*012 Viiict'iit Mclrtaac • »8 VV.nt India ' Halifa\. N.S, j Limn .riiiiv. 45.Sii«wx MimraKSiirViKiitra tiiio Wei.i j O)., 8ii~-.x, N.U. India Linif.luiw. . ■!.'> National l>nig Co., Stive reign Lini** 1 Halifax. \ .ItiicH. . 45 Havclock M ineral! I Spring Co., Have- I l.wk, N..S. UI.VrKlCT OF NKW IJKL'NSWICK- 3!tB2? Th.' Ni'- ..al Drug ft ClHiini' .1 (;<>.. Ud.. y< '..lin N H. 3W124 K. - V k, Ired.ric 3!H>25(t«i. K Crawford, St. Stephen. N.H. 3062(i Fair^.'eatlier Hro»., Monetun. SMtOT .r. Mel). < ec. 10 10 BottLxl .luiee 22 .. 22 •• 22 " Lime! .WOf-i W. (!. IK.yle, \Vi.«t:3bot8.'l Fn-ntin. ' i 3)'>C93I..acawi« ft Audet. St.' ,■ ' h^lttuard Frent.T<» Falanleau. -.'rii „ .0 ; Rje St. Joaepll. 1 ; S.'j'WhiUad ft Turner, i t^uelH-<:, 75 N. Tnrcotte 4 Cie, i (i'leU-c. 75 National Drug Co., Montreal. -IL. RR.naudftCie., I t^iiel)ec. ObJ. .». Cliabot, Quo- ! bea UME JUICK. KnViTn »"»• As iLV»l>. - -1 'is'" -r; "S a. - •^ •* atf Keactiim i i with ttlcohul 3 Pn«,v„iv«..4^j:j.^ to a By nip.) I "5 J B 9 a; Kctuarka and Opiniiin of tbn Chiet .Vnalyat. K. J. WAt'fJH. INSPKCTOR. 1 oaiwi so ^ B (n 1 03U, ii;i 01 ■Ml 1 03131 0!( sj em 1 ikSH] 90 o{ 6 30 1 034o! Ittt 7. 16 Hulioylic acid Bulky ppU. iiri-l (i.-imiiif with trac*' of a pirMrvativo. I tl762|(!«nuine biic ccntaina a prmerrativto. 417il3,l>«niiinii with > .rac« nf iw-wsmtivK, 41764 Qonuin* but containn a pn'wrvative. THKO. M(M)KK. INSl'KCTOR. 1 (K!2o i;: r> 1 itXSK lOL' 5 I ()364 116 I 0345 111-5 1 0103 12S I 72 ' I !> Sajicrylic acid Btilky ppte.. prtiwnt. 7 17 00 „ ..! 8 12 -0 4 Salicylic acidi ti act*. 7 80 0.>rMM«rvativ«. 38613 (icnuin** btit with a prt'Hi>rvative adtled. I 3H614 (irnuine with a prewrvativn. StWl.") (Jenuine but coiitaina a preservative. .1. C. KEatfJUSON, INSPKCTOR. I 03W 123 8 CI I U;<64 11.5'5 8 08 — 0-6 None .. -0-4 1 03tl0 1 0346 126 a 8 82 lit 7 98 HI I' 7 77 Salicylic acid ! preccnt. 00;None 51 Bulky ppte.. 39623IOenuin«. I %624 3!)63n 39626 39627 Genuine but contains n prewrrative. (Senuine. E. BELAND, INSPEi lOK. 1 (>3I7 114 5 8 01 1 0287; 90 1 ()296| 93 8 11062 610 I 03481 HI 6 SO 684 367 777 I I — 01 Xone jBulky |ipte.. -0 2 -0 3 -27-8 00 Salicylic acidjFpte. l)eli)W present. normal. None Bulky ppte.. 36692 Genuine. S6603 36694 36695 Rotation after inversion —27 8. Cnn tains a yellow dye (small aiiiouut) Sold as a cordial. 36696 (ienuine. BOTTLED LIME Xature of Sample. Ji s Name and AddrcM Vendor. of Name and Address » » ■ »> of Manufacturer '""PWitor s Report. or KumUher (■» o"* •" , as given by the expression of Vendor. opinion.) DISTRICT OF ST. HYACINTHK- 19C9. Dec. 7 .. 10 .. 21 .. 21 :$ c. Bottled Lime: 38884JPh.rm. Larochelle. 3 Bot,^ 76N.t. Un« ft Chem.i "Sovereign" B^nd '38885A.,^l;y.St.Jean..., „ :..20jL^^Si^'^'..Mo„t«.rr.t.".... A II .» ^ „ Montreal. j \f.;J *"■* * ^°-' " 75Nat. Drug ft Chem.! "Sovereign." U H. Oliver, Sher- ., " " brooke. Thw. Hebert, St. Hy- „ : 73 J aciuthe. ' 38887 33888 anadal "Montserrat." Robt. Simpson ft Co., ' 'Jiontebello. " MontreaL DISTRICT OF MONTREAL- Dec. 3; Bottled Limei 40381 Jno. T. Lyon.s Co. I.,- •'"'"' ' Corp. 8 Bleury St., ! Montrt-al. 40382 .St. Lawrence Grocery Co., 395 St. Law. mnce R, Montreal. 40383 K. Blain, 8 (;uilbaalt St., Montreal. 40384 Nat Druif ft Chem Co.,Ltd.,3U;abriel St., Montreal. 40385 Lyman's, Ltd., St. I ; Paul St., Montreal.! 3BoU SS'RioUeti ft Co., St. I Thomas. 7»!t. a. Lyttle Co., I Toronto. eojSutclilTe ft Bingham, Ltd., Manchester. 66jNat Drug & Ciiem. 1 Co., Ltd. j 66, Lyman's, Ltd., Mon treal. Lime Juioe Cordial '■Sterling.". "K. Kovat." "Sovereign." Dominica DISTRICT OF OTTAWA- Dec. 6 B a . per 1 term* pit mi •^4 188 » & Rpactiun with alcohol Preeervative*. (aftrr eva|ioration toa Syrup.), a I Remark* and Opinion of the Chi-^f Aualyat. J. C. ROULEAU, INSPECTOR. r0292| 93 l-03fi0 114 10276 1 0360 1 0!»t P.O. 51 98 -0 —0 4 12 ! -0 2 26 j 00 1 43 !-2r-5 None Bulky ppte. Mioylio acid present. 38884 (ienuine. 38H86 Very alight; 38S88,Rotationafterinveraion— 27 8. Contains ppte. j conaiderable sugar. Sold as a cordial . I I Contains a pieservative. J. J. C03TIGAN, INSPECTOR. i 1 0168' 100 1017s 1 1206 1 0266 105 60'S 31 860 98 0; 6 86 00 17 00 T 0-8 +23 02 i- 2 None Very slixhti ppte. after; stirring. I No ppte Salicylic acid; Bulky ppte.l trace. I None 4038 IjConUins 16-86 p.c. proof spirits. Sold as a cordial. 40382 Rotation after neutralizing +26. Con- tains a yellow aniline dye. Artificial ' and contains tartaric acid. AdulterateG. Miihoud, Kingston 42786 W.W.Cilaon, Kings. t 3n«72'jack»on & Son, .. i ;i0883 Edward Flaherty, i Stratford. 4470!»\V. K. Butther, St. i Mary's, 44712^Jna Levenston, Lis- towel. .0 70 . 76 . 30 i -iO 75 Simpson Bros., liuelph. Sin^lKon Bros. & Co., Halifax. Taylor ft Pringle, Owen Sound. Elliot, Mar ft Co., London. Nat. Drug Co., To- ronto. 11 JUICE— Continued. Results or Analtsis. S-B 3^3 *• i per temu u Acidity CC in CCft. Per oen in Vol. calcula trie aci 3 3 Reaction with aloohol' (after I evaporation \ to a Symp.) I Remarks and Opinion uf the Chief Analyst. JAS. HOtJ.VN, INSPECTOR. 0360| 113 I 03U| 111 0278 880 I 2301 U295 41 93 P.O. 7-84 in 016 2 87 6 51 -0 8 00 - 4 -«7-8 — 0-4 None Salicylio acid trace. None Salicylic acid ;,'e8ent. None Bulky ppte. Slight ppte. Bulky ppte. 42782 Genuine. 42783|Genuiue with trace »f a preeervative. 42784 Oenuinu. I 42785 Contains a large amounc of sugar. In- I vert rotation — 70'0. Sold as a cordial. i Contains a preservative. 42786 Genuine. H. J. DAGER, INSPECTOR. 1 02S2 1 0940 I 0188 10316 10273 66 4 62 106-5 7 46 i 560! 3 92 100 0! 7 00 810 5 67 +3-6 None. —03 Salicylic acid I present. I + 8 3 None O^Salicylic acid I trace. -fO'S Salicylic acid I present. Bulky ppte. No ppte Bulky ppte. 41441 Rotation after lieutralizin^ +88. Arti- ficial and coutainn tartaric acid. Adul- ' terated. 41442 Genuine but contains a preservative. 4144? Rotation after neutraliting +100. Con- tains a yellow aniline dye and tartaric acid. Is artificial. Adulterated. 41444, Genuine but contains a preservative. 41445 Abnormal and contains a preeervative. I Doubtful. T. KIDD, INSPECTOR. 10349 1 2896 1 0311 1-2361 10262; 1126 787 +07 525 367 -85-4 960 672 +62 620 4 34 -66-8 83-5 5-84 -OS Salicylic acid trace. None Bulky ppte. S^'ght ppte No ppte . . 30871' Abnormal rotation and contains a trace of I a preservative. 30872| Contains a large amount of sugar. In- ! vert rotation —90 8. Sold as a eon' >l. 30883' Rotation after neutralizing +17 '8. Con- tains aniline dye and tartaric acid. Is artificial. Adulterated. 44709i Rotation after in version — 65 6. Contains a lar(-a amount of sugar. Sold aa a cordiai. 44712 Doubtful. 6 "8 Nfttnn.' : Sample. IS d Nune and Address of Vendor. BOTTLED LIME Name and Addrew of Manufacturer or Furnisher as tnven by the Vendor. Insiiectur's Re|x)rt. (Is not an expression of 1%c opinion. ) 1U09 Dec. 9 .. 10 10 10 10 Bottle. j 42686 -0-8 -0-2 + 3 2 Bulky ppte. Slight ppte 426(M« 42694 Abnormal rotation and contsinii a trace of a prewrvRtive. Rotation after neutralizing +0'4. Con- tains a yellow aniline dye. Is artifi- cial. Low in acidity and otherwise doubtful. Genuine. Gfniiine. Rotation after neutralizing -fOO. Con- tains a yellow aniline dye and tartaric acid. Is artiHcial. Adulterated. A. C. LARJVIRRE, INSPECTOR. 1-0306 91-0 tfS7 ■(-06 None Bulky ppte. 39831 Genuine. 1 0236 745 631 ■^o 4 Salicylic acid present. .. 39832 Acidity low and contains a preservativ Doubtful. 1 0265 800 660 00 .. .. 39833 Acidity low and contains a preservative 1 0341 1 0313 1080 107 6 7-56 7.68 -H05 00 Salicylic acid trace. Salicylic acid preaent. ppte. below nonnal. 39834 39836 Genuine, with a trace of (ireaenratire. Genuine but contains a preservative. R W. FLETCHER, INSPECTOR 1 0282 1'0»44 1 0833 10388 1 0282 910 6-37 113 6| 7 94 108 8 7 59 116 6 84 -01 -03 -0 2 None IBulky ppte. 8 15 f -(-7 6 No ppte. 388 I +57 Salicylic acid present. I 43636 Genuine. 43637 4S6S<« 43639,Rotation after neutralizing +210. Con- tains a yellow aniline dye and tartaric acid is artificial. Adulterated. 43040| Rotation after neutralizing + If ' Con- tains a yellow »niline dye and tartaric acid is artifi^^ii. Adulterated. saMtiiu 14 BOTTLED LIME Nature „l Sample. I Nam** and A'idresH i Vendor. J Nun>> and AddrtMW of Manufactiirar or Fumii*her H fciven by the Von lor. Inapectur'i Report. ( In not »n exprnMion of opinioii. ) Di.sTRirrr of Vancouver - l!)0!t. • c Dec. 13,B<>ttled Lime' 3771W Kelly, DtrnKliw * Co., 3 pU.,i» 7S Juice. i Vancouver. i 13 .. ..j 3779)1 Huddon Bay Co.,Van- , 105 couver. 1 14 I 37HOOAV, H. Mulkin Co.,' Ltd., Vancouver. 37801. W. ,J. McMillan A Co. I Vanomver. «0 90 378021 A *C.tJn)cerv Vendom |" Nabob" Pure Lime Fruit Juice Kopa Brewrriea iMad? from the fi- I nest Lime Juice. ! Special quality Vveat India Lime J uice. 1 8 enti rely free from alcohol. Prepar'd from their original Lime .luice Syrup Re- ceipt. This cor- diaJ m*f*d. from pure iuiw of fruit free from alM)hol. '•Sovereign " L. Htm- ft Co., I. . Albert Riddell ft Co. OflOjNat. Drug Co., Van- UISTRICT OF VICTORIA- Dec. 10 10 14 14 14 Bovtlt-d Juice. liime 4lri04 W. Sjieed '3 botn. 7J Simon Leiiier ft Co., Ltd.,Victcria,B.C 41605 The Saundert Grocery; Co., Ltd. I 41606 41607 Copa.s ft Young . 1). H. R<»» * Co., I Victoria, B.C. 416(J8K. Er»kine ft Co., Victoria, B.C. 'Royal "West In- dia Lime Juice. 1 20 Evans Sona, Lescher Montserrat Lime I ft Webb, Ltd.,! Fruit Juice. I London, Kng. jOeOH. Moss, Victoria, "Royal " Wejit In- I B.C. dia Lime Juice. |0 7» Law, Young ft Co., I Montreal. ■'S.TheWest India Lime Finest West Irdia I Juice Co., St.; LimeJuiue ' Thomas, W,I. i u JVICE—CoMltided. RUVLTI) OF Analvhiii. is 8-8 X&-8 «4 ill's ■'-i ■so 'J < PrH«t)rv»tive». Reaotion «ith alcohul (after I vaiwrating to » Syrup. ) •8 k ii Keniarka and Opinion of the Chief Analyxt. .;. F. POWER, INSPECTOR. 1 0' J9j 117 Oj 8 1» j -0 3 None 10836 1060 7'66 j o! .. I 1 U236 80 R 6 C3 11392 37 6' 2 72 40-2 -36 6'SaIicyllc a^id ' present. Bulky ppte.. 1 OJoO 112 7 M +0 9 None SliKht ppte Bulky ppte 87798 37799 37800 37801 37802 (Genuine. Low in acidity. Rotation after inver»ion — 36 0. Con- tains con«idera))Ie sugar. .Sold aa a cordinl Abnormal rotation. D. O-SULLIVAN, INSPECTOR. 1 OSOOj 100 1 0345 111 1 0288^ 96 6, 6 1 03:": 114 Oi 7 1 0201 C8 4 +l-2jNone I Bulky ppte.. -tlKOtRoUtion abnormal. —0 3' „ „ . 41605 CJenuine. + 10 + 5 Salicylic acid^ trace. i 41606 Rotation abnormal. 41607jGenuine. 41608 Low in acidity, and oontaina a trace of I preservative.